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By Kenneth J. Miller

The Federal Bureau of Mines coal-pyrite flotation process has been modi¬fied to produce a concentrated final clean coal slurry underflow that could be dewatered more effectively by filtration or centrifugation. This change was accomplished by redesigning the Bureau's two-stage flotation pilot plant facility and running the second-stage flotation step with undiluted or only partially diluted first stage coal froth concentrate. Results of the pilot plant flotation tests showed that substantial sulfur reduction could be achieved by flotation with undiluted pulp but some dilution is recommended for maximum selectivity. For example, coal-pyrite flotation in slurry of 25 percent solids yielded clean coal products analyzing as low as 0.7 percent pyritic sulfur and froth reject products containing slightly over 3.0 percent pyritic sulfur. In comparison, coal-pyrite flotation with pulp diluted to about 12.5 percent solids yielded clean coal containing as low as 0.4 percent pyritic sulfur and froth reject of 5.6 to 6.7 percent pyritic sulfur. Despite the need for some dilution, it was concluded that excellent coal-¬pyrite flotation selectivity could be achieved without diluting to 6 or 7 per¬cent solids as done in the earlier work. Thus the economics of coal-pyrite flotation would be improved by easing clean coal dewatering problems and by reducing second-stage flotation cell volume requirements.

Jan 1, 1977

By S M. Roscoe

Relationships of Noranda sulphide deposits to volcanic rocks are reviewed and chemical variations within the volcanic sequence are described. The assemblages of minor elements in the pyrites and pyrrhotites of the Noranda and l\llatagami deposits are similar and are characterized by a high content of cobalt, tin and other elements. Isotopic compositions of lead, other geochronological data and stratigraphically disposed zonal distributions of sulphides and minor elements indicate that the deposits were formed prior to folding and metamorphism. Lead isotope data indicate that the Matagami deposits, and several others, were probably formed about 2.95 x 109 years ago and that the Noranda deposits may be about 50 million years younger. The volcanic sequence at Noranda is younger than the thick sequences bordering it on the east and on the west. The relationships are consistent with the hypothesis that these strata-bound sul1>hide de-posits are coeval with their associated volcanic rocks. T HE writer has been engaged in a metallogenic study of the region between Sault Ste. Marie and Chibougamau. An essential objective of this study is the classification of mineral deposits with regard to their composition, form, geological

Jan 1, 1965

By J B. McConnell

The Thompson smelter has three unique features which form the basis ~f its design: fluid bed roasters which treat nickel concentrate filter cake from the mill, as well as the flux, in order to achieve partial desulphurization; the use of electric furnaces for the smelting of the partially desulphurized, preheated roaster product; and the disposal of slag by water granulation and slag slurry pumping. The installation consists of three fluid bed roasters, each feeding an electric furnace. Nickel concentrate is received at the smelter via pipe line. It is thickened and filtered, and the filter cake, together with siliceous flux, is fed through rotary bin feeders and reciprocating double-gate seals into the fluid bed roasters. Air injected into the roasters through club-head tuyeres oxidizes part of the sulphur and associated iron in the concentrate. The heat of reaction dries and heats the charge. Roaster product is recovered from the gas stream in cyclones and from the roaster bed through automatic valves.

