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By F. Rosenblum, P. Spira

A laboratory test has been developed for assessing the patential hazard from self-heating of sulphides. The technique consists in measuring the rate of self-heating, from near ambient temperature, of a 1-kg sample in an insulated chamber controlled at standard atmospheric conditions. The rate of oxygen consumption is monitored simultaneously. The paper describes the apparatus and test procedure, and reports data on various ores and mill products. Tailings known to have caused problems underground when used as backfill have shown heating rates of over 3°C/h. A preliminary hazard rating guide for backfill based on the known behaviour of several sulphide materials is presented.

Jan 1, 1981

By H. H. Claudet

PROBABLY the first flotation mill for treating molybdenite ores was put into operation .in Norway during 1913, when the writer was employed to introduce and apply the Elmore vacuum flotation process at a mine in southern Norway. These operations proved successful and led to other similar installations in that country. It remained, however, for Norwegian engineers themselves to iron out their difficulties and establish the molybdenum industry on a basis which ultimately attained world importance. Just as today, an urgent demand for molybdenum arose during the world war of 1914-18. By 1916, many molybdenite properties were in operation in Canada and several small concentrating mills were under construction. At one of these, in the Ottawa Valley district, the opportunity came for applying the Elmore vacuum flotation process, using a flow-sheet similar to that adopted in Norway. Later, as one of the staff of the General Engineering Company, who had already developed a highly efficient flowsheet for treating molybdenite ores, using the Callow pneumatic flotation process, the writer devoted considerable time to research work and investigations on a number of molybdenite projects and deposits in eastern Canada. The bulk of Canada's production of molybdenite was coming at that time from the Moss mine at Quyon, Que., where concentration of the ore was effected by water-film flotation. It is of interest to note that this process, based on the principle of surface tension, had been developed and introduced by the late Henry E. Wood, of Denver, Colorado- one of the original owners of the Moss mine-at the time he was investigating the Elmore vacuum process in his Denver plant. The process, with certain modifications, was used at several other properties in eastern Canada, and notably in the ore dressing laboratories of the Department of Mines at Ottawa and in a plant at Renfrew, Ont., in both of which ore from deposits in various parts of Canada was treated, with recovery of very appreciable amounts o much needed molybdenite. During the summer of 1917, the water-film flotation mill at the Moss mine was dismantled and the plant was re-modelled by the General Engineering Company to include the Callow system. This installation, using improved flotation methods, was highly successful both as to recovery and grade of concentrate, and proved a decided advance in molybdenite concentration, a recovery of upwards of 90 per cent being obtained, with a concentrate grading over 90 percent MoS2.

Jan 1, 1944

By R. Y. K. Yang, O. Olajide, E. H. Cho

"This study focuses on partial leaching of coal pyrite with sodium sulfite in order to increase its degree of liberation from the coal matrix, which might help to increase the removal of coal pyrite, together with trace elements of arsenic (As), selenium (Se) and mercury (Hg) by froth flotation. The U.S. Bureau of Mines’ two-stage reverse flotation process was applied to further reject coal pyrite in the second stage, where pyrite was floated while coal was depressed. The results show that the leached coal flotation with sodium sulfite produced lower pyritic sulfur content in the clean coal by approximately 25% compared to the flotation of unleached coal. The synergism mechanism between the leaching and the two-stage flotation is delineated. The rejection of trace elements (As, Hg and Se) after the two-stage flotation process with unleached coal followed approximately that of pyritic sulfur (64.6%). However, after the two-stage flotation with leached coal, the rejection of Se was as high as that of pyritic sulfur (77.9%), while the rejections of As and Hg were 20% lower than that of pyritic sulfur, or followed approximately the same rejections obtained through the two-stage flotation with unleached coal.IntroductionSO2 is a reducing reagent, but when it is combined with oxygen in an acidic solution, it will become a strong oxidizing reagent for leaching coal pyrite. Sundaram et al. (2001) found that the reagent could leach coal pyrite to produce ferric iron, which, in turn, catalyzed the oxidation of SO2. Similarly, Cho et al. (2009) found that the reagent could leach pyrite as well as mercury from coal. In the present study, coal was preconditioned by partially leaching coal pyrite in water-coal slurry with sodium sulfite at 48° C. The partial leaching of coal pyrite may enhance its degree of liberation from the coal matrix and give a chance to be rejected more effectively during the flotation.The two-stage U.S. Bureau of Mines’ reverse flotation process (Miller, 1975) was used in this study. The first stage is conventional flotation, in which coal is floated while material with higher ash and pyrite content remains in the cell. Kerosene is used as a promoter to float the coal and MIBC (methyl isobutyl carbinol) is used as a frother. In the second stage, the floated coal from the first stage is depressed using a starch-based reagent, while coal pyrite is floated using potassium amyl xanthate. In this second stage, the liberation of coal pyrite from the coal matrix seems to be an important factor for successful rejection of coal pyrite."

