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By Patrice Favreau, R. F. Ph. D. Professor Emeritus Favreau

After Nobel invented dynamite, blasts were carried out by trial and error, without the use of equations based on the fundamental principles of Chemistry and Physics, although everyone accepted that shock waves were involved; but no equations were available to calculate their intensity. Around 1950 however, M.A. Cook proposed a procedure to calculate the thermochemistry of an explosive, and thus evaluate theenergy released during the explosion of a fully confined explosive. Some blasters then began to use theEnergy Factor; the latter, however, does not subdivide the energy into its three kinds of activities necessaryfor a successful blast, as demonstrated in 1968 by reference 2, namely i) the shock wave which weakensthe rock; ii) the stress field SS which fully fragments the rock; and iii) the release of the stress SS whichcauses the fully fragmented rock to burst out with the velocity necessary to move the rock into the muckpile. The article explains that the way to achieve a successful blast is by insuring that the explosive energy divides properly into the weakening action of the shock wave which is necessary to prevent large collar blocks and toe, and into adequate stress field intensity SS which is necessary to obtain good fragmentation size distribution at the crusher, as well as adequate burst out rock movement to achieve easy mucking.

By M. C. Flemings, A. A. Tzavaras

Analytical and experimental procedures are descrihed for quantitative determination of volume-fraction microporosity in metals by mimorarlio-graphg. The analysis assumes spherical pores but allows for the observed fact that pores or portions of pores smaller than a given thickness do not project an image on the film. Volume-fraction microporosity was measuured in cast low-alloy steel and shown to vary from 0.6 x 10-4 to 10 x 10 depending on mode of solidification and on whether the material was air- or vacuum-cast. The aim of work described herein was to develop a method of quantitative measurement of the volume fraction of microporosity in cast metals. Microporosity, present in nearly all castings and ingots, is always interdendritic in nature and may be large enough to be seen on a polished surface with the naked eye. More generally, it is smaller in size, and its detection more difficult. Three techniques might be considered for measurement of microporosity: 1) lineal analysis of a polished metallographic surface, 2) density measurement, or 3) quantitative microradiography. As will be shown later, volume fractions of porosity in directionally solidified castings may be the order of 10-4 to 10-3; such small amounts of porosity are difficult to identify and measure on a polished surface. Density measurement is also not a suitable technique (for alloys) when the volume fraction of porosity is low. This is because the density of the base metal is often not known within the necessary accuracy, due to microsegregation or partial phase transformations. In general, it is not possible to completely eliminate microsegregation without also altering the porosity. Because of the limitations of the foregoing techniques, quantitative microradiography was employed to determine amount of porosity. In recent work, microradiography has been found to be useful for qualitative measurement of porosity, including determination of size and shape of individual pores;&apos;)&apos; however, quantitative determination of amount of porosity has not been attempted. I) CALCULATION OF VOLUME-FRACTION POROSITY The following analysis employs procedures similar to those of Cahn and Nutting3 and Hilliard.4 Major simplifications are that pores are assumed to be spherical and to be present in sufficiently small quantities that no overlapping occurs. A basic difference from the previous treatments is that the limited "sensitivity" of microradiography is considered. Assume first 1) cavities are spherical and of uniform diameter, 2) cavities are randomly distributed, 3) volume-fraction porosity and specimen thickness to pore radius ratio are sufficiently small that overlapping of the projected images of cavities is negligible, 4) sensitivity is limited (i.e., holes or portions of holes of less than a given thickness do not project an image on the film). The sensitivity, is defined as: where 5 = minimum thickness of void from which an image will be projected on the film and t = specimen thickness. Now, from Fig. 1, it is possible to distinguish between two different types of holes. These are 1) holes whose centers lie within the region t/2 > X > 6/2, where X is distance from one surface of the specimen (positive into the specimen), and 2) holes whose centers lie within the region (6 — r) < X < 6/2, Holes whose centers lie outside X = (6 -r) project no image on the film. These two types of pores are considered separately below. Type 1 Pores. When 6 is greater than 0, the image of a spherical cavity of radius r appears on the film as a circle of radius a which is smaller than r. From geometry, Fig. 1: a2=r2-52/4 [2] where a = radius of image of pore on film and r = radius of pore. Since the pores are randomly distributed and spherical V =4/3pr2Nv [3] where V = volume fraction of voids and Nv = number of pores per unit volume and the number of images of Type 1 pores per unit area of film, N&apos;A, is

