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With the iron ore industry in Australia producing hundreds of millions of tonnes of ore per annum, the associated costs of these operations extend into the billions. It is no surprise in the current economic climate that more and more companies are looking into different ways of optimizing their costs to keep their sites operational. One way of improving operations is the use of electronic initiating systems like i-kon and Uni tronic detonators. These systems have been used around the world to improve current practices and optimize drill and blast costs. However, these systems have yet to make an impact upon the iron ore sector in Australia. Some of the potential improvements include:pattern expansion and a subsequent reduction in drilling and explosive costs;improved fragmentation and hence increased dig rates, thereby driving $/tonne down;embracing the 'mine-to-mill' concept by reducing the downstream costs of crushing and milling;improving the overall condition of pit walls and floors, leading to a safer working environment in which optimal haulage performance can be achieved; and improvements in vibration management around heritage sites and critical infrastructure, thereby saving the cost of relocation works. This paper introduces some of these concepts and the process of making the changes leading to potential savings from the improvements, using various examples as proof of the concepts.

Jan 1, 2009

By AIME AIME

MINING geology has been at once the vocation and avocation of John M. Boutwell, newly elected Director of the Institute representing Utah and Colorado. Geologists were looked at askance by most of the "big" men in mining when, from 1896 to 1900. Mr. Boutwell was teaching geology at Harvard, his alma neater; and his success in applying geologic principles to the business of finding ore contributed much to changing the attitude of scepticism. From 1900 to 1908 lie was with the U. S. Geological Survey, with service in Bingham, Utah; Morenci, Ariz.; and Park City, Utah. Since then he has been engaged in private practice as a consulting mining geologist retained by many of the leading mining companies. A dozen men now recognized as outstanding geologists got their early

Jan 1, 1937

By Leonard Obert

THIS REPORT presents methods and principles useful in designing underground mine openings and pillars in competent rock formations. Two types of formations are considered: (1) Massive formations, in which openings are generally mined with an arched roof, and (2) bedded formations, in which openings are generally mined with a flat roof. Design principles for openings and pillars in massive formations are obtained by considering the maximum tangential stresses developed around single and multiple openings for stress fields of various types. Design principles for openings and pillars in bedded formations are obtained by considering the average stress in pillars and the maximum stresses in roof layers. Experimental procedures for making stress, strain, and in situ physical-property measurements in underground mines to check design calculations are outlined and the results discussed.

Jan 1, 1960

By Shillabeer J

Paste backfill has been adopted by many underground mines in North America and a growing number elsewhere. Paste offers a number of advantages. This paper suggests wider applications of paste technology to surface tailings disposal and water management. Advantages include improved overall stability, potentially easier permitting, smaller water inventory and earlier reclamation. It may be feasible to use the same plant to prepare backfill and to dispose of surplus tailings. Example cost models are given to illustrate potential applications.

Jan 1, 1998

By S C. Dominy

Current and proposed methods of resource classification relate to the geological, economic and technical confidence in the estimated resource. Geological confidence is, however, only vaguely defined. It is largely related to the level of drilling and sampling, to the geologistÆs perceived level of confidence in his/her work and on the continuity of the mineralisation. Rarely has any real attempt been made to assess how well a deposit has been explored, sampled and evaluated and how accurate or realistic the geological model is for the deposit. This contribution reviews the impact of two of the potential sources of error, ie sample recovery and quality. The first of these parameters is measured during logging and assaying, but is often forgotten during grade and tonnage estimation, and resource classification. Preliminary studies have shown that modelling of this parameter is a valid exercise, which should accompany the evaluation of grade and other economic parameters. The sample recovery factor for an ore block can then be used to reassess the confidence in the block. It could, for example, downgrade the status of a Measured Resource to an Indicated Resource even though standard methods might indicate that the higher classification is applicable. A method is proposed by which this recovery factor could be incorporated into current resource classifications producing a more sophisticated and comprehensive measure of sample quality. A review of the sources of error naturally leads to the assignment of scores to each stage of the evaluation process, depending on the methods used and assumptions made. Sample recovery is one important factor, which is likely to appear at several stages. These scores can then be weighted and combined in a manner resembling that used in the CSIR Rock Mass Classification. This score will then allow the resource estimate to be rated on a scale from 0 to 100 per cent to produce a Quality Control Index (QCI). However, this index must then be modified using an Evaluation Difficulty Index (EDI), which reflects the difficulty of a particular style of mineralisation to accurate resource estimation. This results in the production of a Resource Reliability Rating (RRR), which can then be linked to international classifications, such as the 1999 JORC; 2000 CIM; and 2001 EURO codes. This will permit a more precise definition of geological confidence levels or, combined with estimation error, produce a classification system in its own right. This same rating can also be used as the basis for technical audits of mineral projects.

