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By M. J. Ferrante

High-temperature enthalpy and X-ray powder diffraction studies were con-ducted on aluminum sulfide (Al2S3) as part of the Bureau of Mines effort to provide new data for the advancement of mineral technology consistent with environmental preservation and energy conservation. Relative enthalpies were measured with a copper-block calorimeter from 298.15 to 879 K. Tabulated values are listed for heat capacity, entropy, Gibbs energy functions, and relative enthalpies between 298.15 and 900 K. Enthalpies were also given in the form of an equation and combined with published data to calculate standard enthalpies of formation and Gibbs energies of formation for reactions of crystalline aluminum with crystalline, liquid, and gaseous diatomic sulfur. The hexagonal, rhombohedral, and cubic phases of Al2S3 were identified by X-ray powder diffraction studies, and the indexed powder diffraction patterns of these phases are given. The hexagonal phase was stable to about 852 K and was partially converted to the rhombohedral form at 879 K.

Jan 1, 1981

By R. A. Jankowski, J. D. Potts

Four underground respirable dust surveys were conducted to determine factors affecting belt entry dust levels and how using belt air to ventilate work areas affected dust exposures. Belt entry dust levels on the surveyed longwall and continuous miner section averaged 0.59 and 0.26 mg/m3, respectively. The stageloader/crusher contributed an additional 0.5 to 0.9 mg/m3 of dust to belt air, while the feederbreaker contributed 0 to 0.2 mg/m3 of dust. A 1000 ft (305 m) increase in belt entry length or a 200 to 500 tons/shift (181,000 to 454,000 kg/shift) increase in production resulted in roughly a 0.1 mg/m3 increase in dust. Using the belt entry as an intake entry on the continuous miner section appeared to reduce dust levels by 0.1 to 0.3 mg/m3 during cutting. Belt air was not used to ventilate the face on the longwall section.

Jan 1, 1992

By K. Wood, L. Duval

"The paper discusses the approach used to add a new, separate 5000 t/d copper-zinc treatment circuit to an existing, 1650 t/d copper circuit, essentially within the existing mill building. Temporary installation of new equipment allowed renovation and expansion within existing operating areas. Production in the original circuit was maintained at rated capacity throuqh0ut the construction period through close co-ordination between operating and construction groups. Downtime for circuit and service tie-ins was minimal. Both circuits are described briefly.For presentation at Canadian Mineral Processors Conference Ottawa, January, 1987.INTRODUCTIONLes Mines Selbaie is located in the Abitibi region of northwestern Quebec, in what has recently become better known as the Casa-Berardi-Joutel area. Les Mines Selbaie is operated as a joint venture project managed by Selca Division of BP Canada Inc. and owned 55% by BP Canada, 35% by Esso Minerals Canada and 10% by Trans Canada Pipelines."

Jan 1, 1987

The National Institute for Occupational Safety and Health (NIOSH) recommends that occupational exposures to respirable coal mine dust and respirable crystalline silica* be controlled by complying with the provisions presented in this document. These recommendations are designed to protect the health and provide for the safety of workers exposed to respirable coal mine dust and respirable crystalline silica for up to 10 hr/day during a 40-hr workweek over a working lifetime. The information presented in this document demonstrates that underground and surface coal miners are at risk of developing simple coal workers' pneumoconiosis (CWP), progressive massive fibrosis (PMF), silicosis, and chronic obstructive pulmonary disease (COPD). Adherence to the recommendations in this document should prevent or greatly reduce the risk of adverse health effects in workers exposed to respirable coal mine dust and respirable crystalline silica. NIOSH recommends that preventive efforts be focused primarily on reducing worker exposures. Effective health and hazard surveillance and medical screening are also useful components of a comprehensive prevention effort.

Jan 1, 1997

By Rob McIvor, Joe Keating, Gary Simmons

As more complex ores are processed, finer grinding becomes more necessary. A cross section of several industries will be presented with discussions not only of find grinding issues but also the classification of fine particles. JOHN MANSANTI: Our next topic will be fine grinding. Again, the intent is to present a topic that is generic enough to apply to multiple industries. Our first speaker is Gary Simmons. Gary is filling in for Phil Walker from Twin Creeks. Phil was not able to join us this week, because of some issues they're having with the autoclave. Gary, being involved in the development phase, is very familiar with the topic. Gary spent about three years with American Cyanamid and another four years with Noranda. He also spent some time with Meridian Gold, then became the director of metallurgy with Santa Fe Pacific Gold. He spent seven years there and is presently the director of process technology with Newmont Gold.

