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By Bruno Michaux, Markus Reuter, Martin Rudolph

"It is relatively well-established in the literature that the flotation of calcium minerals using fatty acids as collector is very sensitive to the process water composition. In particular, hard waters have often been reported to strongly reduce the target mineral recoveries due to the formation of insoluble compounds such as calcium and / or magnesium dioleate, thus reducing the amount of collector available for adsorption onto the mineral surface. In this study, the flotation of a fluorite pre-concentrate was performed with tall oil, an industrial collector essentially containing fatty acids. The tests were performed in a variety of synthetic waters to simulate multiple degrees of water hardness, and to differentiate the role of magnesium and calcium ions on the flotation performance. The flotation tests revealed that, under the studied conditions, a significant difference between flotation in calcium-rich and magnesium-rich waters was observed, suggesting strong ion-specific effects in the system. Specifically, calcium-rich waters slightly improved the fluorite recovery, whereas magnesium-rich waters caused a decrease in recovery by as much as 20%. This paper is focused on the flotation kinetics aspect of the system. This approach highlighted the interesting finding that calcium ions did not simply increase the fluorite recovery, but also significantly increased its flotation kinetics. The magnesium ions, on the other hand, had the exact opposite effect.INTRODUCTIONAs the mining industry is facing an increasing number of issues related to its fresh water consumption, the idea of using alternative water sources for mineral beneficiation is gaining significant momentum. As a result, a proper understanding of the role of water chemistry in flotation is becoming more and more urgent, leading to an increasing number of studies on this topic."

Jan 1, 2018

By Z. C. Zhen

Basing on character of fine ores, and employing all the advantage of dissolved-air flotation, the study within the dissertation put forth the methods of superfine metal mineral flotation with dissolved-air flotation equipment, and constructed a full set of laboratory flotation system. Experiments both in water and in slurry were respectively carried out by means of this flotation equipment. Further study was also fulfilled on mechanism of air-dissolved released devices, and the key components of system including ejector, releaser and saturator were designed. Optimizing devices parameters were chosen by taking ideal performance of the devices into consideration, according to orthogonal experiments and tests on bubbles factors, those performance factors were called air release rate, air release efficiency. The results with some minerals are better than JJF flotation machine with 30 litres bulk. The Dissolved-air Flotation(DAF) machine shows great potentiality in treating super-fine metal mineral concentration. The research indicates the Dissolved-air Flotation(DAF) system has superiority over mechanical flotation machine in fine flotation. Air-dissolved released bubbles appear on the surface of hydrophobic minerals in priority, solving collision probability less in the tradition fine mineral separation, such that the metallurgy technology of fine metallic minerals are improved. The exploratory research is a foundation for industrial pilot, commercial test and equipment maturity in the future.

Jan 1, 2014

By Emery Chilton, Charles Taylor, Mark Senk, Linda McWilliams

Three-axis ultrasonic anemometers are used to study airflow in the NIOSH ventilation gallery where ventilation in an underground mine is simulated. In this study, performance characteristics of this anemometer are evaluated and the effects of sensor orientation and sampler location on flow readings are examined. The study results provide guidelines for more effective use of the ultrasonic anemometers in the ventilation gallery.

By K. S. Whiting

Elevated concentrations of copper, cobalt, and arsenic within the Panther Creek Basin sediments in north central Idaho prompted an evaluation of the sources of the metals. Potential tailings and waste rock source samples collected at the head of Blackbird Creek were compared to sediment samples in the Panther Creek Basin using electron microprobe techniques. The mineral types, degree of alteration, and the morphology of the metal-bearing sediment grains within Blackbird and Panther Creeks were found to consist of copper-, cobalt-, and arsenic-bearing sulfide minerals.

Jan 1, 1997

By Glenn E. Johnson

The Bureau of Mines investigated the production of hydrogen cyanide by reacting powdered coal (minus 300 mesh) with ammonia at 1,250° C in a bench-scale study. Both metallic and ceramic reactors were used. Yields up to 0.7 cu ft of hydrogen cyanide per cubic foot of ammonia consumed r- obtained. The resulting ammonia conversion of about 75 volume-percent approximates conversion obtained commercially in processes utilizing natural gas and platinum catalysts. The coals that had higher volatile-matter contents gave the best yields of hydrogen cyanide. Allowing the coal to adsorb ammonia before reaction resulted in increased yields of hydrogen cyanide. Cost studies for a plant with a 40-million-pound-per-year capacity indi-cate that hydrogen cyanide can be profitably coproduced with carbon black, from coal and ammonia, at the current market price of hydrogen cyanide (11.5 cents/lb). These figures are based on heating the reactor electrically. If a cheaper heating method were devised the economics of the process would be more favorable.