Jan 1, 1963

By Mark Van Dyke, Gamal Rashed, Khaled Mohamed, Timothy Barton, Morgan Sears

"The unconfined compressive strength (UCS) of coal is an important parameter that controls the stability of coal ribs in underground mines. Estimation of the UCS of coal units composing the rib is required for conducting the rib stability assessment technique. This technique requires conducting large numbers of conventional UCS tests in a laboratory, which are expensive and time consuming. The research work outlined in this paper examines the use of indirect strength estimation methods—the point load test (PLT) and the in-situ Schmidt hammer test (ISHT)—for evaluating the intact strength of coal. The conventional UCS test was conducted on 80 coal specimens from 10 different coal seams for eastern coals. For each coal seam, the PLT and the ISHT were compared with the UCS test results to establish a correlation between the strength indices from the PLT or ISHT and the UCS. Moreover, to simplify the estimation of the UCS, a correlation between the megascopic coal lithotype and UCS was established.INTRODUCTIONBased on Mine Safety and Health Administration (MSHA) reports, rib failures have resulted in 17 fatalities, representing 52% of the ground-fall fatalities in underground coal mines in the United States over the past decade (MSHA, 2018). In an attempt to control rib failures in underground coal mines, the National Institute for Occupational Safety and Health (NIOSH) is working on developing a coal rib stability rating technique to provide a quantitative means to characterize the stability of coal ribs and to provide guidelines for early selections of rib support. The unconfined compressive strength (UCS) of coal units composing the ribs is one of the key input parameters required to estimate coal rib stability. The UCS of coal is an important parameter that controls the resistance of coal ribs to fracturing and slabbing. Direct determination of the UCS is time-consuming and expensive. Moreover, the UCS may be limited to testing only the strong coal samples since the weak or highly cleated samples might not survive the transportation and the preparation process (cutting and grinding). Therefore, alternative methods have been tested to indirectly find the intact strength of coal, such as the point load test (PLT) and the in-situ Schmidt hammer test (ISHT). The acronym ISHT refers to Schmidt hammer tests that were conducted in-situ on coal pillar ribs, while the acronym SHT refers to tests that were conducted on small scale blocks of coal."

Jan 1, 2018

By B. Alegria

The depressing effects of different inorganic chemicals on the flotation of pyrite have been investigated in this study. The results of the flotation tests indicate that pyrite can be depressed by oxidizing as well as reducing agents under controlled conditions of pH and reagent dosage. Oxidizing reagents such as potassium chromate and potassium dichromate were found to cause complete depression of pyrite in the acidic pH range. These effects are similar to those obtained in the pyrite-cyanide system. A less stable oxidant, potassium permanganate, inhibited the flotation of pyrite at a concentration as low as 0.1 mol/L at all pH values, Addition of reducing chemicals such as ferrous chloride or manganous sulphate to the flotation of pyrite were found to produce depressing effects depending on the additive concentration and pH of the solution.

Jan 1, 1982

By J S. J van Deventer, D C. Shallcross

New developments are taking place in the recovery of gold from leached pulps that are based upon the adsorption of the metal cyanide species onto ion exchange resins. Despite the success of several resin-in-pulp pilot plant operations in the Western World and large-scale plants in the former Soviet Union, the process is yet to gain recognition as a viable alternative to the carbon-in-pulp process. An experimental research program has investigated the use of a variety of different types of resins for the recovery of gold, but to-date no resin studied has the desired properties of high selective loading capacity for gold cyanide and a simple inexpensive elution procedure. In addition very little is known concerning the physical strength of resins and their ability to resist shattering due to osmotic shock during cycles of adsorption and elution. The ability of ion exchange resins to enhance the leaching of refractory and re-adsorbing ores has not been investigated. This paper highlights the necessary factors that need to be addressed before commercialisation of ion exchange technology for gold extraction is feasible.

Jan 1, 1998

By Hugh Haddow

This paper describing the methods of recovery and treatment of a sand and gravel deposit and the preparation of these materials for a number of special markets is one of a series being prepared by the U. S. Bureau of Mines. It is of particular interest to those sand and gravel operators who have a surplus of fine sand which must be sent to waste, both from the point of view of, equipment and the variety. of markets supplied, and in that it describes one of the few sand and gravel plants which have resorted to hydraulic classification for sizing fine sand. ACKNOWLEDGMENTS The author wishes to acknowledge the assistance of J. R. Thoenen, mining engineer of the Bureau of Mines, in the preparation of this paper.