Jan 1, 1965

By Adnan A. Malik, Tadashi Maejima, Jiro Kuwano

"The use of steel screw piles has greatly increased in recent years because of the advancement in the installation mechanism and its performance under compressive, uplift and lateral loads. In a steel pile system, the strength of pile material limits the end bearing resistance of the pile due to strong subsurface conditions. The installation mechanism of screw pile can reduce the end bearing resistance due to the torque and axial force. However, if the installation mechanism does not reduce the bearing resistance of the pile, another important factor that can reduce its performance is the strength of the helix/wing plate. In this study, the effect of wing plate deformation on the performance of single helix/wing plate pile bearing resistance investigated. A model ground was used to investigate the effect of wing plate deformation. Dry Toyoura sand was used as a ground material and was compacted to denser states of 80% and 92%. The shaft and wing plate material of the pile was the same to actual piles that are used nowadays in Japan. A series of load tests were performed with different wing plate diameters and thicknesses. It was observed that deflection in the wing plate reduces the bearing resistance of the pile. The increase in the thickness of the wing plate was seen to restore the reduced pile resistance due to deflection. It was also observed from the experimental results that the ratio of wing plate diameter to shaft diameter (Dw/Ds) greatly affects the deformation of wing plates, which ultimately affects the end bearing resistance of the pile. The results obtained in this research suggest that the outstand length (Lw) of wing plate should be less than 5.6 times the thickness of wing plate for piles having a large Dw/Ds ratio under strong ground conditions.INTRODUCTIONThe first use of screw pile was almost 180 years ago by Alexander Mitchell. He patented his invention in 1833 with the name “Screw Pile”, and used it for ship moorings. The use of screw piles has since been adopted in various areas such as lighthouses, fencing for agriculture and marine structures. The use of screw piles in civil works started in 1985, after the invention of the hydraulic torque motor, as it eases the installation process. Nowadays, screw piles are used in the foundation of transmission towers, elevators, buildings and many other civil structures.Screw pile has an edge over other steel pile systems due to its high bearing, uplift and lateral resistance. The end bearing resistance of screw pile depends on installation, strength of subsurface material and the pile material. The screw pile is installed by applying torque and axial force. The pile torsional strength should be more than the applied torque and axial force to avoid deformation before reaching the final depth."

Jan 1, 2015

By L Torckler, R L. Brathwaite

At Neavesville gold-silver (electrum) mineralisation occurs in steeply-dipping zones of intense fracturing, brecciation and quartz veining within rhyolitic pyroclastics, carbohaceous shales and andesites. Hydrothermal alteration extends over an area of greater than 3 by 1.5 km. In rhyolitic tuffs, highly silicified zones containing quartz-adularia-illite assemblages are flanked by less silicified assemblages composed of albite, illite-montmorillonite and chlorite. The mineralogy and sequence of alteration are comparable with the alteration zones which envelop the steam-producing fissures of the active Wairakei and Broadlands geothermal fields. Primary fluid inclusions in quartz from five fissure veins in the Neavesville field show maximum homogenisation temperatures ranging from 220&nbsp;- 260¦C and salinities of 0.0 - 1.1 wt&nbsp;per cent&nbsp;NaCl equivalent, which cover a similar range to actual measured temperatures and salinities in geothermal fluids at Wairakei and Broadlands. The age of the rhyolitic pyroclastics and related alteration and mineralisation is probably Pliocene and Neavesville therefore represents a fossil geothermal system. The intensely fractured zones containing the gold-silver mineralisation were probably produced by hydraulic fracturing generated by accumulation under pressure of hydrothermal fluid in blind fault zones. Study of fluid inclusions indicates that hydrothermal quartz associated with electrum was deposited under boiling conditions. High grade electrum mineralisation at Graces workings appears to be localised by reaction of hydrothermal fluid with sedimentary marcasite in black shale.