Jan 1, 1967

By W. L. Cornell

The Missouri Pb ores are the only domestic Co resource being mined and processed for other metals; therefore, they present a viable short-term opportunity for Co production. Lead, zinc, and copper concentrates are produced from the ore. The Cu concentrate can contain up to 30 pct Co and the Pb concentrate up to 15 pct Co. Since Co is detrimental to the processing of the Zn concentrate; the remainder of the Co is rejected to the tailings. The tailings can contain as much as 50 pet Co originally present in the mined ore. Researchers at the U.S. Bureau of Mines have successfully tested on a continuous basis a process that recovers a bulk sulfide concentrate from mill tailings. The concentrate contains up to one-half of the Co and from 50 to 90 pct of the Pb, Zn, and Cu. Concentrate weight represents 10 pet or less of the total tailings.

Jan 1, 1989

By M. A. Reinsel

New technology for removal of nitrate from low-temperature waters has been developed. Typical results from the first operational-scale system (operating at a metal mine in Montana since January 1996) are over 90 percent nitrate removal at a flow rate of 130 gpm and a water temperature of 12°C. The system also operated successfully at flow rates as high as 300 gpm and water temperatures as low as 2°C. The ABC is advantageous because it is: a) cost-effective to design, construct and operate, and b) effective at cold water temperatures. The system can be designed for a variety of flows, nitrate concentrations, water temperatures and water qualities.

Jan 1, 1998

By Ashish Agarwal

For a correct evaluation of the performance of any process, it is important to reconcile the data gathered in the plant from the material balance point of view for all the streams flowing in and flowing out of the process unit. There are two main approaches to reconciliation of data, which involve minimization of the sum of the squares of: (i) the closure residuals and (ii) the component adjustments; both weighed with the estimated variances of the components. Though, these approaches have served us well, it has not been possible to ascertain if the reconciled values for various components and the split factors obtained using these approaches are truly the best estimates. In this paper, this aspect has been investigated by analyzing pseudo-experimental data of known error structure on size classification of particles in a hydrocyclone. Three types of basic error structures were considered for the measured component values: absolute error, relative error and chi-square error. The error structure was modified by adding a random component of error using normally distributed random numbers corresponding to zero mean and different levels of variance. By carrying out a large number of simulation experiments, it has been shown that in the presence of random errors, irrespective of the basic error structure of data, which is usually unknown, the chi-square error minimization criterion can be used to obtain most reliable results. Keywords: data reconciliation methods, chi-square error minimization

Sep 1, 2012

By Erico Tabosa, Meng. Jun, Kym Runge, Matthew Brennan, Weiguo Xie, Dee Bradshaw

Turbulence and its distribution are of great importance in flotation cell design as they affect suspension of particles, air dispersion and particle-bubble collision rates, which in turn determine flotation performance. However, there is no mature technique to measure turbulence in three phase (liquid-solid-gas) systems such as in flotation cells. In this article, the authors present two new approaches that are suitable for measuring turbulence distribution in three phase systems and validate their applicability. The first technique uses a piezoelectric vibration sensor (PVS) to measure fluid kinetic energy standard deviation and the second technique applies electrical resistance tomography (ERT) to measure conductivity variation at a measurement position in a flotation cell. For the PVS technique, calibration of the sensor was performed to determine the values of parameters that were needed to calculate the force applied to the sensor. Then measurement was conducted in a 60L batch flotation cell and the results were compared with LDA measurement. This demonstrated that the piezoelectric sensor signal provides a good representation of fluid kinetic energy standard deviation at the position of measurement. For the ERT technique, conductivity distribution data was processed to give conductivity variations, which were then used to calculate fluid kinetic energy standard deviation at the measurement position. The spatial distribution of turbulence obtained by performing multiple measurements at different positions in the 60 litre batch flotation cell was found to agree with the PVS measurement results. These two techniques are potentially powerful tools for turbulence measurement in flotation environments, enabling a clearer understanding of turbulence’s influence on flotation performance to be determined.

