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By Xianjun Lu

This paper presents gold occurrence investigations on the altered rock gold deposit from Jiaodong area of China, and comparisons of gold occurrence in the ore samples from different mining levels. According to the results, the chemical and mineral compositions of raw materials from different mining levels are quite similar. However, the relative content and grain size of gold minerals are quite different between the two mining levels of -130m~-340m and -550m~-650m. In the ore of upper mining levels of -130m~-340m, electrum is the dominant gold mineral and accounts for about 80% of the total gold minerals, while native gold is minor and accounts for about 20%. As for the ore of deep mining levels of -550m~-650m, the major gold mineral shifts to native gold which accounts for 67%, while the ratio of electrum drops to about 33%. Coarser gold grain size was observed in the upper mining level ore with a mean size of 33.05µm while the gold grain size was much finer in the ore of deep mining levels with a mean size of 22.85µm. Furthermore, the gold mineral associations also show different patterns between the upper mining level samples and the deep mining level samples. Of the three observed gold association types such as inclusion gold, fissure gold and interparticle gold, more inclusion gold was found in the ore of deep mining levels. The inclusion gold accounts for 62% in the ore of deep mining levels, while that in the ore of upper mining levels accounts for about 56%. Further study revealed that the dominant gold associated minerals are pyrite and sulphides and only a small amount of gold is associated with quartz and silicates. It was shown that the altered rock gold ore from Jiaodong area can be regarded as a free milling gold ore, but the processing parameters should be optimized for the ores in different mining levels according to the different gold occurrence. In addition, it was predicted that enhanced gold liberation is necessary for the ore in deep mining levels.

Sep 1, 2012

By H. Pearce, A. E. Lewis, A. Ochieng

Hydrodynamics and mixing are fundamental to the operation of mineral process systems such as flotation cells and metal precipitation reactors. The computational fluid dynamics (CFD) technique has been employed in the present work to study the hydrodynamics in a mixing vessel stirred with either a Rushton turbine or a pitched blade impeller. The multiple frame of reference (MFR) approach has been used to model both impellers. A draft tube was used only in the Rushton turbine stirred vessel. The flow profiles for the pitched blade impeller have been studied in three regions; below the impeller tip, at the middle of the tank, and near the liquid surface. The simulation results were compared with literature data obtained using a laser Doppler velocimetry in the three regions of the vessel, and it was found that the model predictions were better in the impeller region. There was a poor prediction of the experimental results in the region closer to the liquid surface; however, this was improved when the turbulence parameter (C2) in the k-e model was set to a higher value. The value of the impeller clearance at which the Rushton turbine generates an axial impeller type flow has been determined and it has been shown that, at this clearance, a draft tube can be used to enhance axial flow in a Rushton turbine stirred reactor.

Jan 1, 2003

By R H. Knight

Uncertainty in prediction and modelling of geological (physical) ore continuity in geometrically complex ore deposits is a key risk factor in mining. Reducing geometric uncertainty of hard-boundary ore/waste contacts and related geological features improves the efficiency of local mineral resource estimation and reserve calculation, mine/stope planning, ore control and in-mine exploration. Detailed underground mapping of serial-level drives provides a continuous record of the characteristics and contact configuration of ore, as well as crucial ore-related geological features that are required to resolve geometrical variability when closely spaced drilling proves inadequate or is cost-prohibitive. The mapping-based approach described in this paper re-establishes the focus on the geology of the orebody by incorporating high-value, detailed geologic mine mapping information. Mapped ore-related configurations and relationships, recorded on a succession of faces or on a series of levels, provide the basis for 3D interpolation and extrapolation of the local geologic continuity of an orebody. Correlative points representing locations of key ore-related geologic features on each face or level are linked by 3D polylines or trajectories forming a coherent geometrical framework. The coherent progression of geometric changes mapped by these trajectories reveals the overall ‘dynamic’ of the geometrical framework, as well as the spatial tendencies of its geological constituents. Distinct sets of ore control trajectories are selected from within the framework and are used in the construction of alternative geological ore continuity models. As mining proceeds, alternative models are evaluated, and are then either refined or rejected. The geometrical framework is used to evaluate theoretical models and practical heuristics, focus exploration targeting and inform and guide all aspects of mine geology in active mines. This approach also lends itself to analysis of global ore continuity in the re-evaluation of mature or abandoned mines. Its use is particularly effective in geometrically complex orebodies such as the West Branch orebody and the orebodies of No 2 mine of the Balmat-Edwards-Pierrepont zinc district, which are used to illustrate the method. CITATION:Knight, R H, 2014. A mapping-based approach to geological continuity prediction using examples from the Balmat-Edwards-Pierrepont Zinc District, St Lawrence County, New York, USA, in Proceedings Ninth International Mining Geology Conference 2014 , pp 65–76 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 18, 2014