Jan 1, 1980

By R. August Heindl

[A proposes process for recovering manganese from open-hearth steel-plant slogs is indicated by the flow diagram shown in figure 1. Investigation of the process, the laboratory development of which was reported previously,4/ was expanded to a larger scale. Mixtures of flush slags and limestone were proportioned to have molar [SiO2] ratios of 1.5 to 2.2 and were fired at temperatures up to 2,400° F. In an oxidizing atmosphere. This produced clinker consisting principally me various combinations of the oxides of manganese, iron, aluminum, and magnesium aloe with a dicalcium silicate phase containing the phosphorus. Some tests were made with a continuous sintering machine of the traveling-grate type, but a rotary kiln was the most satisfactory apparatus for this operation. Material was fed at 150 to 200 pounds per hour after first being agglomerated either on the sintering or else binder extruding and drying finely ground mixture of the sing, limestone, binder, and water. Tests with slag; from tree different source indicated overkill manganese recoveries of 65 to 80 percent by ammoniacal-ammonium-carbonate leaching.]

Jan 1, 1955

By W. E. Brigham, P. W. Reed, J. N. Dew

Effect of Hydrophobicity and Frother Concentration on Bubble-Particle Interactions in Turbulent Flow

Sep 13, 2010

By A. E. Desrosiers, R. L. Kathren, D. L. Haggard, J. M. Selby

INTRODUCTION The radiological health significance of thorium-230 stems from its tendency to separate from the uranium238 parent, concentrate in bone tissues, and to subsequently irradiate the radiosensitive tissues lining the bone surfaces and the bone marrow. Indeed, thorium-230 may be the radionuclide which contributes the major dose following intake of natural uranium (Hartley and Pasternack 1979). This is reflected by the most recent recommendations of the International Commission on Radiological Protection, which specify the limits shown in Table I for the annual intake of radionuclides by occupationally exposed workers (ICRP 1979). TABLE 1. Occupational Annual Intake Limits (microcuries per year) for Selected Uranium Nuclides and Daughters (ICRP 79) [Radionuclide Ingestion Inhalation] [Uranium-238 200 0.05 Uranium-235 200 0.05 Uranium-234 200 0.03 Thorium-234 300 200 Thorium-230 3 0.02 Radium-226 2 0.5] Clearly, the relatively low annual limit of intake for thorium-230 shows it to be of greater radiological concern than its parent radionuclides. Because of the greater toxicity and different metabolism of thorium-230, monitoring only for uranium-238 does not satisfactorily identify the possible hazard from thorium-230 nor does it provide any real indication of the metabolism or biodynamics of these two radionuclides. Thorium-230 has a half-life of 80,000 years and can be detected by direct counting of the alpha particles or photons emitted during its transformation to radium-226. The 4.69 and 4.62 MeV alpha particles are distinctive and specific indicators of thorium-230 and are emitted with abundances of 76% and 24%, respectively. The principal photon, a 68 keV gamma ray, is emitted in only 0.37% of the transformations and is, therefore, not useful for low level measurements. The other photons emitted have even lower yields, or, in the case of radium L x-rays, are non-specific and, hence, useless for quantification. High sensitivity measurements of thorium-230 currently are usually accomplished by wet washing of the sample substrate, quantitative chemical separation of thorium atoms, and, finally, direct measurement of the alpha particles emitted from a massless deposition. This procedure is complicated, expensive, and time-consuming, and subject to interferences from uranium, other actinides, and other thorium isotopes. Recently, the feasibility of low-level measurement of thorium-230 by neutron activation analysis (NAA) was demonstrated (Kathren, Desrosiers and Church 1980). Two principal variations of the NAA method were used in this study: 1) instrumental NAA technique and 2) post-irradiation radiochemical separations (RCS). Instrumental NAA procedure is a nondestrucive technique which is preferred because of its simplicity. The procedure is as follows: after irradiation with a known neutron fluence, the samples are transferred to a clean container and quantitative gamma spectroscopy performed. With the radiochemical separations procedure, the sample is initially treated as in the instrumental technique. However, after irradiation, a known amount of "carrier" is added to the sample. The element(s) of interest are then separated from the rest of the matrix by distillation, precipitation and extraction techniques. The resulting sample, now free of interferring elements, is then ready for gamma-ray analysis. The use of a "carrier" is to determine the loss of element-of-interest during the chemical separations process. The neutron activation cross section of thorium-230 has an epicadmium resonance value of 1,010 barns (Mughahghab and Garber 1976) and a thermal neutron cross section of 23 barns. The 25.52 hr thorium-231 produced releases two photons of significance: an 84 keV complex, (6.5% yield) and 25.6 keV (15% yield) (Lederer and Shirley 1978). The 84 keV complex is particularly useful for quantification since neither natural uranium, thorium, their daughters, or activation products emit photons in this region. However, the higher yield of the 25.6 keV photon may result in increased sensitivity if there are no other photons of similar energy emitted by other radionuclides in the sample. PRELIMINARY STUDIES Thorium-230 standard stock solution was prepared from a pure sample of the oxide purchased from Oak Ridge National Laboratory. From this stock solution a series of samples were prepared for irradiation in the TRIGA Mark I reactor at Reed College. Various dilutions were prepared as well as thorium-230 spiked urine samples. Irradiation times varied from 1 to 54 minutes in a neutron fluence rate of 1.84 x 1012 n/ cu m-sec. The neutron spectrum was abundant in thermal neutrons, having a Cd ratio of approximately 10. Treated urine samples were also analyzed by the NAA instrumental method. Analysis of untreated urine samples was not possible due to the high background