Jan 1, 2014

By Xiao Jian Li, Dai Xiong Chen, Jian Wen Yang

In one kind of lead and zinc bearing polymetallic ore containing secondary copper, the characteristic of low sulfur, high zinc, and particularly the existing of secondary copper minerals can lead to lead concentrate with high content of zinc because the dissociation of Cu2+ in the grinding process may have an activation influence on sphalerite. Considering its process mineralogy analysis, a new process of seperation of lead and zinc has been put forward. The experiments focused on the analysis of the advantages and disadvantages of the inhibition effect of traditional adjustment reagent + zinc sulfate on activated sphalerite compared with new organic inhibitor, polysaccharide xanthate. According to the numerical calculation and test results, a reagent system of polysaccharide xanthates is developed, which has a good inhibition effect on Cu2+ activated zinc minerals, achieving high-efficiency separation of lead and zinc. A new reagent system and flotation process was developed under optimal conditions. Under the condition of the run-of-mine ore containing 2.37% Pb and 12.48% Zn, lead of 67.69% grade and lead concentrate with the recovery rate of 86.06%, zinc of 60.32% grade and zinc concentrate with the recovery rate of 96.15% were achieved.

Jan 1, 2014

By Alain Blanchier, Anne Charline Sauvage

Rock mass variations have a huge influence on explosives efficiency and on blasting results. Numerous blasting improvements could be gained by taking into account rock mass and its variations. However, extracted rock mass is generally considered as statistically homogenous. The development of a panel of pre-blast survey procedures that every blaster can use, consists in the realization of a process integrated into every day work: for example as well as toe burden or blast hole depth, discontinuities spacing or the weathering expanse have to enter in rule book, if it provides blasting efficiency and security improvements.

Jan 1, 2004

By T. Gonzales

Magma Metals Company operates an Outokumpu Flash Furnace, four Peirce-Smith Converters and two Anode Casting Wheels supported by six Anode Vessels. Process gasses from the Flash Furnace and Converters are treated in a two train/double contact sulfuric acid plant. Sulfur capture for the smelter is +98%. The new flash furnace was commissioned on July 7, 1988 and has processed over three million tons of sulfide concentrate without a major rebuild. Magma has gained unique experience in the operation of the flash furnace at high oxygen enrichments with low off-gas dust loadings. New procedures have been developed to maintain secondary material generation at equilibrium and for maintaining metallurgical control of operating parameters. This paper describes all the procedures, operation control parameters and operating philosophy that has allowed Magma to achieve superior performance.

Jan 1, 1992

"Real-time, on-stream analysis of the metal content of process slurries is an essential prerequisite for process monitoring and advanced control of mineral processing circuits. On-stream X-Ray Fluorescence (XRF) sensors for base metal applications are available commercially and form the basis of many plant monitoring circuits. To date, these commercial technologies have been insufficiently sensitive to measure precious metals such as gold and platinum group elements, typically present at part-per-million (ppm) and sub ppm levels. CSIRO has developed a novel X-ray based technology, called UltraGold, which enables detection of gold in slurries on a real-time basis with a precision below 100 parts-per-billion. This technology is based on the use of advanced X-ray optics, extensive Monte Carlo computer modelling for analyser design, high accuracy X-ray spectrum fitting where the X-ray intensities are matrix corrected. In this paper, we will introduce this technology and discuss the results of a proof of principle study performed in the laboratory with plant slurries (tailings and concentrate) from an Australian beneficiation plant. Finally, we will discuss further planned improvements. As projected grades in (gold) mining around the world fall and several large-scale mines approach the limits of their economic reserves, this method can enable significantly reduced operating costs by rapid analysis to improve circuit efficiency and hence improve recovery significantly.INTRODUCTION This paper describes a study undertaken to explore the feasibility of applying CSIRO?s UltraGold XRF technology to the on-stream measurement of gold in process slurries. The provision of rapid, accurate information of gold grade in feed, tailings and concentrate streams would facilitate significantly improved process control and early detection of plant upsets, resulting in substantial cost-savings. CSIRO have patented X-ray fluorescence (XRF) techniques for the analysis of key elements in slurries present at part-per-million (ppm) and sub-ppm levels. Conventional, commercially available on-stream XRF instruments generally have detection limits in the tens of ppm range, precluding their use for analysis of elements like gold that are mined and processed at much lower concentrations."