Jan 1, 2015

By R. Fernando

"The National Institute for Occupational Safety and Health (NIOSH) National Personal Protective Technology Laboratory (NPPTL) is leading an effort to develop the next generation of self-escape breathing apparatus for egress from confined spaces in emergency scenarios. A backpack style closed-circuit mine escape respirator design was one configuration explored as part of the research imperative directed by the 2006 MINER Act. Stakeholder feedback from MSHA and at the NIOSH Breathing Air Supply Partnership Meeting indicated a smaller belt worn unit that does not sacrifice performance is desirable. This paper outlines some further technology advancements that may be investigated toward developing such a small-sized respirator. Technologies being considered are novel chemicals for improved carbon dioxide (CO2) absorption and oxygen (O2) production, eliminating a dedicated CO2 scrubber by incorporating its function in the spaces of the respirator’s breathing loop and storing O2 in a liquid form with long standby capabilities. When these technologies are applied to a future design, there is the possibility of having an escape respirator that can be belt worn and capable of being certified to 42 Code of Federal Regulations (CFR) Part 84 standards, including sub-part O for escape purposes including mine escape. BACKGROUND NIOSH NPPTL has a Research and Development effort to provide mine workers with state-of-the-art breathing air technologies to comprehensively support initial and continued self-escape, refuge alternatives, and rescue needs, resulting from mine emergencies. As part of this R&D effort, NIOSH invested in the development of a next-generation closed-circuit mine escape respirator (CCMER) which would be compliant with NIOSH’s respirator standard requirements, 42 Code of Federal Regulations Part 84, including sub-part O. The design features of the CCMER also address the MINER Act’s requirements for transitioning between devices without the need for doffing the initially donned device. It would also allow for improved protection when using voice communications with a donned device ."

Jan 1, 2018

By W. Miola

The MSHA prescribed method for the determination of quartz in airborne respirable dust samples from underground coal mines is the P-7 method, a combination of low temperature radio-frequency ashing (LTA) and infrared analysis (lR). There is no prescribed procedure for quartz analysis in bulk samples of coal and host rock. Dispersive Infrared (IR), Fourier-transform Infrared (FTIR), and X-Ray Diffraction (XRD) methods are most commonly used for quartz analysis in powders. Several aspects of the experimental procedures such as the analysis sample preparation from bulk samples, ashing techniques, scanning procedures, peak measurement location, calibration techniques, sample amounts, size consist, and data interpretation affect differently the results from each of the methods. Significant differences in analysis results from X-ray diffraction (XRD) and infrared spectroscopy (IR) on the same samples are reported. All these studies point to the need for reliable quartz analysis methods. In a recent research, a procedure for preparing bulk coal and host rock samples for quantitative quartz analysis was developed. Further the results from X-ray diffractometry and infrared spectroscopy for quartz content on identical samples were compared. Calibrations with pure and mixed standards were used to assess the influence of particle size distribution, matrix, and calibration on analysis results. In this paper, several issues with the measurement of quartz in the samples of coal, host rock, and airborne respirable dust from mines are outlined and quantified.

