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By J. C. Mertz

ACCURATE knowledge of the solid solubilities of the elements that dissolve in the important base metals is needed for guidance in the preparation and heat-treatment of the alloys derived from these compo-nents. While there is still difference of opinion concerning the merits of the X-ray and microscopic methods of determining such solubilities, it is certainly true that the recent extensive use of X-ray diffraction to review the existing constitutional data has revealed many glaring inaccu-racies and has brought about a much improved knowledge of phase-boundary locations, which will inevitably come to include all of the important alloy systems. When the work is done with all necessary precautions it appears that in the majority of cases where the solubilities extend beyond a few tenths of a per cent the X-ray back-reflection technique is capable of furnishing the best of information in this field. For the most prolonged and thorough studies it is obviously advisable to combine the results of several methods, in particular, to obtain an agreement between X-ray and microscopic data. This paper reviews the work previously done on the solubilities of phosphorus, arsenic, antimony and bismuth in copper and, in considera-tion of the uncertainties thus made apparent, presents, new X-ray data obtained with the first three members of this group.

Jan 1, 1936

By C. H. Jr. Herty

DURING the past few years frequent reference has been made to a certain type of iron known generally as "bad iron," "dirty iron," etc., both by steelmakers and producers of iron castings.1 Open-hearth operators have claimed that such iron was entirely within the specified limits as to ordinary analysis but it was difficult to make good steel from it. It has been suggested that unreduced material in the iron is responsible, also that most trouble is experienced with the iron when the blast furnace is delivering a product whose analysis is more or less variable. Other reasons suggested are the use of scrap or borings, unsintered flue dust in the burden, a cold hearth, too high a proportion of unsuitable grade of ore, or the form of the carbon in the iron. Accordingly, a subcommittee was appointed at the fall meeting of the Open-hearth Committee of the American Institute of Mining and Metallurgical Engineers held in Pittsburgh in October, 1926, to investigate the reasons for the occurrence of this bad iron and suggest methods for preventing its appearance. This committee enlisted the cooperation of the U. S: Bureau of Mines Experiment Station at Pittsburgh in undertaking a study of pig-iron quality as affecting the open hearth. The following is a report of the findings to date:

Jan 1, 1929

By K. G. Tshilombo

It should be possible to use an oxygen probe to follow iron removal during converting, if local equilibrium is established between iron in the matte and the iron oxides in the fayalitic slag. The oxygen activity is expected to increase strongly as the iron content of the matte decreases (and the iron activity in the matte drops) while the iron oxide activity in the slag remains constant. To test this idea, oxygen activities were measured in synthetic mattes (made up of mixture of Cu2S, FeS and Ni3S2) when in contact with silica saturated SiO2-FeO slags, and silica and (initially) magnetite saturated SiO2-FeO-Fe3O4slags. The measurements were performed on laboratory scale at 1250°C, using an oxygen probe consisting of a stabilized zirconia electrolyte and Fe/FeO reference, and containing the sample in a silica crucible. Electrical contact to the matte was by means of a platinum wire. The measured oxygen activity was sensitive to the iron content of the matte, and insensitive to the composition of the gas atmosphere over the melt. The measured oxygen activity was generally close to that predicted by Fact Sage calculations. This indicates that such oxygen activity measurements could be useful to monitor iron removal during converting of nickel-copper-iron mattes.