Jan 1, 2017

By L. B. Berger

This information circular is a revision of I.C. 7238, Danger from Carbon Monoxide in the Home, by L. B. Berger and H. H. Schrenk, issued in April 1943. Each winter brings its toll of deaths and serious accidents from the deadly gas, carbon monoxide. Newspapers carry warnings to the public of the, dangers of this gas, and frequent news items report the finding of persons dead at unconscious from the effects of carbon monoxide, yet these accidents continue. Either these warnings are not read, or they are unheeded by people who feel that, "It can't happen to me." It can happen to you carbon monoxide is no respecter of persons.

Jan 1, 1954

By D. Bogunovic

The objective of this research was to conduct field-scale experiments at an operating surface coal mine in order to determine the impact of the bucket fill factor on dragline production rate and energy consumption. Data collected from a dragline monitoring system were recorded in a specifically designed software tool and the relationship among these parameters was established. an algorithm for the determination of the ?best? fill factor was developed and integrated in the software. It was determined for the analyzed dragline in the mine that energy consumption in the digging phase can be reduced by 36% and production rate can be increased by 1.4% for a bucket fill factor of about 80%, a fill distance of 19.8 m (65 ft) (i.e., 3.1 bucket lengths) and a bucket fill time of 15 sec. the method developed and applied in this study may help dragline operators to determine the fill factor that will increase production rates and reduce energy consumption in specific surface coal mines. Mining Engineering, 2011, Vol. 63, No. 8, pp. 48-53. Official publication of the society for Mining, Metallurgy and Exploration, Inc.

Jan 1, 2011

By Erik Westman, Benjamin Mirabile

"Ongoing research is being conducted to evaluate secondary support performance in longwall ventilation entries. In a three-entry longwall gateroad, secondary supports are applied in the #2 entry to maintain a functional airway for the entirety of second panel mining. This airway represents a pathway for contaminated mine air to travel from the longwall tailgate to the mine bleeder system. The ground response curve concept may be used as a design basis for selection of appropriate secondary support in these ventilation entries. Two types of secondary supports are monitored for load and convergence in this project. These monitored supports are pumpable crib supports and interlocking wood crib supports. To evaluate the effect of support density, two installation patterns are monitored for each support type. Both a single-row, protected airway pattern and double-row, full entry support pattern are monitored for each support type. Load and displacement data is collected for all support patterns as second panel mining retreats past instrumentation sites. Data is collected for approximately 200-feet inby the second panel face or as long as safely possible. Load and convergence data collected will be used to calibrate numerical models that will simulate ground response curves for the #2 entry inby the second panel face.INTRODUCTIONWhen a bleeder ventilation system is used, the #2 entry of a three-entry longwall gateroad system is designed to function as a pathway for contaminated air from a longwall face to the bleeder system during second panel mining. The #2 entry is subject to substantial ground movement and loading during its function as an air course because it is a single entry between two longwall gobs. Secondary support is regularly applied in this entry to maintain air course functionality during second panel mining.Research on performance and design of secondary supports has been conducted extensively over the last 30 years (Barczak and Gearhart, 1993; Barczak and Gearhart, 1994; Mucho, Barczak, and Dolinar, 1999). This research has focused heavily on the application of secondary support in longwall tailgate, with little research on the application of secondary support in bleeders or other ventilation entries (Mirabile and Westman, 2018). Secondary supports in #2 entry are likely to experience similar loading and ground movement as those applied in the tailgate entry. However, the designed lifespan of the mine entry and the definition of acceptable ground conditions differs from mine entries where more extensive research has been conducted."

Jan 1, 2019

By D. A. Stanley

Researchers at BCD Technologies and the University of Alabama have applied three statistical techniques to the information contained in a large database of measurements from a phosphate ore processing plant. The rust, Principal Components Analysis (PCA), replaces many measured variables with a few fundamental and un-correlated variables. The second technique, Projection to Latent Structures (PLS), is an extension of PCA that explores the relation between variables identified as either independent or dependent. The third technique, Cluster Analysis (CA), is applied to the results of the PCA or the PLS calculations, and identifies individual data clusters that represent uniform operating conditions in the plant. All three statistical methods can be seen as geometrical operations on the data viewed as points in space. A Viewer gives a corresponding graphical presentation of the data points. This paper describes the use of the above three techniques and the Viewer to explore part of the phosphate flotation database.