Jan 1, 1994

By C. Harry Benedict

This paper, describing the leaching practice at the Calumet and Hecla mills, Lake Linden, Mich., is one of a series on milling methods and costs being published by the United States Bureau of Mines. GENERAL DESCRIPTION The reclamation plant is located along the shores of Torch Lake at a slightly lower level than the concentrator itself. The entire location of the original concentrator, in connection with the present reclamation plant, has been ideal, lore particularly as the leaching and flotation departments are common to both units. After 15 years of operation and with the reclamation sands just a little more than half exhausted it would appear that the remaining life of the deposit could be worked by the present plan, without decided changes or renewals of plant or equipment.

Jan 1, 1930

By Jianping Li, Fei Peng, Yunbo Xu, Jiayu Li

In this study, in order to achieve ultra-high strength without reducing plasticity, a novel heat treatment involving a pre-quenching process prior to conventional intercritical annealing (P-IDP) was proposed in a low carbon low alloy DP steel. It revealed that abundant fraction of banded structure was observed after conventional intercritical heat treatment (IDP) due to the inheritance of cold rolling deformation. However, the banded structure in novel heat treatment was eliminated significantly, whilst the refined microstructure was relatively more homogeneous with ultrafine ferrite grains. Moreover, obvious chain-networked martensite grains along the ferrite grain boundaries were obtained. The optimum mechanical properties with ultimate strength of 1238 MPa, total elongation of 17%, product of strength and elongation (PSE) of 21GPa% were obtained by P-IDP treatment, which was much higher than the values reported with similar composition. As to pre-quenching treatment, all of grain refinement, homogeneous distribution of martensite islands and precipitated strengthening of microalloyed carbides were beneficial to improve the final strength and ductility.

Oct 1, 2019

By Emmanuel V. Manlapig

The variables involved in a complex process like flotation can be classified as follows: a. Disturbance variables - which are undesired properties of the process input which affect the value of the process output but which are not subject to adjustment. They are the result of changes in the properties of the feed, like changes in head grade, flow rate, fineness of grind, etc. b. Manipulated variables (sometimes referred to as process variables or control variables) -which are those that are adjusted - reagent addition, aeration, pulp level - in order to compensate for the disturbances in the properties of feed. c. Performance variables (sometimes referred to as controlled variables) -which are those whose values measure the performance of the process. They are properties of the process output such as grade and recovery. The function of a control system is to maintain the process performance equal to the control objective in spite of the disturbances by adjusting the manipulated variables. Attempts at developing automatic control systems for mineral processing operations date back to the thirties and in many of these attempts the results were not surprisingly poor and un-stable. The poor results brought indifference and suspicion towards automatic control on the part of operators and management. The reasons for the apparent failure of these attempts were two-fold: a. the lack of adequate understanding of the behavioural responses of the process from the control point of view, and b. the lack of reliable control instrumentation which could withstand the harsh environment in mineral dressing plants. Many operators had accepted the fact that control of mineral dressing could be best conducted manually. In the case of flotation circuits, control had been virtually based on the skill and experience of operators particularly their ability to identify and rectify poor flotation performance aided by results from the laboratory (chemical) analysis of regularly collected samples from strategic points in the circuit which are at best, hourly collected samples.

Jan 1, 1978

By C. S. Harloff, Frank R. Corwin

THE Nichols Copper Co., associated with the Phelps Dodge Corp. and the Calumet & Arizona Mining Co., has constructed at El Paso, Tex., and is now operating a copper refinery with a yearly capacity of 100,000 tons of anodes. Transportation facilities were perhaps the most important of the considerations that led to the selection of this site. The rapid industrial development of the Middle and Far West has increased the consumption of copper there. The advantage of local refining as against shipping the copper to the Atlantic sea- board is apparent. Copper refined in the Southwest is equally competitive for export shipment, either from the Gulf or the Pacific Coast ports. The tonnage of copper produced in the Southwest not only justifies the construction of this plant, but may warrant considerable expansion in years to come.