Jan 1, 1931

By Mike Dry, Mani Manimaran, Mykolas Gladkovas, Mariam Melashvili, Chris Fleming

Development of a new hydrometallurgical flowsheet requires quantitative description and optimisation of all chemical processes in each step in the process, as well as mass and energy balances across a fully integrated circuit incorporating all the unit operations. This paper covers steps leading to early modelling of a gold processing plant based on a bromine/bromide lixiviant. Research conducted at SGS Lakefield in collaboration with Albemarle provided the data that were used in the development of this model. A previous investigation in this series described the leaching behaviour of various mineral types in Stabilized Bromine reagent. This paper is concerned with the gold recovery operations associated with a conceptual bromine leaching process. The recovery of gold by different types of resin and activated carbon was studied, along with various methods of stripping the gold from the extractant. The circuit is closed by electrolysing the spent leach liquor to oxidize some of the contained bromide back to bromine that would allow recycling the regenerated leach solution back to the leach step in the process.

Jan 1, 2015

By V Glenn, P McKenna, H Vickers, P Audet, M J. Gillespie, A Gravina, D R. Mulligan

A requisite corollary of mineral sand mining on North Stradbroake Island (Queensland (Qld), Australia) has been the progressive rehabilitation of post-mined lands for the revegetation of native subtropical Eucalypt communities. Since 2005, rigorous environmental monitoring has been undertaken to verify the annual development of post-rehabilitated sites. From these long-term analyses, a chronosequence of land revegetation (ranging from three to 26 years postrehabilitation) was developed to examine the rehabilitation trajectories of various post-mined sites in relation to proximal undisturbed locations. Here, we identified that some sites may be deviating from the intended natural analogues as evidenced by the opportunistic colonisationand otherwise æinvasiveÆ behaviour of a regionally native species (Black Sheoak - Allocasuarina littoralis), which appear to be displacing the intended Eucalypt varieties. Although it is recognised that the broader data trends correspond to distinct periods of adaptive modifications to the implementation of rehabilitation (ie pre- and post-1995), this analysis focuses on further identifying potential above- and belowground feedback mechanisms underlying these divergent ecological outcomes.CITATION:Audet, P, Gravina, A, Glenn, V, McKenna, P, Vickers, H, Gillespie, M J and Mulligan, D R, 2012. Above/belowground feedback may facilitate and sustain mono-dominance on rehabilitated North Stradbroke Island, in Proceedings Life-of-Mine 2012 , pp 15-24 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Jul 10, 2012

By R. W. O. Kersten

"The aim was to investigate stable pillar design procedures currently in use on chrome and platinum mines, subject them to a critical appraisal, and review some of the alternatives proposed in the literature. It is concluded that these pillar design methodologies suffer from drawbacks that can be detrimental to the mining industry and that an improvement is essential.It was decided that the increased availability of analytical models and failure criteria could be exploited to update the empirical to an analytical/empirical method. The proposed methodology adopted FLAC2D simulations using the Hoek-Brown failure criterion to calculate full stress-deformation curves for typical pillars. The mine stiffness concept was introduced to determine the pillar load, integrating the influence of the pillar and strata stiffness and mining geometry.The proposed methodology was calibrated by comparing experimental and predicted deformations and failure depth of pillars in one hard-rock mine. The conclusion was that the methodology is an improvement over the one currently in use. An improved factor of safety is given by the intersection point of curves for the stiffness of the system and the pillar strength. IntroductionThe paper describes part of the findings of a PhD thesis (Kersten, 2016) on an alternative stable pillar design methodology. This publication contains sufficient information to implement the method for further interpretation and testing. A detailed comparison of measured and predicted data is dealt with in the thesis, and the results show that there is promise in the methodology.The design of stable pillars in mining is of fundamental importance, not only in the Bushveld Complex mines but throughout the mining industry. Wherever mining occurs, pillars are formed at some stage and it is essential to predict their behaviour, i.e. whether they will burst, yield, or remain stable. Although of crucial importance, pillar design still suffers from major shortcomings and weaknesses."