Jan 1, 1998

By R. E. Ford, P. Tarassoff, P. H. Jennings

Copper oxide ore may be leached at all sizes from run-of-mine down to pulp, and consideration must be given to all available methods in determining the most economical one. Heap leaching was evaluated in a pilot plant at Gaspe Copper Mines, Ltd. which was designed to simultaneously leach two 1200-ton dumps of ore. The plant was operated for two years, in part under severe winter conditions. Two modes of leaching were investigated: acid leaching in which sulfuric acid was added externally to the leach solution, and pyritic leaching in which pyrite concentrate was added to the dump and acid was generated in situ by bacterial action. The pilot plant operation is described, and the results are compared with laboratory data obtained in 6-in.-diam columns. It is concluded that pyritic leaching offers certain operating advantages over acid leaching when copper is recovered by cementation in that iron buildup in the solution is prevented.

Jan 1, 1974

By N. Solak

CrN, TiN and Ti-B-N coatings were deposited onto H13 hot-working tool steel and alumina substrates by arc-PVD. The coatings were characterized with respect to their mechanical and structural properties. Oxidation behavior of the coatings on alumina substrates was investigated by TG/DTA. Samples coated on H13 substrates were oxidized in a tube furnace under atmospheric conditions at specific temperatures determined from TG/DTA tests of the same coatings deposited on alumina substrates. The oxide scale morphology was characterized by scanning electron microscopy and X-ray diffraction. Oxide scale thickness change and TG data were used to calculate oxidation reaction activation energies. It was determined that boron addition into TiN coating improves not only mechanical properties but also oxidation resistance. Depending on the substrate material different oxidation activation energy values for the TiN and Ti-B-N coatings were determined revealing the importance of film morphology on oxidation resistance.

Jan 1, 2006

By Michael Louis, Charles Dowding

Concern over construction vibration-induced cracking has led to development of a new approach to vibration monitoring called autonomous crack measurement (ACM) and illustrated in Figure 1. This paper describes the concept as well as sensor performance in the first test house fitted an ACM system. Response of three cracks in this concrete masonry unit (CMU) house was measured as part of the system verification. ACM employs a single sensor that measures both weather-induced micrometer changes in crack width and those produced by habitation and ground motioninduced vibration. This comparison is displayed in real time via the Internet without human interaction. Graphic display through the Internet provides a new pathway for communication with the public. Such visual comparison of changes in crack width provides a simple alternative to the present system of comparison of measured and allowable vibration time histories. Measurements reported herein show that weatherinduced response of cracks is greater than that caused by presently allowable construction-induced vibration.

Jan 1, 2003

By G. B. Gibbs

Various semiempirical equations which relate defect-formation energies and entropies with elastic and thermal properties of a metal crystal are shown to be related by a simple model for lattice energy. An illustrative comparison of theory with experiment is made using self-diffilsion data for fee metals. SEVERAL workers have related the free energy of defect formation with elastic and thermal properties of a crystal lattice, particularly elastic bulk modulus and Debye temperature. The present note shows how the various approaches are related by a simple model for lattice energy. A comparison of theory with experiment is given using the self-diffusion parameters of fee metals. 1) A MODEL OF THE CRYSTAL LATTICE The internal energy per atom in a metallic lattice may be written U=Ui-Ue [1] where Ui and Ue refer to ion-ion interaction and valence electron energies, respectively. The volume per atom V has an equilibrium value 52 for which

Jan 1, 1968

Develop technology for preparing thick corrosion-resistant coatings and electroforms of iron-chromium-nickel alloys. Approach To reduce the United States' dependence upon foreign sources for supplies of strategic and critical metals such as chromium, cobalt, and nickel, new technology must be devised to conserve these valuable commodities. One approach being investigated by the Bureau of Mines is the use of a modified-aqueous-electrodeposition method to prepare thick (-25 µm), complex alloy coatings (e.g., stainless steel composition) with properties similar to the commercial alloys. An alloy coating on a low-alloy steel or carbon steel substrate would require significantly less strategic and critical metals than those contained in an equivalent mass of the commercial alloy. Coatings applied to appropriate mandrel materials make possible the preparation of intricately-shaped alloy electroforms (near-net-shape parts). As a result, the loss of valuable metals associated with machining finished products would be minimized.