Jan 1, 1930

By C. Tom Blevins

The purpose of this paper is to discuss production and roof control problems associated with directional lateral stresses in an in situ stress field and the approach that Inland Steel Coal Company made in trying to cope with them. Before proceeding, a description of the mine location, product, geology, restraints, and mine history is in order. The mine is located in Hamilton County in Southeastern Illinois. It produces a high volatile metalurgical coal and is slated to produce 2.1 MTY. Product ion is in the Illinois No. 5 seam at a depth of 930 feet, approximately 490 feet below sea level. The scam height averages from 5.5 to 6.0 feet throughout the reserves with height increasing in the eastern reserve area to approximately feet and a 5 Foot average in the West. The scam tends to dip to the North, North East, but is locally very undulating. The Galatia channel washout outlines the eastern boundary of the reserves and there is a split coal area toward the central part of the property than runs south-southeast. The top above the #5 seam is laminated medium gray shale called Dykersburg. Individual shale bedding planes vary locally From ½ to 1" in thickness to a more normal thickness of 1 to 1 ½ with some areas being interlayed by thin carboncous material. The top normally must be considered as materially competent. Even though the mine is still relatively small in area with only 1.3 million tons of total production to (late, we have encountered dense zones of slicker sides and premining, stress cracks (joints). There are also areas of siltstone, that vary from a few inches to several feet thick, and areas of rider coal, clay instrusions, and rolls. We have crossed lineament concentrations that show strong evidence of corelation to localise top problems. These are being monitored closely to see their predictability on our present and future mining conditions. The face cleat runs N 55° E and butt cleat runs S. 25° E. On a regional basis, there are several anticlinal belts that trend in a northerly direction. The one major restraint is that Inland does not own surface subsidence rights. Therefore, a partial extraction mining plan is being followed. The Holland-Gaddy formula for pillar strength design is used to calculate theortical pillar sides. When production began in March of 1979, it was noted that ground control problems occurred as we drove north entries. East-west cross cuts tended to have better working conditions. This phenomia occurred from a couple hundred feet, but seemed to dispate as we got away from the men and material shafts. Once the production shaft was connected and enough entries extended for installation of belts, ground control problems were again experienced in north-south headings. It was also observed that when mining north-south headings with east-west crosscuts, if the crosscut was driven through ahead and supported, the intersection was stable upon entry connection. This held true even where fairly extreme ground control, problems were encountered. The reverse held true. when driving east-west headings with north-south crosscuts. At this time, we started searching in earnest for a working theory to explain this roof phenomia. It also became the first step of what eventually was a four step sequence to derive a workable solu¬tion to the problem. The combination of the many geological changes and the fact that north-south condition was at times intermitent, helped to disguise the stress field. The mine also being in a fairly virgin area with no mines in approximately 25 milt, radius, meant we didn't have a reliable case history to examine. Various theories were researched before it was concluded that our primary ground control problem was a directional lateral stress Field, with the major stress axis in an east-west direction. The second stop of the procedure was then to test. mining methods and determine if these stresses could be modified to a

Jan 1, 1982

By H. J. Handewith

"After having performed qualitative and quantitative tests on nearly 550 rock specimens from tunnel projects throughout the world and comparing the results with actual boring in eight distinctly different rock types which varied in compressive strength from 12,000 to over 34,000 psi, it has been concluded that any rock -andesite, granite and even taconite -can be machine-bored. The question is -can it be bored economically? The intent of this paper is to delineate the investigative needs to accurately and reliably answer this question. A piece of NX core in the hand represents less than 50 per cent of the worthwhile geologic information that could have been obtained from a given core hole. A thorough site investigation by competent personnel can gene-rally foretell to what extent, if any, varying geologic conditions will hinder machine progress.A laboratory testing technique has been developed that has been correlated well (80 to 120 per cent) with actual boring results. This technique will be discussed in detail. Rock cutter life is a function of the penetration rate and the forces required to sustain that rate. Cutters are now, and will be for .some time to come, the single, most expensive consumable item involved in continuous tunneling in hard rock. It is by strict attention to predicting these rates and forces that tunneling costs can be optimized."

Jan 1, 1970

By Markus Aspiala, Fiseha Tesfaye, Pekka Taskinen

In this paper, the standard thermodynamic properties of Ag3Sb and Ag6Sb intermetallic compounds have been studied by the solid state EMF-method, using Ag+ ion conducting β- alumina and AgI. The intermetallic compounds were synthesized from pure substances in evacuated silica ampoules and their formation were confirmed by the SEM-EDS analyses. The EMF measurements were made on electrochemical cells of the type [Ag | β-alumina | Ag-Sb] and [Ag | AgI | Ag-Sb]. The usage of β-alumina electrolyte, in this study, enabled thermodynamic measurements of the Ag-Sb-intermetallic compounds above 710 K, hitherto unreported. Based on the new experimental data, thermodynamic properties of the Ag-Sb-intermetallic compounds have been determined. The obtained experimental values have been compared with the available literature data.