Jan 1, 1998

By E. L. Litchfield

Descriptions are given of the techniques and apparatus used by the Bureau of Mines for determinations of flat plate ignition quenching distance and minimum spark ignition energy. The descriptions include discussions of reaction vessel materials, shapes, and sizes and discussions of electrode configurations. Spherical, hemispherical, or flat plate electrodes are recommended. The preferred metal in electrodes and electrode supports is stainless steel; the flat plate electrodes incorporate flanges of low electrical conductivity which are most frequently formed from glass. Various aspects of the electrical energy supply system are discussed and suitable arrangements of components are indicated. The concept of a thermal relaxation time is introduced as a basis for the choice of a minimum interspark time during the testing of a gas mixture. The following indicate the varied conditions under which these tech were utilized: Mixture pressures between 10 mm Hg and 45 psig, initial temperatures between -78° and +198° C, and gaseous mixtures representing wide ranges of cL.. D reactivity and corrosiveness. Minimum ignition energies were determined which varied from about 10-7 joule to nearly 103 joule.

Jan 1, 1967

By Scott Lewis, Andrew Kositsky

"INTRODUCTIONThe South Napa Earthquake of 2014 caused ground motion at numerous reinforced concrete-lined (shotcrete-lined) winery tunnels in Napa County and Sonoma County, California. The occurrence of seismic ground motion at these tunnel complexes, known as wine caves, presented an opportunity to reevaluate seismic performance of reinforced concrete and reinforced shotcrete lined tunnels. The authors of this paper updated the most recent comprehensive compilation and evaluation of case studies by Power and others (1998), which correlates peak ground acceleration (PGA) at tunnel sites to damage. For this update, the authors evaluated the seismic performance of 31 wine caves near the South Napa Earthquake epicenter; including some of the 90 wine caves they designed since 1991, some caves designed by others, and additional caves constructed by contractors that they frequently work with. Tunnel designers can use the new data presented in this paper to help evaluate the usefulness of detailed seismic design analyses. THE SOUTH NAPA EARTHQUAKE The South Napa Earthquake occurred at 3:20 AM Pacific Daylight Time on August 24, 2014. Figure 1 shows the approximate location of the epicenter, the measured/estimated PGA contours, and the location of wineries with wine caves added to the database where the PGA was at least 0.2 g. The epicenter was along the West Napa fault, about 5 miles south-southwest of downtown Napa, California. The earthquake moment magnitude was 6.0, and measured/estimated PGAs were up to about 0.7 g. The duration of strong shaking was about 10 seconds. This earthquake was characterized by right lateral strike-slip fault movement, ground surface rupture, and after slip at the ruptures. Increased surface water flows were observed at seven creeks after the earthquake. Groundwater level rises of up to 5 feet were observed in Sonoma County wells after the earthquake. The earthquake was the largest seismic event in the San Francisco Bay Area, which includes Napa and Sonoma Counties, since the 1989 Loma Prieta Earthquake. The Napa event caused an estimated $400 million in damage. This damage included moderate to extensive structural damage to older commercial buildings and to some newer buildings in downtown Napa. This damage resulted from ground motions, subsequent fires, and failed underground utility systems."

Jan 1, 2016

By Michael Young, Rodrigo Araya, Cesar Gomez, Le Huynh, James Finch

The performance of flotation machines is closely related to the gas dispersion characteristics achieved in their operation. It is known that frothers play a major role not only in the size distribution of the generated bubble population, but also on the swarm rise velocity. A program to characterize frother effects on two-phase hydrodynamics (air-water) of Jameson cells was undertaken in a fully instrumented pilot unit installed at McGill University. Gas dispersion parameters (gas velocity, gas holdup and bubble size distributions) of the gas-liquid mixture generated in the downcomer were measured after its release into the separation chamber. The unit was operated under different conditions including gas velocity, liquid jet velocity and frother concentration (MIBC). Bubble size distributions for concentrations above the critical coalescence concentration (CCC) were narrow with Sauter mean diameter between 0.6 to 1.3 mm. The bubble size followed the general trend as encountered in other types of flotation machines, i.e., rapid decrease with increasing frother concentrations below 10 µL/L, and almost no change in size for concentrations above 30 µL/L. The CCC was between 10 and 15 µL/L. Strong correlations were found between bubble size and air-to-liquid flow ratio (APR), and between the bulk density of the aerated solution in the separation tank and the vacuum inside the downcomer. An equation is proposed to estimate gas holdup in the separation tank from vacuum and bulk density readings.

Jan 1, 2014