Jan 1, 2002

By Marcos V. F. Fonseca, Djalma Souza, Luiz G. X. Borges, Sergio Monteiro, Caroline G. de Oliveira, Ygor M. de Moraes, Janine F. de Deus, Frederico M. Margem

Recently, the natural fibers have been studied as alternative reinforcement material to the use of synthetic fibers. Aiming to improve the properties of natural fibers composites, it is investigated the use of natural fibers fabrics, since they provide multidirectional reinforcement and enables the introduction of a larger fiber volume fraction. In this work, it was investigated the tensile behavior of the epoxy matrix composites reinforced with different volumefractions offabric made of Ramie, a highly resistant lignocellulosic fiber. The specimens were made by pressing the fabric with liquid resin to guarantee total impregnation, and then cutting the fabric in the mold format. Finally ,the fabric layers were placed into the mold with the liquid resin and catalyst. They were cured for 24 h and tested. The results revealed an increase in the tensile strength and almost no effect in the elastic modulus with the increase of fabric volume fraction.

Mar 1, 2017

By Mine F. J, Woods P. H

The Top End of the Northern Territory lies in the monsoonal zone and receives rain during the November-April period. Initially, at the start of the wet season, rain storms are localised, but, following the descent of the monsoonal trough from below the equator, widespread rain occurs. Overflow incidents at mine sites tend to arise midway through the annual wet season when excess water accumulated in ponds begins to discharge to the external environment. Remote-access monitoring may be undertaken at mine sites using equipment to continuously measure water quality parameters with storage of the information on a data logger. The data is then retrieved by visiting the site and transferring it to a portable computer or by remotely accessing the system using a telemetry system and transmission via telephone, VHF/UHF or satellite. Such systems are readily available and vary in cost depending on the sophistication of the data transfer system. Available sensors for continuous monitoring include those for conductivity, temperature, pH and other ion selective electrodes, eg nitrate, and water level. Of these variables, conductivity is most useful due to its inherent accuracy and stability of reading. Remote monitoring capability is able to provide: (i) more intensive monitoring of key issues; (ii) more timely information; (iii) correct perspective on the degree of environmental problem; and (iv) information from remote locations, which would be difficult to monitor by more conventional methods. Examples are given for applications of continuously logged measurement of conductivity of waters discharging to drains and in creeks at Pine Creek, Ranger, Nabarlek and Woodcutters mines in the Northern Territory. These applications demonstrate the timeliness of the continuous monitoring technique.

Jan 1, 1994

By S. J. Schatzel, R. B. Krog, H. Dougherty

Longwall face ventilation is an important component of the overall coal mine ventilation system. Increased production rates due to higher-capacity mining equipment tend to also increase methane emission rates from the coal face, which must be diluted by the face ventilation. Increases in panel length, with some mines exceeding 6,100 m (20,000 ft), and panel width provide additional challenges to face ventilation designs. To assess the effectiveness of current face ventilation practices at a study site, a face monitoring study with continuous monitoring of methane concentrations and automated recording of longwall shearer activity was combined with a tracer gas test on a longwall face. The study was conducted at a U.S. longwall mine operating in a thick, bituminous coal seam and using a U-type, bleederless ventilation system. Multiple gob gas ventholes were located near the longwall face. These boreholes had some unusual design concepts, including a system of manifolds to modify borehole vacuum and flow and completion depths close to the horizon of the mined coalbed that enabled direct communication with the mine atmosphere. The mine operator also had the capacity to inject nitrogen into the longwall gob, which occurred during the monitoring study. The results show that emission rates on the longwall face showed a very limited increase in methane concentrations from headgate to tailgate despite the occurrence of methane delays during monitoring. Average face air velocities were 3.03 m/s (596 fpm) at shield 57 and 2.20 m/s (433 fpm) at shield 165. The time required for the sulfur hexafluoride (SF6 ) peak to occur at each monitoring location has been interpreted as being representative of the movement of the tracer slug. The rate of movement of the slug was much slower in reaching the first monitoring location at shield 57 compared with the other face locations. This lower rate of movement, compared with the main face ventilation, is thought to be the product of a flow path within and behind the shields that is moving in the general direction of the headgate to the tailgate. Barometric pressure variations were pronounced over the course of the study and varied on a diurnal basis.