Jan 1, 2015

By Breno T. Maia, Débora C. O. Silveira, Mariana A. Ribeiro, Daniel A. G. de Carvalho, Roberto P. Tavares, Raissa S. Salgado

Mixing time is an important parameter when considering chemical and thermal homogenization in steelmaking reactors. It can also be relevant in the kinetics of chemical reactions. Different methods have been used to estimate mixing times in physical models of steelmaking reactors. In the present work a new method to estimate mixing times in physical models has been proposed. This method can be used when transparent fluids are used to simulate the liquid steel and the slag. Results of mixing times in a physical model of a BOF obtained with different techniques were compared. It was shown that the new method is more reliable and consistent than the common methods based on electrical conductivity measurements and colorimetric analysis.

Oct 1, 2019

By Ulf Nyberg, Changping Yi, Daniel Johansson, Håkan Schunnesson

To investigate the non-ideal detonation properties of aluminized emulsion explosive, a series of tests for an emulsion explosive with 5% aluminum powder additive were carried out with mortar confinement. The velocity of detonation (VoD) and the curvature of the detonation front for different charge diameters were obtained from the tests with a high-speed camera. The burning process of the aluminized emulsion explosive has been modelled with the ignition and growth (I&G) flow model in the LS-DYNA code. A routine based on the optimization program LS-OPT code was developed to identify the parameters in the burning rate function with the detonation velocities and the front curvature radii from two tests. A Perl code was implemented in the routine and was used to calculate the VoD, fit the detonation front and obtain the detonation front curvature radii. The calibrated parameters were used to predict the VoDs and the detonation front curvature radii for the rest cases. The results indicate that both the VoDs and the detonation front curvature radii from the numerical modelling are in good agreement with the experimental results. The numerical results also indicate that the variety of the burn fraction and the peak pressure with the change of charge diameters is reasonable with the calibrated parameters.

By Ulf Nyberg, Changping Yi, Daniel Johansson, Håkan Schunnesson

To investigate the non-ideal detonation properties of aluminized emulsion explosive, a series of tests for an emulsion explosive with 5% aluminum powder additive were carried out with mortar confinement. The velocity of detonation (VoD) and the curvature of the detonation front for different charge diameters were obtained from the tests with a high-speed camera

Feb 1, 2020

By Alan P. Prosser

The heap leaching of gold ores by cyanide solution was simulated by computer program. The program uses only basic m1neralogical and chemical data; no process testwork data, such as column leach results, are required. The simulation can be used to forecast the consequences of various changes before and during the testwork, design and operation stages of a particular ore-process system. Also, data about the state of different parts of the heap at various times help create an understanding of what is happening. The effects of mineralogical and process variables on the overall performance of the ?heap leaching process are illustrated. Comparisons are made to column leach tests and production data. The potential of the simulation strategy is discussed for making better use of operating experience and for suggesting specific research objectives. It has become clear that more attention should be paid to other metals that dissolve in the solution.

Jan 1, 1989

By J. Asfahani

"The Schlumberger configuration used in geoelectrical sounding is slightly adapted here to obtain reliable data for both shallow and deep penetration depths from the same survey. In this configuration, two kinds of current electrode half-spacings are used: the first enables construction of vertical electrical resistivity sounding (VES) curves for shallow depths (<50 m), and the second for depths =250 m. For a given VES location, two field curves are measured and interpreted using two standard approaches. Practical characteristics of such a modified configuration are illustrated with two field applications in Syria. The first aims to characterize the structure of Quaternary and recent deposits in the Al-Ghab depression region, and the second deals with exploration for phosphatic sedimentary units in the Al-Sharquieh mine. La configuration de Schlumberger normalement employée dans les levés géoélectriques a été légèrement modifiée afin d’obtenir des données fiables à faible et forte profondeur durant le même levé. Dans cette nouvelle configuration, deux types de demi-espacements des électrodes sont utilisés : le premier permet le développement de courbes de sondage de résistivité électrique verticales (REV) pour les faibles profondeurs (<50 m), et le second atteint des profondeurs =250 m. Pour une localité REV donnée, deux courbes de champs sont donc mesurées et interprétées grâce à deux approches standardisées. Les caractéristiques pratiques de cette configuration modifiée sont illustrées par deus exemples d’application en Syrie. Le premier vise la caractérisation de la structure des dépôts Quaternaires et récents de la région de la dépression d’Al-Ghab, et le second traite de l’exploration pour des unités phosphatiques sédimentaires à la mine Al-Sharquieh."