By K Gottliebsen

Many hydrometallurgical and chemical processes produce large amounts of acid waste. This is illustrated by the copper S/X-E/W process used at the Mount Gordon mine in North Queensland, which produces a tank house bleed in the form of a concentrated sulphuric acid stream. The bleed stream is necessary to remove impurities such as iron that decrease the efficiency of the electrowinning process. However, this bleed stream comes at a high financial cost due to large quantities of make up sulphuric acid required as well as the need to neutralise the bleed stream prior to disposal. The present work describes the approach taken to develop a solvent extraction process for the selective recovery of sulphuric acid from copper tank house bleed liquor. The proposed extraction system was investigated using a branched long chain aliphatic tertiary amine tris(2-ethylhexyl)amine (TEHA) as the extractant, Shellsol 2046 as the diluent and octanol as a modifier. Computer simulations were used to determine the optimum operating conditions for the recovery process. It was found that the process was able to selectively recover up to 90 per cent of the sulphuric acid from the copper electrolyte. This is recovered as a pure aqueous acid stream at a concentration of up to 130 g/L that can be recycled back into the tank house circuit or other areas of the process. The raffinate acid concentration was reduced from 180 g/L to as low as 18 g/L, significantly reducing waste disposal and the environmental impact of the copper process. The equilibrium data and simulation results were also compared with an alternative extractant, CYANEXR 923. Finally the efficiency of the TEHA extraction system was investigated on a pilot-scale in a pulsed perforated plate column. This information was used in order to scale the process for an industrial application. The same methodology applied in this case study could be used to provide innovative and cost-effective solutions to waste streams encountered in other hydrometallurgical or chemical processes.

Jan 1, 2000

By D. W. Frommer, M. M. Fine

Early in 1957 St. Joseph Lead Co. announced discovery of three new centers of iron ore deposition in east central Missouri.1 The discovery resulted from exploratory drilling in the vicinity of a magnetic anomaly or high. A deep hole, drilled into the Pre-Cambrian porphyry to determine the cause of anomaly, penetrated a magnetite-rich deposit.2 The magnetic surveys that revealed the anomalies were begun by the Missouri Geological Survey in 1929 and were continued into the 1930's 3. At that time an area in Crawford County known as the Bourbon magnetic high was located. A second anomaly, similar in size and intensity, was discovered about six miles to the northeast in Franklin County in the vicinity of Sullivan. This area was not studied in detail until the early 1940's.

Jan 3, 1959

By G J. Lyman, S A. Tittlemier

International regulations exist to manage the concentrations of mycotoxins such as Ochratoxin A (OTA) and deoxynivalenol (DON) in grains and prevent health risks from excessive exposure to OTA and DON. Since the permitted levels of these mycotoxins are very low (existing maximum levels are in the range of 5 ppb for OTA and 1–2 ppm for DON), sampling for these mycotoxins is potentially challenging. Given that the distribution of infected kernels in a consignment of wheat can be highly heterogeneous, detection by current sampling methods is subject to a high variance. Furthermore, the concentrations of mycotoxins in individual kernels vary over orders of magnitude, intensifying the heterogeneity of the bulk grain.In these circumstances, there is much interest in developing sampling plans that inform regulatory agencies, and mitigate the risk of misclassifying grain shipments as compliant or non-compliant within the global grain trade, when correctly implemented.Experimental data from laboratory and field studies describing individual wheat kernel concentrations of OTA and DON were combined with experimental data describing the variance due to the analytical methods used for OTA and DON to calculate the sampling distribution for wheat having various levels of contamination. This work has focused on quantifying the heterogeneity of samples at the point of submission for analysis and within subsequent sample preparation to arrive at total sampling distributions that include uncertainties due to the intrinsic heterogeneity and the analytical uncertainties. The sampling uncertainty that relates to the difference between the primary sample analysis and the true lot analysis is not included as it has been dealt with elsewhere.CITATION:Lyman, G J and Tittlemier, S A, 2017. The sampling characteristics of grains contaminated by mycotoxins, in Proceedings Eighth World Conference on Sampling and Blending , pp 281–294 (The Australasian Institute of Mining and Metallurgy: Melbourne).