Jan 1, 2006

Develop a safer, more effective, and more efficient method to control fires in abandoned coal mines and waste banks. Maintain the costs of this new method at less than or comparable to conventional AMI fire control methods. How It Works Cryogenic extinguishment of subsurface fires is a method of heat transfer. Bureau-designed injection equipment produces a pumpable slurry of liquid nitrogen and solid particles of carbon dioxide. Liquid or gaseous carbon dioxide from a pressurized tank flows to a bell-shaped nozzle where the change in pressure causes the carbon dioxide to form a granular snow. The solid carbon dioxide is mixed with liquid nitrogen. A jet pump is used to move the slurry through the delivery lines and into a simple injection probe. At injection, the nitrogen vaporizes and the carbon dioxide sublimes. This phase change produces a cold gas (-180° C) that, as it expands and moves in all directions, removes heat and also displaces oxygen. This combined process inhibits the combustion process and lowers the temperature below the reignition point. When the liquid nitrogen and solid carbon dioxide are converted to gases, the expanding gas acts like a piston, forcing warm air out of the porous bed, Although smoke and hot gases arc forced from the burning coal, generally there is no significant increase in the odor associated with burning coal.

Jan 1, 1992

By Yap Chu-Phay

IN the previous paper, the writer showed how, on the basis of thermodynamic reasoning, it seems probable that when true equilibrium conditions obtain, carbon exists as Fe3C in the liquid state and as elementary carbon in the solid state (7 Fe), in which case the solidus would be a straight line from 0.18 to 1.70 per cent. carbon (Fig. 1). In the same paper he concluded that the solidus obtained by Honda 'and his co-workers1 probably does not represent the same conditions, insuring a complete equilibrium. Except for a downward temperature displacement, the solidus obtained by Gutowsky,2 using the Heycock and Neville method, practically coincides with Honda's solidus as shown in Fig. 1. The writer at first thought that perhaps in some way Gutowsky's thermocouple was improperly calibrated for high-temperature measurements, as his liquidus was also much lower than those obtained by Carpenter and Keeling3 and by Ruer and Goerens.4 However, the eutectic temperature obtained by Gutowsky agrees with the generally accepted value of 1130° C., so that the validity of the inference regarding improper temperature calibrations is to be strongly doubted. In Fig. 1, Gutowsky's solidus is shown both in the original and in the corrected form. In the latter, a correction of 29.2° C. is made for all temperatures above 1416° C. in accordance with-

Jan 1, 1931

By J de Cuyper, S. R. Rao, J. Leja, K. S. Moon, W. Freyberger

A prolonged grinding of sulphide ores in steel mills appears harmful to flotation recovery and selectivity whenever xanthates are used as collectors. Particles finer than about 10um show a pronounced decrease in floatability. A supposition was made that the cause of the reduction in floatability of ground sulphides is the presence of metallic iron abraded during grinding and deposited on the ground particles. Electro- chemical measurements were made of mixed potentials developed by different sulphide-mineral electrodes (galena, chalcopyrite, pyrite, marmatite, pyrrhotite) in xanthate solutions, without a direct con- tact or in contact with a metallic iron electrode. These measurements showed that without a galvanic contact between the sulphide and the iron, the values of mixed potentials were in the vicinity of the xanthate/dixanthogen redax potential. When contact with iron was established, the mixed potentials shifted towards the more negative reducing or cathodic values, The shift was greater the higher was the ratio of the surface areas: iron electrode to sulphide electrode. Further, the shift in mixed potentials was greater the more reducing were the conditions on the sulphide electrode. Chemical analysis of reaction products produced on the surfaces of sulphides and in the bulk solution showed that less thiosulphate was formed in all of the sulphide-xanthate systems and that more elemental sulphur was detect-

Jan 1, 1976

By A. Chryss

Tailings management aims to dispose of tailings at the minimum cost consistent with meeting or exceeding imposed standards, including legislative obligations. This simple business objective requires managing the tailings storage facility (TSF) risks associated with surface water, groundwater, dust, sustainable closure, and potential catastrophic failure. The individual nature of every orebody and specific site topography ensures that no one size fits all. It has been suggested that paste and thickened tailings (P&TT) provides the ability to tailor the production and transportation of tailings to suit the deposition site, rather than the traditional approach of accepting that the deposition site has to accommodate tailings of high variability. While the traditional approach can be made to work, it is directly linked to the catastrophic failures of tailings impoundments, where large volumes of decant water have triggered failures due to overtopping, piping or slope instability, or saturated tailings have simply liquefied. P&TT offers an ability to mitigate these risks, and when implemented into new projects with variable tailings streams there are significant benefits to be realized. This paper identifies the interdependencies between the various tailings disposal processes, such as thickening, pumping, and deposition. It demonstrates that there are benefits in taking a more integrated approach to the design and operation of tailings disposal facilities. A collaborative industry project to tackle this challenge is described.