Jan 1, 2009

By K Zunica, A R. Penney

The principles of three-dimensional geological modelling are well understood and routinely used. Sample data is collated and geostatistical tools used to ensure that sample data is suitable for its end use, which is typically a block model that is appropriate for mine planning. What has become increasingly apparent is that physical rock properties and geotechnical parameters need to be incorporated into the three-dimensional geological model to create an integrated mine model.The approach to the collection of geotechnical information is not as highly prescribed and controlled as collection of geological data. Commonly, the geotechnical data set is incomplete and inconsistent, with little consideration of what the end use will be by those collecting the data, or how the geotechnical data might relate to the geological data. In some cases, specific geotechnical investigation programs are completed, yet correlation between those programs and previously collected data is rarely undertaken to the same level of diligence as found in the geology field.There are some obstacles that need to be considered when attempting to incorporate geological parameters, such as grade, lithology, and geological domains with geotechnical information such as rock quality designation (RQD), rock mass rating (RMR), rock strength, and geotechnical domains into the same three-dimensional block model. Interpolation or geostatistical estimation methods used for grade estimates might not be appropriate for many components in rock characterisation, particularly search geometries. A number of examples are provided to illustrate issues underlying some of the data collection procedures, and their effects on three-dimensional geotechnical modelling.The example presented attempts to highlight generally observed shortcomings in the collection of geotechnical information, parameters which need to be considered when combining geological and geotechnical data into the same model, and the benefits of having a combined block model from the beginning of a project.CITATION:Zunica, K and Penney, A R, 2014. Integration of geological and geotechnical data for three-dimensional modelling, in Proceedings Ninth International Mining Geology Conference 2014 , pp 291–298 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 18, 2014

By John A. Organiscak

The Bureau of Mines conducted a survey of eight shearer longwall operations to identify factors that affect respirable dust generation from longwall roof supports. The longwalls surveyed were in coal seams located in different geographic regions of the United States. Data were collected on mining (geologic) conditions, support design, operational characteristics, and amount of respirable dust generated from roof supports. Analysis indicated that mining conditions are the main factors that affect the generation of dust during roof support movement. Both roof strength and depth of cover above the coal seam showed relationships with the amount of support dust generated. Several practices are currently employed to effectively control roof support dust; however, some of these controls are limited. More research and development is needed to improve dust control technology for longwall roof supports.

Jan 1, 1985

By R Gilbertson, N Freeman

Metallurgical accounting is key to the control and production planning process of any mining operation. This is even more crucial for complex operations involving mining, concentration, smelting, refining and marketing. The tracking of multiple metal product and contaminant components through the operation can improve process predictability and inventory management. Appropriate use can be made of æhigh quality dataÆ for strategic reserve utilisation, mining operations, milling operations, etc. This information enables the optimisation of all aspects of the mining and processing operations. This case study discusses a metal balance implementation for WMCÆs Olympic Dam operations; a large integrated mining, concentration and refining operation, which used an existing off the shelf statistical data reconciliation package developed for the oil industry. It was extended to track and balance the metal co-products across the entire integrated mining, mineral processing and refining plant. The key benefits discussed are tight integration with existing data collection systems, formalisation of previously informal processes, and leveraging the development and support available for a widely used package. The project provided a solution for the site metallurgical balance spanning the mine and processing plant. The solution facilitates a bridge between the planning and production worlds, using a common data model across the site.

Jan 1, 2002