May 9, 2017

By Daniel Johansson, Markus Danielsson, Håkan Schunnesson

In sublevel caving, blasted material flows gravitationally into the drawpoint from above in a periodical manner. This type of flow behavior entails muck pile conditions that are variable along the course of extraction. The effect of this variability on the LHD (Load-Haul-Dump) operation in terms of loading efficiency and ability to undermine the blasted ring is not fully understood as of today. This paper presents results from a field test in LKABs Malmberget mine in Sweden, where the influence of fragmentation on the loading operation has been studied in detail. Drawpoint filming was conducted for extraction of two rings equivalent of roughly 10000 metric tons (~9842 long tons) of material each. The analysis includes fragmentation measurements, muck pile classification, and general estimations in terms of loadability. Further, an evaluation of LHD machines from two different manufacturers was conducted to identify and highlight differences. The results show that fragmentation, muck pile compactness, and flow characteristics are all interdependent. Flow disturbances and the subsequent loading of compacted fine material in the back of the ring have been identified as the main reason for occurring problems and prolonged digging times. However, the ability to sufficiently undermine the blasted ring has been identified to primarily depend on digging depth which is only observed to be high during flow disturbances. An absence of flow disturbances seem to promote high loading efficiency but simultaneously limit the maximum digging depth. A mid-range particle size distribution with a low amount of fines has proven beneficial for overall loading efficiency. The various LHDs employed showed significant variations in terms of ability to handle difficult loading situations (e.g. compactness, boulders, etc.).

Jan 1, 2018

By Daniel R. Shawe

Ore deposits of the western U.S. are divisible broadly into two genetic groups, a smaller one that fits the plate tectonic model of subduction and a larger one that appears unrelated to subduction. Some of the middle Paleozoic and lower-middle Mesozoic ore deposits in the western U.S. are associated with eugeosynclinal rocks and lie a few hundred kilometers west of reconstructed continent margins. These deposits probably formed as a result of subduction beneath oceanic or thin continental crust that was analogous to subduction predicated for the Kuroko massive sulfide deposits of Japan. Some middle Mesozoic porphyry copper deposits may have formed east of the continental margin when subduction-generated magmas were emplaced high in continental crust in a manner analogous to subduction-generated magmas that formed the Andean porphyry copper deposits. Most Cretaceous-Cenozoic ore deposits lie in a broad region extending many hundreds of kilometers east of the continent margin and characterized by conjugate tectonic zones, high terrestial heat flow, and low seismic velocity in the upper mantle. The deposits likely were formed in relation to magmas generated along the conjugate tectonic zones during differential northwestward drift and internal wrenching of the continental plate.

Jan 1, 1978

The 107th Annual General Meeting of The South African Institute of Mining and Metallurgy was held at The Country Club, Johannesburg, Napier Road, Auckland Park on Wednesday, 11 August, 2004. Welcome The President extended a special welcome to the guests and representatives of our sister institutes and other associations, also to recipients of awards, senior members of industry, Honorary Life Fellows, past-presidents, our members and other guests, among them the following: Ralph Bagirathi, Executive Member, African Mining Association Rudi Rudolph, President, Association of Mine Managers of South Africa Andrew Whibley, President, Association of Mine Resident Engineers of South Africa Dr Con Fauconnier, President, Chamber of Mines of South Africa Nxolisi Diliza, Chief Executive Officer, Chamber of Mines of South Africa

Jan 1, 2004

By Jens Kristen Laursen

In 1999, Molymex S.A. de C.V. (Molymex), Mexico. (a company wholly owned by Molibdenos y Metales S.A. (Molymet), Chile) decided to install the Haldor Topsrae Wet gas Sulphuric Aicd (WSA) process for cleaning of the 4-5% SO2 off-gas from their molybdenum sulphide master in Cumpas, Mexico to produce sulphuric acid. The decision to install a WSA plant was based on the successful operation of a WSA plant at Molymet's molybdenum sulphide roaster in Santiago, Chile since 1993. This paper describes the process layout of the Cumpas plant, the operating experience of the Santiago plant, and the, differences in. process design between the two plants. It will furthermore summarise the applications of the WSA process for other roasting plants and smelters within the non-ferrous. metals industry producing metals such as copper, lead, and molybdenum.