Jan 1, 1981

Technically speaking, the concept of NDT sounds like the "magic bullet" when faced with a questionable drilled shaft. All the Contractor or Engineer needs to do is select an NDT method, apply it, understand the details and extent of the defect and determine whether it will impact the load carrying capacity of the shaft during it’s design life. Unfortunately, it is not that simple. NDT is a tool utilized to indirectly assess the condition of the completed drilled shaft. For the most effective interpretation, NDT data should be correlated with the subsurface information, visual observation, and detailed shaft installation records. The basis for acceptance or rejection of drilled shafts should not be solely based on NDT. The parties responsible for specifying, interpreting and using the NDT results must understand the capabilities and limitations of the method to be utilized, in conjunction with the relevant subsurface conditions of the site, before selecting and specifying a system and acting on the results. This is necessary so that an appropriate NDT method can be specified and contracted. In this manner the results and roles of the responsible parties can be clearly defined.

Jan 1, 2004

By M. Taheri

Multiple Attribute Decision Making (MADM) method is applied to select tailings site of the Gol-e-Gohar Iron Ore Processing Plant in the Kerman province, south-eastern of Iran. To select tailings site, screening is applied on eight location proposed by Binnie and Granges. Consequently three sites identified for further studies. Evaluation factors include only the most important factors such as efficiency ratio, elevation and distance to processing facilities, occurrence of faults and fractures. Crisp values such as efficiency ratio, elevation and distance can be determined by measurements and calculations, but some factors such as occurrence of faults and fractures are presented as linguistic values that can be described with triangular fuzzy numbers. Based on evaluation values obtained an optimal tailings site can be selected using a modified Technique of ranking Preferences by Similarity to the Ideal Solution (TOPSIS) given crisp data and linguistic variables as the alternatives of attributes. Each attribute?s weight is assigned using the analytic hierarchy process. The final ranking order aids in the selection of tailings site. Finally, the stages of modified TOPSIS method were applied and site No.2 situated in 5400m to the mill was selected as the best alternative.

Jan 1, 2014

By Jian Wu

In this paper, the surrounding rocks and the supports in a longwall are taken as an integral, i.e. a system. The structural characteristics and behavior of the system are discussed based on in-situ observations. A set of equations, which describe the interaction among the support, immediate roof and main roof, are developed. These equations can be used to design the longwall powered supports more reasonably and economically.

Jan 1, 1989

By Hugo Cabrera-Real

This work investigated the chemical and mineralogical properties of CaO-SiO2-CrOx-CaF2- MgO slags. Synthetic slags were prepared and the effect of the slag basicity (CaO/SiO2) and MgO contents on the stability of the mineralogical species formed was analyzed. The morphology and composition of the slags were analyzed by XRD and SEM-EDS, whilst their chemical stability was evaluated by leaching with an aqueous acetic acid solution. It was found that in slags with CaO/SiO2 = 1, the main Cr-compound was MgCr2O4 spinel, which forms octahedron crystals. Small amounts of CaCr2O4 and CaCrO4 were also observed. It was found that increasing the slag basicity from 1 to 2 the compounds MgCr2O4 and CaCr2O4 were formed together with the Cr(V)-containing compound complex Ca5(CrO4)3F which forms hexagonal crystals. The results showed that the highest chromium concentration levels in the leaching liquors corresponded to slags with CaO/SiO2 = 2, probably owing to the formation of Ca5(CrO4)3F.