Jan 1, 1986

By Charles E. Glass

As partial implementation of the Surface Mining Control and Reclamation Act of 1977, the Office of Surface Mining (OSM), Department of Interior, has requested each state to inventory hazardous abandoned mining areas within their boundaries. Primary interest is in such areas .as unstable waste-banks, subsidence and slumping, contamination of water supplies, and preservation of overall aesthetic qualities through reclamation. In addition to the concern expressed for abandoned mining areas, the legislation requires a complete inspection of operating mines quarterly and a partial inspection monthly. In Arizona copper has been mined for over 100 years and coal and uranium mining promises to expand in future years. The OSM requirement for a waste inventory and frequent monitoring of Arizona's large, widely spaced mines places a severe demand on limited personnel and operating budgets. Remote sensing by satellite provides an attractive and effective approach to aid the inventory and monitoring requirements of the OSM legislation.

Jan 1, 1979

By Thomas R. J

Following asmallnumberofpollutionincidents involving the death of cattle from ingestion of cyanide that had escaped from gold processing plants, the Queensland Government undertook to develop competent guidelines addressing this problem. These guidelines, "Queensland Government Guidelines on Prevention of Water Pollution from Cyanide Use in Gold Ore Processing", issued by the Department of Environment and Heritage, Department of Resource Industries and Water Resources Commission, cover hydrology and general house-keeping intended to reduce the likelihood of significant impact from a spill or unintentional dis- charge of contaminated material. There are three major advances for Queensland embodied in this Guideline: ò the use of a design approach that gives site specific standards rather than trying to give a multitude of standards broad enough to cover all situations, ò the use of hazard assessment and a "critical period" hydrologi- cal design technique, and ò new monitoring and reporting requirements. The guideline is presented here in a summary form:

Jan 1, 1991

Any project carries a number of challenges and risks. Inappropriate design, poor project management, time, industrial disputation and capital over runs are all areas which can impact on a project cash flows and return on investment. In the resource Industry you have the added complexity and risk of geology which is difficult to predict and sometimes unforgiving. The Dartbrook Mine was designed and constructed as a high output longwall mine and has overcome a number of hurdles to produce over 2.3 million tonnes for the first year of operation. A number of problems were encountered during construction which resulted in the inseam development being delayed for six months. Dartbrook people have demonstrated they can manage adversity and produce world class results. The mine has been through a very steep learning curve during 1997 and with this experience behind the mine is now producing at an annualised rate of 3.4 MTPA.

Jan 1, 1998

By Kot F. v. Unrug

In spite of extensive research and accumulated experience from mining operations, appropriate coal strength values for pillar design remain debatable. Coal strengths determined in the laboratory on standardized samples vary widely among various coal seams with poor repeatability. Penetrometric in situ strength testing obtains multiple measurements at multiple horizons within the coal seam to provide a strength profile. Alliance Coal has used that method in many of its mines for pillar design. Pillars in these mines perform well. This paper presents a series of case studies and discussion of issues related to coal pillar design. The analysis demonstrates that the proposed default in situ strength of 900 psi is appropriate when no other data exist. However, in the case of appropriate strength measurements combined with analysis of pillar structural composition, differing values can be used successfully. In areas where the penetrometric derived in situ strength is greater than the standard 900 psi in situ strength, reserve recovery has been optimized as required by law without compromising safety.

Jan 1, 2009

By L. Béjar-Gómez

The aim of this research work is to study and characterize precipitates in structural microalloyed steel by transmission electron microscopy and analysis by high resolution (HRTEM). Microalloyed steel with titanium was produced by casting in an electrical induction oven of 25 Kg. capacity. Carbon content in steel was less than 0.1 % and titanium content of 0.04%. Steel was processed thermomechanically; reheated to 1250ºC and hot rolled on a laboratory mill to a 13.0 mm thick plate with a finish rolling temperature of 900ºC and thickness reduction of 80%. Analysis by High Resolution Transmission Electron Microscopy (HRTEM) identified precipitates in the steel; type and morphology. Energy Dispersive Spectroscopy (EDS) analysis was applied to obtain the chemical composition of precipitates and the matrix. STEM-EDS analysis was also applied to obtain the element profile of precipitates. The results showed the presence of carbonitride precipitates of titanium, Ti (CN), with a circular morphology and size of 10 nm and less.