May 1, 2019

By George C. Toland

Most existing impoundment ponds and dams leak effluent into the soil or rock upon which they are constructed. However, proposed environmental legislation will require very stringent control on the release of toxic effluents such as cyanide. More exacting investigation, design, and construction techniques than have been used in the past will be required to satisfy these new regulations. This paper discusses the types of field and laboratory investigations required to develop the data for the design of an impoundment system containing toxic effluent, and discusses in detail technical considerations necessary to design this system. Design topics include reservoir sealing with natural and man-made materials; embankment sealing; embankment design considering stability, surface hydrology, capacity, and downstream catchment basins; and special implications of cyanide effluents.

Jan 1, 1975

By K. V. Raj

"The development and advancement of computational fluid dynamics (CFD) has made it possible to better understand pollutant flow and distribution in deep open pit mines. Open pits located at higher latitudes, especially in the Arctic and sub-Arctic, face a unique problem due to atmospheric temperature inversion, which is prevalent during much of the winter. A three-dimensional CFD model of an actual open pit mine in the Arctic was developed to analyze the problem of pollutant growth during inversion, and mitigation of the pollutants through improved ventilation schemes. Due to the availability of mine-specific data, such as contaminant concentrations and coordinates of sampling locations, the actual 2013 pit geometry was used for model validation Concentrations predicted by the selected realizable ?-e turbulent model are compared to measured pollutant concentrations at the open pit. Pollutant concentrations at selected locations showed differences, but remained within the same order of magnitude in most cases. INTRODUCTION Computational fluid dynamics (CFD) has emerged as a useful tool for ventilation modeling in underground mines (Edwards and Hwang 1999, Purushotham and Bandopadhyay 2009, Wala et al. 1998, Xu et al. 2011). Application of CFD in open pit mines has been limited, however, since most open pit mines located at lower latitudes do not encounter considerable ventilation problems. Open pits located at higher latitudes, especially the Arctic and sub-Arctic, face a unique problem due to atmospheric temperature inversion, which is prevalent during winter. A number of Russian researchers have tried to understand the air inversion and resulting pollutant transport problem by modeling air flow phenomena in open pit mines (Baklanov and Burman 1996, Baklanov 1984, Baklanov 1995, Belousov 1985, 1989, 1995). Much of their work, however, was based on numerical models and methods of finite difference. Baklanov (2000) applied a modified ?-e and a ?-l CFD model to air flow phenomena on various terrains. More recently, Choudhury (2011) used the COMSOL CFD package for modeling pollutant transport for an idealized open pit mine. Collingwood et al. (2012a, 2012b) used a two-dimensional model for fluid flow and contaminant transport at an Arctic open pit mine. The authors have also previously presented work on CFD modeling of an actual open pit mine at high latitude (Bandopadhyay et al. 2014, Raj et al. 2015a). However, the CFD work done by the above-cited researchers lacked model validation with field-measured data. Validation of a developed model is important in assessing the quality and accuracy of the predicted results. In general, experiments are done numerous times in controlled environments to assess the validity of collected data. There are two types of assessments used in CFD simulations: (1) verification and (2) validation. Model verification is checking the accuracy of the computer codes during the implementation phase of a real-world problem, within the specific limits of accuracy (Oberkampf and Trucano 2002). Since, the pollution transport model presented in this paper used the commercial ANSYS-FLUENT CFD package, verification is not needed as the program has been tested widely, and verified numerous times."