Jan 1, 2010

By David A. Lee

It was estimated in Chemical Week1 that the uranium fuel requirements for the U.S. Electric Utility Industry by the mid 1980&apos;s would be about four times that-of what it is today. This corresponds to approximately 45,000 tons per year of &apos;yellow cake&apos; - of which a good portion is represented by ammonium diuranate - vs. the 11,700 ton total estimated for 1975. Perhaps just as significant is the 40-fold increase in thirty years projected for the entire world since 1970. Thus by the year 2000. &apos;yellow cake&apos; production could be in the order of [3]50.000 short tons annually.2 &apos;Yellow cake&apos;, so named because of its inherently bright yellow color, is a finely divided precipitate that can be formed after the leaching step when refining uranium ores. Feed solids enhancement then occurs to at least 50% by weight using filters or centrifuges This is followed normally by drying and then calcining with the conversion of ammonium diuranate to triuranium octoxide represented by the following equation: [9 (NH4)2 U2 07 heat 14 NH3 7 + 15 H2O7 + 2N2/ + 6 U308 4] Theoretically, assuming 100% conversion every 100 kgs. or 100 lbs. of ammonium diuranate will result in 90 kgs. or 90 lbs. of triuranium octoxide.

Jan 1, 1976

By M. H. Dunn, T. P. Danehy, C. F. Denholm, S. L. Busler

The problems associated with abandoned minelands are so extensive that neither federal, state, or local governments nor the mining industry nor watershed groups can adequately address these problems individually. By combining talents and resources, however, these problems are being solved efficiently, effectively, and economically. Utilizing existing water monitoring data, local public-private partnerships have successfully designed and built passive systems within five weeks to six months which treat discharges up to hundreds of gallons per minute that vary in quality from net alkaline to highly acidic, containing as much as 200 mg/L dissolved iron and 70 mg/L dissolved aluminum.

Jan 1, 2002

By S Talu, E Savage, P Sturm, A van As

It is estimated that substandard ground support installations and elements cost the Rio Tinto Copper Group millions of dollars between 2000 and 2014. These issues have also created significant safety and financial risks in Rio Tinto mines. As a result, Rio Tinto Copper has developed CaveCAD, an integrated system to collect, store and analyse all ground support-related data. The CaveCAD system stores geotechnical data and has the ability to automatically import data, collect data through tablet applications, report processed/analysed data and present this data through 3D visualisation software.The CaveCAD Ground Support module closes the design–implementation–verification loop by providing a method of verifying the compliance of all installed ground support, recording manufacturer specifications, recording quality control test compliance and rectifying any non-conformant areas. The module uses innovative technology to create value through cost saving, safety improvements and data collection efficiency. Cost savings will be achieved by a decreased need for excavation rehabilitation, less ‘waste’ due to faulty installation and quality assurance checks reducing the likelihood of substandard support units being used. Data collection will be improved through the use of a mobile tablet application that can be used underground in ‘off-line’ environments.CITATION:Savage, E, Talu, S, Sturm, P and Van As, A, 2016. Development and implementation of the CaveCAD ground support module for cost and safety improvements in block cave mines, in Proceedings Seventh International Conference and Exhibition on Mass Mining (MassMin 2016), pp 769–772 (The Australasian Institute of Mining and Metallurgy: Melbourne).

May 9, 2016

The Bureau of Mines conducted a field study to assess the performance of various chain pillar configurations in terms of gate road entry sta-bility. Vibrating wire stressmeters (VWS&apos;s) were installed in four consecutive gate road chain pillars. Field data collected during panel retreat were analyzed to gain a better understanding of the mechanics of vertical load redistribution in gate road chain pillars as it relates to ground control problems. Several different pillar configurations were investigated including abutment-yield and yield-abutment-yield designs. VWS data indicate that average pillar loads were lower and appeared abutment-yield pillar arrangement was utilized. port the occurrence of severe roof and pillar to stabilize when an Data analyses also supdeterioration that was visually observed in the tailgate entries during panel extraction.

Jan 1, 1988

By F. Soumis

We propose an advanced truck dispatching system which uses mathematical optimization approaches including integer programming, non-linear networks and the assignment problem. The system produces better operation control than existing algorithms. Furthermore, it provides planning tools for choosing equipment and finding an equilibrium between the quality and quantity of production.