Jan 1, 2018

By S. J. Schatzel, R. B. Krog, H. Dougherty

Longwall face ventilation is an important component of the overall coal mine ventilation system. Increased production rates due to higher-capacity mining equipment tend to also increase methane emission rates from the coal face, which must be diluted by the face ventilation. Increases in panel length, with some mines exceeding 6,100 m (20,000 ft), and panel width provide additional challenges to face ventilation designs. To assess the effectiveness of current face ventilation practices at a study site, a face monitoring study with continuous monitoring of methane concentrations and automated recording of longwall shearer activity was combined with a tracer gas test on a longwall face. The study was conducted at a U.S. longwall mine operating in a thick, bituminous coal seam and using a U-type, bleederless ventilation system. Multiple gob gas ventholes were located near the longwall face. These boreholes had some unusual design concepts, including a system of manifolds to modify borehole vacuum and flow and completion depths close to the horizon of the mined coalbed that enabled direct communication with the mine atmosphere. The mine operator also had the capacity to inject nitrogen into the longwall gob, which occurred during the monitoring study. The results show that emission rates on the longwall face showed a very limited increase in methane concentrations from headgate to tailgate despite the occurrence of methane delays during monitoring. Average face air velocities were 3.03 m/s (596 fpm) at shield 57 and 2.20 m/s (433 fpm) at shield 165. The time required for the sulfur hexafluoride (SF6 ) peak to occur at each monitoring location has been interpreted as being representative of the movement of the tracer slug. The rate of movement of the slug was much slower in reaching the first monitoring location at shield 57 compared with the other face locations. This lower rate of movement, compared with the main face ventilation, is thought to be the product of a flow path within and behind the shields that is moving in the general direction of the headgate to the tailgate. Barometric pressure variations were pronounced over the course of the study and varied on a diurnal basis.

Jan 1, 2017

By M. Olalde, I. Watson

"The consequences of ineffective mine closure in South Africa are evident from the number of abandoned mines and operations on extended care-and-maintenance, the on-selling of mines to less well-resourced companies to close, and increasing illegal mining activities. However, the data to substantiate these observations and provide insight into the underlying issues has not been available. Through the Promotion of Access to Information Act, a list of mine closure certificates applied for between 2011 and 2016 and a list of certificates granted over the same period for all nine regions of South Africa was obtained. From the analysis of this data, we show that the mine closure system as implemented in South Africa is largely ineffective. Although closure certificates are being granted, these are for prospecting sites and small-scale mines, which have a relatively small environmental impact. No large mines of any environmental significance were relinquished over the period under review, with very few applying for closure certificates. Furthermore, the issuing of closure certificates varies significantly between regional offices, with the success rate for applications being generally low and issuing of certificates taking an extended period. IntroductionThere are a number of concerns with the mine closure process as practiced in South Africa, and these have largely been laid at the door of government. Alberts et al. (2017) stress that the legislation generally conforms to international best practice. However, the system is ‘complex and unwieldy’, involving various pieces of legislation and different government departments with overlapping requirements and different interpretations of the law. A further area of concern is the capacity and competence of government to implement legislation. The ‘shortage of relevant mine closure skills and knowledge within the regulator’ was identified by van Druten and Bekker (2017) as a key contributor to unsuccessful closure. Lack of capacity and resources within the regulator has also been highlighted by Botham, Kelso, and Annegarn (2011) and Milaras, McKay, and Ahmed (2014). A recent study of the mineral application process by Corruption Watch (2017) indicates that positions in the regulator have been frozen for many years, leading to a shortage of staff, and that unqualified individuals have been appointed. There is also the perceived reluctance of government to grant closure in order to limit transfer of the liability to the state and delay the inevitable job losses."