Jan 1, 2016

By P S. Jaitawat, M Sarim, M P. Roy, P K. Singh, A Joshi

Mining is being carried out using the sublevel open stoping method at the Kayad underground mine. The mine will ultimately reach a depth of 390 m. Kayad village is only 100 m (horizontally) from the underground mining areas. As a result, blast-induced ground vibration is one of the major issues for the residents of the village. This paper deals with the process involved in optimising blast design parameters at the development face blast, slot raise blast and ring hole blast to control blast-induced vibration within safe limits while ensuring improved production, productivity and safety. In total, 1041 development face blasts, 110 slot raise blasts and 52 ring hole blasts were conducted, and 2612 vibration data were monitored in the village at different locations. Initially, electronic delay detonators were used, with an emphasis on controlling vibration in the surface structures. Subsequently, shock tube (Nonel) initiations were used as the blasting faces reached lower depths. A comparative study was also performed for both the initiation systems. The orebody width generally varied from 3.1 to 7 m, and ring hole designs were optimised accordingly. The number of holes in a ring was up to seven and the depth was up to 23 m, depending on the size/width of the orebody. The ring blasts were performed with 64–340 kg of emulsion cartridge explosive and detonated with explosive weight per delay of 10.92–17.16 kg. Extensive experiments were performed and blast-induced vibrations were controlled in the village. Deck blasting (ie up to four explosives decks) was used in a blasthole and the explosive charges were separated by delay detonators, which helped to control the vibration in the village. The actual detonation time of each deck was recorded by monitoring the in-hole velocity of detonation of the explosives, and the charging patterns were optimised accordingly to get the desired blast results.CITATION:Roy, M P, Singh, P K, Sarim, M, Jaitawat, P S and Joshi, A, 2015. Blast design and vibration control at Kayad lead-zinc underground mine, in Proceedings 11th International Symposium on Rock Fragmentation by Blasting, pp 533–544 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 24, 2015

By F. Chevarin

The reaction of O2 with the carbon anode is considered as the main parasitic chemical reaction affecting Hall-Heroult process anodes. The current study aims at investigating the influence of the microstructure of baked anode on its overconsumption. Samples were removed from different positions of an industrial anode. Density, porosity, Lc and BET specific surface area were measured. The anode reactivity was evaluated based on the weight losses for the samples resulting from the reaction of anode with air at 550°C after 7h. The essential parameters determined to control the air reactivity are closed porosity, Lc and pores with a pore entrance radius of 1.5, 8.5 and 12 p.m. The knowledge of effects of these parameters allows better understanding of the reactivity of anodes and consequently reduction of their overconsumption in electrolysis bath.

Jan 1, 2011

By Milorad Cirkovic

Kinetics of copper concentrate oxidation in roasting processes in a fluidized bed reactor has been studied at temperatures between 600°C and 720°C using particles of 0.038 to 2.5 mm in average size. The analysis of composition of samples has been done by chemical methods. Phase composition has been determined by Siemens X-ray equipment with Cu anticathode and Ni filters at a voltage of 40 kV and a current of 18 mA. The content of sulphur has decreased from 33.23 to 19.02 mass percent with the increase of temperature, but the content of Fe304 has increased from 0.15 to 17.14 mass percent. The new mechanism of copper concentrate oxidation in a fluidized bed reactor is proposed in this study. It has been shown from the mathematical model that the velocity of oxidation of copper concentrate between 600°C and 720°C is virtually controlled by the rate of diffusion of 02 through the layer of reaction product.

Jan 1, 1999

By Levi de Oliveira Bueno

Constant stress testing was used for characterization of creep behavior of a 1Cr0.5Mo steel plate in the virgin condition. The tests were performed on creep machines equipped with Andrade-Chalmers type profiles, high sensitivity SLVC transducer extensometry, high stability temperature controllers, and facilities for monitoring the creep curves with an automatic data logging system. Ten creep machines of this type were used in this research, in an experimental work that lasted for one year. Three temperature levels were selected: 538, 565 and 593°C, with stress in the range from 69 to 258 MPa producing rupture times varying from 8 to about 4908 h. The creep curves were all followed with great scrutiny using data logger scanning rates which enabled storing thousands of readings in each case. The experimental analysis involved measurements of minimum creep rate, rupture time and final elongation at rupture. The data were analyzed according to the classical phenomenological / physical relations (Norton, Arrhenius, Zenner-Hollomon, Monkman-Grant) and also considering five traditional parameterization methodologies (Larson-Miller, Orr-Sherby-Dorn, Goldhoff-Sherby, Manson- Haferd and Manson-Succop). Comparisons are presented among the possibilities of data extrapolation from five different methodologies. Comparison is also made with creep results mentioned in literature for the same material in the virgin condition.