Jan 1, 1986

By T Smith, J Hatley

With the increased focus on the need for more uranium mines, this paper presents the design process currently underway for the development of the Millennium deposit in northern Saskatchewan, Canada. This deposit, located 630 - 750 m below surface, will be accessed by two shafts and will be mined by blasthole stoping methods at less than 500 t/d. Mining grade will approximate two per cent U3O8 and mine life is expected to be six to seven years. The project is a joint venture between Cameco, AREVA and JCU. This paper discusses in detail methods used to predict worker radiation exposures, the methods used to monitor the work environment and procedures unique to the uranium industry necessary to minimise worker radiation exposures.

Jan 1, 2008

By P. G. Vikre

Several factors have caused less emphasis to be placed on geologic mapping in mineral exploration in the last 15 years. These include opportunities for "easy" discoveries of near surface gold and silver deposits in developed countries, and of base metal deposits as well in less developed countries, a decline of emphasis on geologic mapping in many universities, and a decline of useful mapping by government agencies in many areas. Geologic mapping is simply a way of recording geologic observations on volumes of rock larger than can be seen from one place. Since most geologic processes involve systems larger than this, mapping is also essential to understand the significance of observations made on smaller volumes of rock, such as thin sections and sample taken for chemical or isotopic analysis. To be useful, the observations recorded through geologic mapping are then interpreted to arrive at an understanding of the 3D geometry and geologic history of a volume of rock, which is used to direct mineral exploration, or any number of other purposes.

Jan 1, 1995

By F. V. Lenel, J. A. Dromsky

The influence of thermal and mechanical treatments upon the elevated-temperature stability, the microstructure, and the mechanical properties of aluminumaluminum oxide alloys is investigated. Compacts from atomized and flake aluminum powders were sintered at temperatures just below the melting point of aluminum in a vacuum of 10-4 Torr for several hours and were then hot-extruded. During this treatment the hydrated oxide present on the surface of the powder particles decomposes, the water vapor produced reacts with the aluminum forming additional oxide, and the hydrogen developed is removed by diffusion to the surface. Extrusions of compacts so treated are stable at temperatures up to the melting point of aluminum and do not form blisters and internal defects typical of extrusions from untreated powder. Electron micrographs of extrusions from unsintered compacts show long parallel oriented platelets typical of the IN previous investigations1,2 the properties and structure of aluminum alloys were described which had been produced by cold compacting aluminum powder and then hot pressing and extruding the compacts. Both the structure and the properties of these alloys differ significantly from those of commercially produced aluminum-aluminum oxide alloys. When commercial alloys are produced, they are given a sintering treatment in air at about 600°C between cold compacting and hot pressing.3 During this treatment the hydrated oxide, which forms the coating on the aluminum-powder particles from which the alloys are prepared, is decomposed.4 The chemically bound water which is released reacts with the aluminum and forms aluminum oxide and hydrogen. Most of the hydrogen is eliminated by hydrated oxide skins on the original powder particles, while the oxide particles in extrusions from sintered compacts are broken up. The strength of extrusions from treated powder is somewhat lower, but their ductility is considerably improved over that of extrusions from untreated powder. The slip-trace patterns on electron microgvaphs of extrusions which had been strained in tension before replication indicated that the grain size of the extruded alloys was approximately the same as that of the original powder particles. Coarse-grained alloys were produced by severe cold work and annealing of the extrusions. They have significantly lower room-temperature strength, but about the same ductility as the vacuum-sintered fine-grained alloys. The size and shape of oxides in the coarsegrained alloys is similar to those of the fine-grained alloys, but the particles are somewhat more uniformly distributed. diffusing to the interior or exterior surfaces of the compact, but it is difficult to eliminate all of it because the solubility of hydrogen in solid aluminum is very low even near its melting point. Extruded alloys which are not sintered before hot pressing and extrusion appear quite sound upon metallo-graphic examination, but develop severe surface blistering and internal fissuring when they are heated to elevated temperatures after extrusion. Fissures and blisters have been observed even in commercial alloys which had been sintered in air, although they are much less severe.&apos; Because of the importance of this sintering treatment it was studied in this investigation in a modified form, using vacuum sintering rather than sintering in air, to insure more complete elimination of occluded hydrogen. The technique is described and the effect of the treatment upon the structure of the alloys is documented. It has been known for some time that extruded aluminum-aluminum oxide alloys are very finegrained, but an exact delineation of grains in electron micrographs has not been possible. In the conventional metallographic-etching techniques etchants attack the interface between the second-phase particles and the matrix in the alloys much

Jan 1, 1964