Jan 1, 2006

By Mahesh C. Jha

Molybdenum, a major refractory metal, is widely used as an alloying element in steels and superalloys to improve their corrosion resistance, physical properties and mechanical strength, particularly at elevated temperatures. The current worldwide production and consumption is estimated at about 130,000 tons contained molybdenum per year. Molybdenum occurs in nature as molybdenite mineral and is recovered by a flotation process as a primary concentrate at molybdenum mines and as a byproduct concentrate at copper mines. The concentrate is roasted to a technical-grade molybdic oxide (tech oxide) in multiple-hearth roasters. About 80 percent of the tech oxide is sold, as such or after conversion to ferromolybdenum, for addition to iron and steel. The remainder is further refined to pure oxide and molybdate chemicals that are used in the manufacture of catalysts, specialty chemicals, molybdenum metal and superalloys. This paper discusses the various steps in the extractive metallurgy of molybdenum, from flotation of sulfide concentrate to reduction of pure oxide to molybdenum metal.

Nov 26, 1999

By Nikhil Dhawan, Veeranjaneyulu Rayapudi, Singh Rahulkumar Sunil

The ever-increasing demand for steel and the subsequent depletion of high-grade ores requires the massive utilization of low-grade iron ores. In the present study, an iron ore slime sample containing 56.1% Fe was investigated using physical beneficiation, carbothermal reduction, and a microwave-assisted process; however, physical beneficiation and microwave exposure were found to be inefficient as they yielded lower iron recovery. Using coconut shell as an alternative reductant was found to be promising and does not lead to the formation of higher iron oxides, such as fayalite and wustite phases. The microwave-assisted carbothermal reduction was found at par with conventional reduction, saving time and heating. The optimum magnetic concentrate obtained in both carbothermal reduction routes (microwave and muffle furnace: Fe grade, Fe recovery, and yield of 64.3, 97, and 84%, and 67, 99, and 83%, respectively) are suitable for alternative iron-making or blast furnace units.

By De Broglio R

The Mae Moh coal deposit was discovered some 60 years ago by villagers who noticed spontaneous combustion of coal outcrops. The first production began in the 1950's to fuel a fertilizer plant and a 12.5MW power station. During the period 1976 to 1979, three 75MW power station units were constructed on site. These have a total daily coal consumption of some 5000 tonnes and are served by a stockyard of approximately 60 000 tonnes total capacity. Stacked coal is reclaimed by means of a front end loader onto reclaim conveyors. During the years 1983 to 1986 four 150MW power station units were constructed east of the eastern seam subcrop, sons 2 km from the original power station complex. These have a daily coal consumption of nearly 12000 tonnes and are served by a stockyard of total capacity 270000 tonnes, equipped with two stackers and two bucket-wheel reclaimers for a totally mechanised system.

Jan 1, 1986

By Torckler L, Brathwaite R. L

At Neavesville gold-silver (electrum) mineralization occurs in steeply-dipping zones of intense fracturing, brecciation and quartz veining within rhyolitic pyroclastics, carbohaceous shales and andesites. Hydro- thermal alteration extends over an area of greater than 3 by 1.5 km. In rhyolitic tuffs, highly silicified zones containing quartz- adularia-illite assemblages are flanked by less silicified assemblages composed of albite, illite-montmorillonite and chlorite. The mineralogy ana sequence of alteration are comparable with the alteration zones which envelop the steam-producing fissures of the active Wairakei and Broadlands geothermal fields. Primary fluid inclusions in quartz from five fissure veins in the Neavesville field show maximum homogenisation temperatures ranging from 220 - 260¦C and salinities of 0.0 - 1.1 wt. % NaCl equivalent, which cover a similar range to actual measured temperatures and salinities in geothermal fluids at Wairakei aria riroaolan¦s. The age of the rhyolitic pyroclastics and related alteration and mineralization is probably Pliocene and Neavesville therefore represents a fossil geothermal system.

Jan 1, 1980

By J. T. Sims, C. E. Karayannopoulos

Today's rare earth industry is undergoing significant and rapid evolutionary change toward greater reliability and diversity of supply, increased security of supply chains, and better price forecasting. Technology innovation is reducing rare earth production costs while decreasing the impact of producers on the environment. Advances in rare earth material science are reducing the need for relatively scarce heavy rare earths (HREEs) in high-performance neodymium-iron-boron (NdFeB) permanent rare earth magnets and opening the NdFeB magnetic market space for a broader range of downstream applications. Rare earth producers such as Molycorp are increasingly able to offer long-term supply agreements with forward price predictability, something that has not been the case for many years. All of these trends are helping to restore the confidence of customers and other stakeholders in the rare earth space. That increased confidence is likely to bolster global demand for rare earth materials and expand innovative utilization of these remarkable materials.

Jan 1, 2014