Jan 1, 2002

By Lewis IE

Copper-lead dross is a by-product of the refining of lead bullion produced by the Imper- ial Smelting Process. This dross contains some 27 percent copper, 50 percent lead, four percent zinc and one percent sulphur. An ammonium carb- onate leach at atmospheric temperature and pressure removed the copper from the dross while the lead zinc and precious metals remained in the leach residue for return to the smelter. The leach solution containing the copper was then purified by liquid-liquid ion exchange using LIX64N in a kerosene diluent. ("LIX" is the registered trade mark of a range of hydroxy oximes marketed by General Mills Inc.) The pilot plant had a capacity of 0.7 kg/h of CuSO4,5H20 and was operated for some fifty days on a two shift basis. Copper sulphate of excellent purity was produced, and the results obtained indicated that a copper recovery of ninety percent from the dross could be expected from a commercial installation.

Jan 1, 1975

By W. B. Boggs

This is a rather comprehensive subject and cannot be thoroughly covered in the short rime allowed for its presentation. This article will touch only upon a few of the chief points of the difficulties encountered in recovering copper from brass shell cases in a primary smelter which was not designed to treat scrap metals. Owing to the fact that the plant is at present (Dec., 1946) closed, and our tests were not completed, full details of the results are not available. As is well known, most primary smelters are situated near the mines in the interior of various countries and are not close to seaports or large industrial and railway centres. Consequently, iris unusual for a primary smelter to be asked to treat scrap metal of any kind. When so required, iris obvious that the primary smelter is at a great disadvantage, for the simple reason that it probably has to pay the freight on the scrap from the seaport or industrial centre to the smelter and then also pay the freight on the recoverable metal from the smelter to the refinery, or seaport or industrial centre. Another disadvantage is that a primary smelter is not equipped to sample and unload the scrap nor bas it usually the equipment adaptable for treating the scrap efficiently, as the plant bas been designed to handle large tonnages of ores and concentrates. This short paper will describe some of our difficulties> and how they were corrected. However, it might be advisable to state briefly some of the methods used in treating brass shell cases in other plants. In the first place, a brass plant producing new brass- especially those producing brass billets for extrusion to make brass tubes or rods, or to be drawn into wire, or making brass cake to roll into brass sheets- generally insists upon using new electrolytic copper and zinc and is opposed to using any scrap or secondary brass . Consequently, such a plant usually will not treat brass shell cases. Therefore, the usual procedure is to ship brass shell cases to a secondary smelter, where it is generally sorted, melted, fire-refined, and returned to the market in the form of a high or low brass ingot which can be sold to brass foundries for making brass castings. This evidently is the cheapest and simplest method. Another method is to ship to a smelter which is a combination of a primary and secondary smelter attached to or near an electrolytic refinery. In plants of both these types, that is a primary smelter with Cottrell dust collectors or a combined primary and secondary smelter with Cottrells or a bag house, the zinc may be wasted. However, if a bag house is used, some of the zinc is recovered, but it is usually contaminated with other metals and further processing is required to recover it.

Jan 1, 1947

By Frank Clowes

This lamp has been devised to burn oil from a flat wick in the usual way for lighting-purposes ; and also to burn a hydrogen-flame of standard size instead of the oil-flame, when delicate and accurate gas-testing is to be carried out. The change from the oil-flame to the hydrogen-flame, and vice versa, can be made with great rapidity, and without opening the lamp or running any risk in the presence of gas. The oil-flame serves for illumination; and when the wick is drawn down by the " pricker," so as to abolish the light, the pale blue reduced oil-flame serves to detect fire-damp or "gas," in any propor

Jan 1, 1894

By D. Mraz

"In certain instances, rocks around underground excavations behave as a plastic mass. This paper offers several solutions to predicting the mode of plastic flow around cavities and designing mining pillars where plastic conditions exist.IntroductionWhen stresses around underground cavities exceed yield limits of the host rock, the material often behaves as a plastic mass. The best example of this phenomenon is the behaviour of salt rocks in deep salt and potash deposits (more than 500 m deep).However, many other soft rocks exhibit similar properties. For example, Jeremic(1) described certain types of coal yielding plastically under high pressure. Alder suggested that granulated rock behaves plastically.The object of this paper is to propose a de sign procedure for mining pillars exhibiting plastic flow due to the combination of rock properties and in-situ stresses.Prandtl(3) mathematically defined a concept of a generalized, perfectly plastic substance, not possessing the property of strain hardening (Fig. I). He had in mind, a solid with a quasi quasi-isotropic , polycrystalline structure having a well defined yield point, and he postulated that its material elements start and continue to deform plastically when the maximum shearing stress ""'MAX"" reaches a sharp limit, dependent on the mean value of the sum of the major and minor principal stresses:"