Jul 1, 2019

By Zhang Wengang, L. John Endicott

The properties of many geological materials are variable. This is especially true for variations in elevation of the top of rock profile, strength of weathered rock, and conductivity of rock masses. Often the site investigation stage is completed by site specific ground investigation utilizing boring, sampling, and testing. Statistically this is a sampling procedure, but the borings are often widely spaced, and ground conditions between borings are deduced by interpolation. Often budgets are a limiting restraint and the information that is obtained may be less than desired. Sampling and testing is often biased. If claims for unforeseen ground conditions are to be avoided, the properties of the ground should be adequately identified. This paper describes how data can be used to evaluate the subsurface top of rock profiles, and can give insight into representative, maximum, and minimum strengths, and variation in conductivity relating to inflow of water into excavations, that can assist in planning the works and also in resolution, or avoidance, of disputes about unforeseen ground conditions. INTRODUCTION The mechanical properties of the ground are naturally variable. The work of Geologists, Engineering Geologists and Geotechnical Engineers is fundamentally investigative. Frequently, budgets for ground investigation are squeezed, resulting in widely spaced boreholes, with conditions between them determined by interpolation. Profiling can be adopted but the measurement, such as seismic velocity, is used as an indirect means of computing in-situ profiles and mass properties. Often a lot of test data are generated on large projects or by many projects in the same vicinity. Published data enlarge the database for a given project, and databases can be interrogated to gain insight into different categories of ground. Integration with geological studies can then lead to more reliable characterization of the ground in terms of identifying the materials present, their extent and their range of properties. This paper focuses on properties of rocks that are generally required for ground engineering, namely the top of rock profile, the unconfined strength of rock materials, and the mass conductivity. Data are obtained from Granodiorite and Granite in Hong Kong, and from Granite and the Jurong Series of weakly metamorphosed sedimentary rocks in Singapore. All four rock types have been tropically weathered, resulting in widely varying top of rock profiles, material strengths and mass conductivity. With a wide range in values for these parameters, project specific ground investigation conducted within a limited budget may run the risk of falling short of obtaining sufficiently reliable data sets, resulting in risk that unforeseen ground conditions may be encountered.

Jan 1, 2019

By Rolf Andreas Lauten, Yanhong Wang, Yongjun Peng

"In mineral flotation, bentonite as a kind of clay mineral imposes deleterious effects on the flotation of valuable minerals, possibly through its ability to increase the pulp viscosity. A higher viscosity lowers the amount of froth and affects the bubble-particle collision frequency. A previous study found that adding gypsum to a bentonite-ore mixture lowered the viscosity, possibly by inhibiting the formation of interconnected network structures. In this study, sulfate as an anion with different types of cations, Na+, K+, Mg2+ and Ca2+ were used to reduce bentonite viscosity and to improve flotation performance. It was found that at the same concentration, MgSO4 was the most effective salt in reducing bentonite suspension viscosity, while CaSO4 was not as effective likely due to the lower solubility of CaSO4. Na2SO4 and K2SO4 reduced bentonite suspension viscosity at high concentration. Flotation kinetics of ore blended with bentonite was increased with increasing the electrolytes concentration, which generally correlated with the reduction of bentonite viscosity. Meanwhile, significant discrepancies were found between flotation results and rheological measurements in the presence of monovalent ions. It is indicated that the morphology of bentonite aggregates in electrolytes solution is likely to influence the hydrodynamics in the froth zone.INTRODUCTIONClay is present in many ore bodies as a gangue mineral. Presence of clay presents several challenges in the processing of valuable minerals. They are soft compared to valuable minerals, which means that during grinding of the ore, clay particles are likely to obtain a smaller particle size than the valuable mineral. Often clay particles may be within the colloidal size domain (<20 µm). The smaller size increases the probability of entrainment in the concentrate. Another challenge is their anisotropic charge distribution, where depending upon the pH, edges (E) and faces (F) carry charges of opposite sign. This facilitates formation of aggregation structures that may impede percolation of bubbles through a froth, but also increase the viscosity more than expected from the mere change in volume fraction. In addition to lowering the froth mobility, a high slurry viscosity will have implications for the gas dispersion in the flotation column as it affects the dispersion of the suspended particles, and it modifies the bubble-particle collision rate and attachment efficiency (Bakker, Meyer, & Deglon, 2009; Shabalala, Harris, Leal Filho, & Deglon, 2011). A pragmatic approach to this problem is to blend high clay ore with ore of lower clay content, reducing the overall clay concentration. Alternatively, one may lower the solids content of the flotation slurry to counteract the viscosity-building properties of clay. While feasible, this approach has the disadvantage of increasing required flotation volume, and it also affects the properties of the froth. Thus, there are currently limited options in lowering the impact of clays and their tendencies to increase viscosity in flotation slurries."