Jan 1, 2012

By W J. Shaw

Geometallurgical modelling is now a hot topic in deposit evaluation and in optimising mine performance; however, its history is long and varied. Historically metallurgical sampling has frequently suffered from a lack of data due to the cost of producing representative bulk samples. In the early 1990s geometallurgical modelling similarly suffered from a lack of data due to complex, time consuming and expensive sampling techniques. More recently, simple and relatively cheap tests for geometallurgical variables such as hardness, grindability, throughput, SAG power index, bond work index, crushing index, mineral recovery and concentrate grade have become widespread. The cheaper sampling has resulted in relatively large geometallurgical databases. However, most of the geometallurgical variables sampled are implicitly (and incorrectly) assumed to be additive when modelled by traditional geostatistical techniques, often leading to ill-informed and costly decisions. Geometallurgical variables are mostly non-additive so the current geostatistical challenge is to develop new approaches to dealing with this type of data. This paper briefly describes a historical case study of geometallurgical modelling of the George Fisher Pb-Zn mine completed in the mid 1990s, then outlines some of the current misconceptions of geometallurgical data and modelling techniques regularly applied to it, and finally discusses some recent developments in geometallurgical modelling, with examples from a number of current clients indicating the direction forward.

Jan 1, 2009

By G. M. Wilemon, B. J. Scheiner

The Bureau of Mines conducted investigations on extracting phosphate values from fine-particle wastes generated during the mining and beneficiation of phosphate ore by leaching dried wastes using a H2SO4-methanol mixture. Although phosphatic clay waste contains up to a third of the phosphate originally present in the ore, recovery of these values represents a significant challenge due to the fine grain size of the material, the particles averaging less than one micrometer in diameter. Waste samples obtained from two Florida producers yielded phosphate extractions of 71 and 84 pct, respectively, when leached under ambient conditions and at a stoichiometric acid ratio of 1.4:l. Elevated temperatures did not improve the amount of phosphate extracted. Undesirable A12O3, Fe2O3, and PlgO impurities were largely rejected; higher grade wastes gave acids that meet established industry impurity standards and lower grade samples yielded acids that marginally fell short of the standard. Separation of the crude acids from the insoluble residues was accomplished via vacuum filtration through either filter paper or commercial filter cloths. Both filtration rates and solids retention were improved by the addition of 0.5 lb/ton of poly(viny1 acetate) (PVAc) or poly(ethy1ene oxide) (PEO) to the methanol-acid slurries. These results show potential for substantially increasing the reserves of an important domestic resource.

Jan 1, 1989

By A K. Raina, P B. Chourdhury

Flyrock is the unwanted throw of rock fragments to excessive distances in opencast blasting. The incidence is relative in nature incorporating the distance of objects of concern like structures within and outside the mine, equipment within the mine & near the blast and persons within and off the mine. Several attempts to predict and defi ne fl yrock made worldwide could not address the problem since the phenomenon is not a regular feature in blasting. This probabilistic nature of fl yrock allows for risk calculation. CIMFR, India developed a Factor of Safety based risk criterion (10, 14) for evaluation of throw/ fl yrock in opencast mines that incorporates all the above in terms of distance and allowable limit of throw – which in turn determines the risk. The criterion provides the blaster a tool for mathematical evaluation of fl yrock risk in terms of a Factor of Safety and threat ratio (defi ned for the 1st time), thereby enhancing confidence when blasting. The method is easy to use and has been applied to several mines in India and the results are signifi cant. This paper details the evolution of the concept and its application in three limestone mines of India and the results obtained. The application of the method for defi ning a fl exible danger zone is also discussed.