Aug 16, 2017

By Farrel W. Lytle

An X-ray emission spectrographic method of analysis is presented for determining rare-earth elements in fractions obtained from bastnaesite ore. The method includes determination of yttrium, thorium, lanthanum, and the rare-earth elements in various complex mixtures. The analysis technique is based upon comparing the samples with synthetic standards approximating the composition of the samples. Working curves are plotted on an absolute-intensity basis, with no correction for back-ground. Examples of working curves and the analyses of typical rare-earth concentrates are included. The selection of spectral lines for the various sample matrices is discussed. A special technique is used for samples in which rapid hydration and carbonation occurred. By analyzing synthetic samples of known composition, the accuracy of the method was determined. The average error of analysis was about 3 percent of the amount present in the range from 5 to 100 percent and about 7 percent in the 0.2-to 5-percent range. A maximum of about 40 samples per day may be analyzed for 7 elements each.

Jan 1, 1957

By R. G. Reddy

Spent potliner is generated in the electrolytic process of reducing alumina to make aluminum metal using molten fluoride electrolytes. Spent potliner (SPL), obtained at the end of the pots life contains a small amount of cyanide and fluoride which present environmental problems. SPL became a listed hazardous waste under RCRA (K088) in July, 1990. One of the possible uses of spent potliner is as a substitute for Calcium Fluoride (CaF2) as a fluidizer in iron-and steel making and in the glass industry. A low viscosity and a low melting point are prime requirements for accomplishing the above. In the present study, viscosity measurements were performed. Effect of various additives, such as sand, limestone, dicalcium silicate dust, and MgO baghouse dust on the viscosity of SPL was studied. The results showed that with the addition of sand and limestone, very high fluidity of SPL melt can be obtained at significantly low temperatures. The results suggest that spent potliner mixed with additives could potentially be used as a substitute fluidizer.

Jan 1, 1999

By Hideya Sato

Refractory wear caused by melts is one of the major determining factors for the interval of shut-down repair of the metallurgical furnaces in general. Calcium ferrite slag employed by M it subishi Continuous Copper Converter, shows hi& fluidity and corrosive characteristics against most of the refractories. In order to improve the corrosion resistance of the refractories, the mechanism of MgO-based refractory wear by the calcium ferrite slag was intensively studied. The dissolution behavior of the refractory into the molten slag and the penetration of the molten slag into the refractory were observed by crucible tests and newly developed oscillating furnace tests. It was found that the wear of MgO-based refractories by the calcium ferrite slag is mainly dominated by the internal structural failure caused by the penetration of CaO-Cu20 rich slag which is formed as a result of the preferential absorption of FeO, from original slag by the spinel of the refractory.

Jan 1, 1999

By H. R. Babitzke

The purpose of this Bureau of Mine- investigation was to develop columbium and tantalum alloys suitable or u at elevated temperatures. Columbium and tantalum were combined with tungsten, hafnium, zirconium, molybdenum, vanadium, and titanium, and the resulting alloys were evaluated with respect to workability, hardness, electrical resistivity, strength at elevated temperatures, oxidation resistance, and weldability. Cb-33Hf-10W-10Ti, Cb-20111-5Mo, and Cb-30Hf-5Mo exhibited superior high temperature properties. Cb-33Hf-10W-10Ti had tensile strength values of 44,300 psi at 1,200° C and 16,500 psi at 1,400° C, Cb-20Hf-5Mo had values of 35,700 and 20,700 psi, respectively. The corresponding values for Cb-30Hf-5Mo were 38,900 and 17,800 psi. These alloys are fabricable by conventional methods with excellent strength at temperatures up to and including 1,400° C. An oxidation rate of 7 to 21 mg/cm2/hr was observed up to 1,000° C.

Jan 1, 1967