Jan 1, 2016

By D Engelhardt, G Lane

The Cadia mine has shifted from an open pit operation to the Cadia East underground panel cave. The resulting increase in milled tonnes, more competent ore and the decrease in fines production through shifting to panel caving were predicted to require an increase of over 25 per cent in installed power. This expansion was accomplished via the installation of secondary and high pressure grinding rolls (HPGR) crushing of the ore, with the semi-autogenous grinding (SAG) mill receiving a combination of primary, secondary and HPGR crushed feed. This design, criteria and rationale for selection was presented at the SAG Conference 2011. This paper reports on the initial impact of secondary and HPGR crushing on the circuit performance with the new panel cave feed.CITATION:Engelhardt, D, Lane, G and Powell, M S, 2014. Cadia expansion – the impact of installing high pressure grinding rolls prior to a semi-autogenous grinding mill, in Proceedings 12th AusIMM Mill Operators’ Conference 2014 , pp 233–240 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Sep 1, 2014

By Hans Jahncke G

El petróleo se forma por rocas porosas, que al producirse se llaman los "reservorios de petróleo". Por lo cual este debe poseer intersticios entre las partículas sólidas, que acumulen ciertos fluidos. Empero este no es el único fluido encontrado, sino que pueden contener aguas, gas, en tanto solución del petróleo libre. En este sentido, el objetivo del texto es señalar el funcionamiento del laboratorio de reservorio, en tanto determine estas propiedades, las cuales son básicas en todos los cálculos de reservorios, determinación de reservas, desarrollo de la producción y las posibilidades futuras de recuperación secundaria. Las funciones del Laboratorio de Reservorios de la International Petroleum Company se dividen en dos partes: El primero refiere el trabajo de campo, que incluye obtención de registros de presión, temperatura y determinación de niveles de fluido en los pozos y el segundo, los trabajos de laboratorio propiamente dichos como la determinación de las propiedades físicas de las rocas del reservorio y de los fluidos que contiene. Estos a su vez comprenden la saturación y permeabilidad. En cuanto a los trabajos de muestras de petróleo del subsuelo, encontramos factores como la presión de saturación, relacion de gas-petróleo, volumen de formación y viscocidad. Asimismo los análisis de trabajos de muestras de gas se realizan mediante el desplazamiento de fluídos por inyección de agua.