Jan 1, 1984

By R E. Langston, S M. Gazioglu

A preconstruction inventory program was conducted to determine the existing conditions of residential, non-residential and all other structures within 2,000 feet of the blasting limits for a highway excavation site in Asheville, North Carolina. Prior to major production blasting, eleven test blasts were detonated to establish site specific propagation parameters in order to develop contours of maximum allowable explosive charge weights per delay. The method of scaling distance by the square root of charge weight per delay was utilized in developing the contours of allowable charge weights. The charge weight contours were revised during blasting operations as additional vibration data became available. The effects of blast induced vibrations on a nearby water storage reservoir, a nearby vehicular tunnel and other adjacent residential and non-residential structures were observed and monitored over a period of two years of blasting operations.

Jan 1, 1980

By S. Shapiro, G. Krauss

RECENT investigations1 3 of the products of marten-sitic transformation in Fe-Ni and Fe-Ni-C alloys have made use of light microscopy to describe mar-tensitic fine structure. The application of conventional metallographic techniques to this problem was possible because of the similarity of distributions of parallel striations developed by etching polished surfaces to distributions of transformation twins which are positively identified in thin films by transmission electron microscopy. The surface striations frequently are not well-defined, and could also be due to, for example, rows of etch pits which are not resolved by the light microscope. This note describes the etching effects revealed by examination of surface replicas of mar-tensite in the electron microscope. The application of a replica technique both extends the observations of fine structure made with the light microscope and allows the results of conventional metallography to be used with more confidence. Samples of an Fe-33 wt pct Ni alloy were used for this study because of the detailed knowledge of the fine structure of martensite which has been developed'-4 for alloys of about this composition. Samples transformed to martensite at -120°C, and transformed samples heated to 340°C to effect a small amount of reversal of martensite to austenite, were examined. Surfaces were first prepared for replication by elec-tropolishing in a chromium oxide-acetic acid electrolyte at a current density of 0.1 amp per sq cm and a temperature of 15°C or a perchloric acid-acetic acid electrolyte at a current density of approximately 2 amps per sq cm and a temperature of 15°C. The polished surfaces were then etched for 4 to 7 sec by immersion in a solution of equal parts HC1, HNO,, and H20. Application of the etchant for this period of time produced discrete attack of certain features without loss of resolution due to overlapping of areas most susceptible to etching. The etched surfaces were replicated by 1) preshadowing with Pt-Pd alloy at an angle of 20 to 30 deg, 2) depositing a thin carbon film, and 3) stripping the film and shadowing material by immersion in a 5 pct nital solution. Two types of etching effects were observed by examination of the surface replicas in the electron microscope: l) continuous striations centered at the bottom of long grooves or the tops of pyramidal elevations on the sample surface, and 2) high densities of fine etch pits. Examples of both types of features are shown in Figs. 1 to 4. The striations are in each case continuous and have the same characteristic configurations as do transformation twins in martensite. Fig. 1 shows that the density of grooves decreases toward the edge of a martensite plate and Fig. 2 shows a region where the striations are of varying length. Similar examples of transformation twin arrangements determined by transmission electron microscopy of thinned foils of martensite have been shown in the literature,'~ and, based on these similarities, the striations and their associated grooves or mounds are considered to be evidence for the presence of transformation twins. The transf~rmation twins in martensite are on the order of l00 A thick, much too fine for resolution by the light microscope. It appears that orientation-dependent etching of the matrix martensite about the twins results in grooves or surface elevations which