Jul 20, 1956

By K. A. Jackson, G. A. Chadwick, A. Klugert

The diffusion field ahead of a lamellar interfnce is analyzed using an electrical analog. A self-consistent solution is obtained for the shape of the interfnce and the diffusion field by an iterative process. The solutions presented here are for a 50-50 eutectoid or eutectic, The shape of the interface is found to he independent of growth velocity and lamellar spacing, and to depend on the relative values of interfacial free energies at the phase houndaries . The mode of growth of lamellar eutectics and eutectoids has been a subject of much interest for many years.1-4 Mehl and Hagel 1 have shown photomicrographs taken by Tardif when he attempted to determine experimentally the shape of an advancing pearlite interface; the results are completely ambiguous. Brandt&apos; and schei13 have made approximate calculations of the composition ahead of a lamellar growth front. The shape of the advancing front and the composition distribution ahead of the front are difficult to calculate because one depends on the other. It is the purpose of the present paper to describe a method by which this calculation has been done. Lamellar-eutectic growth usually occurs under conditions where the growth is fairly rapid, and the interface temperature is close to the eutectic temperature. The growth rate is usually determined by heat flow. Eutectoid growth, on the other hand, can best be studied by quenching to some temperature, and allowing growth to proceed isother-mally. In both cases the growth is believed to be controlled by diffusion* rather than by the atomic kinetics of the transformation. This being the case, a single treatment of the diffusion equation will apply to both cases, provided the region of the interface in a eutectic may be considered to be isothermal. If a part of the interface could appreciably change its thermodynamic driving force by advancing ahead of or lagging behind the mean interface, then the two cases would not be similar. Eutectics normally grow in temperature gradients of the or-der of a few degrees per centimeter. The normal eutectic spacing is the order of a few microns. Part of the interface would have to extend many lamellar spacings ahead of the mean interface before it experienced sensibly different conditions. The interface temperature is usually a few tenths of a degree below the eutectic temperature so that temperature differences of the order of one-thousandths of a degree (a displacement of one lamellar spacing) would be unimportant. Protrusions large compared to the mean spacing do occur when one phase only grows into a eutectic liquid. This is usually a dendritic type of growth, and easily distinguishable from the lamellar mode of growth. A single treatment of lamellar growth will apply equally well to both eutectic and eutectoid decomposition. At the interface, which as shown above is essentially isothermal, the difference between the equilibrium eutectic temperature Teu and the actual interface temperature Ti, can be divided into two parts: 1) the composition varies across the interface, so that the local equilibrium temperature is not Teu; and 2) the interface is curved, so that the local equilibrium temperature is depressed according to the Gibbs-Thompson relationship. This undercooling can be written as Teu-Ti =?T = mAC(x) + a/r(x) [1] where ?C(X) is the departure of the composition at a point x on the interface from the eutectic composition, see Fig. 1, r(x) is the local radius of curvature at a point x on the interface, m is the slope of the liquidus line on the phase diagram, and a is a constant given by where s is the interfacial free energy, TE is the equilibrium temperature, and L is the latent heat of fusion. The calculations in this paper will be made only for the case where the phase diagram is symmetric, that is, the eutectic occurs at 50 pct, the liquidi have the same magnitude slope m at the eutectic temperature, and C,, the amount of B rejected when unit volume of a freezes, see Fig. 2(a), is the same for both phases. As shown in Fig. 2(b), the composition ahead of the a phase will be rich in B, the composition ahead of the ß phase will be rich in A. The composition at the phase boundary is the eutectic composition. The difference between the local liquidus temperature and the actual tempera-

Jan 1, 1964

By Felix Wolters, Michael Schütt

In over 40 years of operation, engineers at Aluminium Oxid Stade GmbH (AOS) have acquired a lot of experience whereby they have developed a series of optimizations regarding the specific primary energy consumption. The tube digester technology, invented by VAW in Germany and applied on an industrial scale for the first time in Stade, was brought to perfection by its innovative cleaning methods, which led to a constantly high heat transfer, low pressure loss and excellent availability of the digesters. Further improvements such as the heat recovery from the exhaust gas stream of the salt heater as well as the optimization of one of the fluid bed calciners and the installation of a combined heat and power generator (CHP) led AOS to where it is now—a leading alumina refinery with regard to the lowest energy consumption per ton of alumina.

Mar 1, 2017

By Carl Faessler

Abstract Some Canadian geologists believe chat, in the Grenville sub-province of Eastern Canada, there is no granitic intrusion older than the anorthosite. The writers are among those who hold the contrary view. They suggest a new means to distinguish between rocks belonging to intrusions respectively older (Laurentian) or younger (Pine Hill) than the anorthosite. This new method is based on microscopical observations which demonstrate that the Pine Hill intrusives contain a large amount of exsolution perthite, whereas the Laurentian intrusives are completely devoid of exsolution perthite. Where perthite is present in Laurentian rocks, it is the result of lacer hydrothermal replacement. Introduction The present paper is the result of a systematic study of some acidic intrusive rocks in the Grenville sub-province. These rocks underlie large areas of the Canadian shield in the Province of Quebec, mostly along the southern border of the shield.

Jan 1, 1946

By B. Csoke

The Bond and the Hardgrove methods are widely used for the determination of the material?s grindability. Generally, the determination of the Bond work index of inhomogeneous materials can be carried out with high deviation using the conventional apparatuses and methods, because of the highly different grindability of components. This is more significant when the composite cement?s grindability is measured, which highly affects the design and operation of cement grinding mills. A possible solution can be the combined application of the Bond-method with the determination of the component?s weight ratio in the product and perform the Bond measurement until the steady state conditions of grindability coefficient (G) and chemical composition of the components are reached. To prove the applicability of the above mentioned idea systematic Bond and Hardgrove grindability tests were carried out of two phase composite materials. The experimental results showed that the application of the combined procedure is proven in order to have a more accurate and reliable calculation of the Bond work index of composite materials, especially when the components have significant difference in the grindability and concentration. The measurements also showed the possibilities and limits of the grindability test methods.

Sep 1, 2012

By H. A. Bedworth, W. H. Bassett

The amount of oxygen present in refined copper bears an important relation to the effects of various impurities on physical properties of copper, as well as the effects of reducing gases at higher temperatures. It seems fitting at this time, when the effects of reducing gases on copper are being discussed, to describe methods that have proved satisfactory for the determination of oxygen and sulfur, and to present some results obtained by investigation of these methods in the authors&apos; laboratory. The procedure for the determination of sulfur is closely interrelated with that for oxygen and has, therefore, been included. It was first proposed by Hampe1 that oxides in copper could be accurately determined by the loss in weight sustained by finely divided copper when reduced at red heat in pure hydrogen, or by the weight of water produced. Hampe&apos;s method was later modified by Archbutt,2 who established the accuracy of the method and demonstrated that equally accurate results were obtained by noting the loss in weight or by weighing the water formed. The determination of oxygen by heating in carbon monoxide has been proposed by West.3 In our hands this method has given slightly lower results than obtained by heating in hydrogen. Heath4 found that the loss in weight after heating in hydrogen did not represent the true oxygen as cuprous oxide but included also gases derived by the metal from the fuel and refining in the furnace, and any trace of mechanically held moisture. He found, further, that the copper after ignition retained hydrogen equivalent to about 0.01 per cent. Heath proposed to determine the amount of occluded gases by preliminary ignition for 20 min. in pure carbon dioxide—and to correct the error caused by absorbed hydrogen by subsequent ignition and cooling in carbon dioxide, finally replacing this gas with air.

Jan 1, 1926

By C. Baldwin Sawyer

During the last half century, much time has been devoted to investigations of the effect of nitrogen on the physical properties of steel, but in all discussions of results there is considerable doubt as to the accuracy and interpretation of analyses. No conclusions concerning the effects of nitrogen on the physical properties of steel can be more reliable than the methods used for determining the quantities of nitrogen present. The work described in this paper endeavors to establish some additional conditions required by the customary distillation method for reliable and nccurate determinations. Results by a combustion method of analysis for total nitrogen content are presented; these indicate that all of the nitrogen in steel, exclusive of that contained in blowholes, may be determined by the distillation method. Based on these more sound and more reliable analyses, results havc been obtained that bear on the following divisions of the general subject, nitrogen in steel: Nitrification of steel by melting in nitrogen, nitrification of steel by heating in ammonia, decomposition of nitrified steel by heating, and thermal analysis of nitrified steel. Consideration of Two Methods of Analysis and Some Results The details of the distillation and combustion methods are chemical in character and of little interest to most readers. They are therefore described in an appendix. The distillation method is essentially that described by Hurum and Fay1 and was generally used throughout this work. It is capable of the greatest accuracy and all results given are significant to the last, figure. Where analyses do not check, the samples

Jan 1, 1923