Jan 1, 1967

By T. J. Yeomans

"The Kidd Creek metallurgical site is situated twenty-six kilometres east of Timmins, Ontario. The site consists of a 4.5 niillion tonne per year concentrator, a 127,000 tonne per year electrolytic zinc plant and a 79,000 tonne per year copper smelter/refinery complex.The concentrator commenced operations in 1966 and was expanded to its present capacity in 1978. The zinc plant commenced operations in 1972, and the copper smelter/refinery in 1983.The concentrator tailings, and both liquid and solid waste products from the other plants are disposed of within a 1215 hectare tailings disposal area. Here, a method known as centraljzecl thickened discharge is used to form a stable cone-shaped hill. A low permanent perimeter dyke structure encloses the cone and directs cone run-off and thickener overflow to a treatment pond. After treatment with lime slurry, this neutralized effluent is recycled to the metsite and also discharged into the Porcupine River system.The tailings system has been in operation in its present form since 1972, upon completion of dykes and a 110 metre thickener unit. Underflow densities were continuously increased until thickener overloading became a serious problem. This necessitated the construction of a second 110 metre thickener, which was completed in 1983. Target densities have been achieved without difficulty since then.This paper discusses the operation of the tailings system, reviews past performance, and outlines future operations."

Jan 1, 1986

By Bob de Raadt

For a long time industrial underwater blasting has stood in need of a calculation method, for the determination of shockwave-proof as well as shockwave-effective charge distances to objects in water. After a brief discussion of the physical background of the shockwave mechanism in water, the author discusses an empirical theoretical computing method based on the "Bubble boundary" concept. The practical application of this model is finally shown in an account of a few underwater blasting operations in which charge weights of c.1-1000 kg were involved.

Jan 1, 1980

By Guiming Yang, Xiaoxian Huang, Zhiyun Ji, Min Gan, Lishun Yuan, Xiaohui Fan, Zhiyuan Yu

"The roasting characteristics of hematite pellets containing MgO were studied where magnesia powder, serpentine and magnesite were used as magnesium-additives respectively. The mechanical strength of both preheated and roasted pellets decreased when MgO content increased, which implied the addition of MgO had an adverse effect on pellet consolidation. By adding flux containing CaO, the mechanical strength of both preheated and roasted pellets were improved. The addition of calcium flux facilitated the formation of calcium ferrite and provided a certain amount of liquid phase, resulting in faster diffusion ofMg2+ and Fe3+. The result showed that diffusing speed of Mg2+ was enhanced by 1.48 times, and rate constant of Fe203 crystalline growth was enhanced by 62% when basicity was around 0.4. Improvement of mineralization degree and recrystallization of Fe203 assisted in consolidation of hematite pellets containing MgO.IntroductionOxidized pellets are ideal iron-bearing burdens in blast furnace. At present, magnetite is the main raw material for oxidized pellet production in China. However, as the rapid development of iron and steel industry, resources of magnetite have been depleted and cannot satisfy the requirement of pellet production. Using hematite concentrates to produce oxidized pellets has become a trend [1, 2]. Many pellet enterprises abroad nowadays have adopted high proportions of hematite concentrates when producing oxidized pellets, e.g. the percentage is 100% in a lot of Brazilian factories [3, 4]. But high proportion of hematite concentrates will lead to low mechanical strength and high reduction swelling index of pellets. Some studies show that Mg-bearing pellets have excellent metallurgical properties, and the reduction swelling phenomenon can be solved by adding fluxes containing MgO [5, 7]. However, there are problems such as low pellet strength and bad roasting characteristics for MgO-bearing pellets, which remains an obstacle in pellet industry. Hence, it's vital to undertake the study on strengthening measures for indurations of Mg-bearing hematite pellets."

Jan 1, 2013

By R. E. Maringer, A. Schwope

IT has been recognized that oxygen in minute quantities is extremely detrimental to the room-temperature ductility of molybdenum. Early fracto-graphic studies' of the cast metal indicated that oxides are formed preferentially at the grain boundaries. Additional verification of this preferential segregation has been obtained from internal friction studies on poly crystalline molybdenum (average grain diameter varied from 0.039 to 0.065 mm) and from observations of the effect of oxygen on specimens of extremely large grain size. Specimens A, B, and C, of 0.040 in. diameter commercial molybdenum wire (Lot FW 13-40) were heat treated in the vacuum furnace described by Few and Manning according to the specifications given in Table I. Internal friction studies of these specimens were carried out using a low frequency (approximately 1 cycle per second) torsional pendulum completely enclosed in a vacuum tank. As the pressure of oxygen in the heat treating atmosphere changed, the portion of the internal friction vs temperature curves ascribed to grain boundary relaxation changed correspondingly, Fig. 1. The decrease in the damping capacity at high temperatures as the pressure of oxygen in the heat treating atmos-

Jan 1, 1955