Jan 1, 2008

Reduce the cost and incidence of low-back pain in underground coal mines through redesign of materials-handling tasks. Background Approximately 25 pct of all injuries in mining involve trauma to the hack. These injuries account for at least 30-40 pct of worker compensation payments made by the industry, are the leading cause of lost work days in mining, and have been estimated to cost the industry $50 million annually. It is clear that the traditional approach to reduce back injuries (i.e., training) has been largely ineffective. Thus, new approaches are necessary to control this problem. This document briefly describes methods that can be used to redesign hazardous materials-handling tasks to reduce the threat of worker injury. Approach A model for redesigning materials-handling tasks is shown in figure 1. The model outlines the sequence of steps that should be followed (and questions that should be asked) when developing new strategies for handling materials in underground coal mines. A critical examination of the current supply-handling system is the first step to developing safer materials-handling procedures. The purpose is to identify hazardous tasks that can be modified to reduce injury risk. Accident analysis (a review of past accident records) and task analy¬sis (usually a videotaped analysis of hazardous jobs or tasks) arc effective methods of distinguishing areas where job redesign is needed.

Jan 1, 1992

By Andrzej Luszczkiewicz, Magdalena Duchnowska, Jan Drzymala

A selected flotation system of beneficiation of the copper ore at KGHM Polska Miedz S.A. has been analyzed in the article. It was found that a proper assessment of upgrading must be based on two elements, that is the upgrading process selectivity and working point of the considered flotation unit, both determined, preferentially by means of the Fuerstenau recovery-recovery upgrading curve. The Cu recovery - non-Cu components recovery upgrading curve was selected for calculations because its background lines (no separation and ideal separation) are insensitive to changes in the grade of feed of the processed material. This approach allows a comparison of upgrading results for feeds having different grade, being upgraded in various flotation machines and under different physicochemical conditions. It was shown in the paper that the main criterion for comparison of two working in parallel systems is selectivity of upgrading. However, when two flotation machines, despite of the same selectivity, produce concentrate and tailing of different grades, it is necessary to analyze their working points using upgrading curves. The proper position of the working point depends on the criterion imposed on the process and is a result of not only basic parameters of the upgrading process such as feed, concentrate and tailing grades but also on economic parameters such as costs associated with the production of concentrates and the time needed for their production.

Jan 1, 2014

Provide a portable crushing capability to keep conveyor haulage close to the working face and permit more efficient and safer ore handling in low headroom, hardrock mines. Approach A readily portable jaw crusher is used which meets machine size, feed rock size, product size, and throughput requirements for low headroom, hardrock mines. How It Works The crusher is mounted on wheels to expedite frequent moves and to allow crushing of mined rock or ore near the working face. The crushed product is then placed on conveyor belts that are ex-tended as the crusher is moved. Keeping crushing and conveyor haulage near the face minimizes the haulage distances for trucks and loaders. Loading and haulage of run-of-mine ore is frequently the highest operational cost in underground mines. These costs can be significantly reduced by use of a belt conveyor, which is a common practice in coal and other soft mineral mines. The new low-profile hard rock crusher gives the same advantage of extensive belt haulage capabilities to low headroom, hardrock mines. The low-profile crusher will accept feed up to 30 inches when operating under 11 feet of headroom. The headroom required for crusher operation was reduced by tilting the jaws, feeding the crusher horizontally, and placing the eccentric shaft at the back or in a horizontal plane with the jaws. Material is fed by an

Jan 1, 1981

By G Giles

One of the main tools used by mining operations to mitigate the risk of rock burst is the installation of a so-called ædynamic resistantÆ support system. Such systems are designed to absorb the impact of shockwaves created by mine-induced seismic events. Dynamic support must be strong and capable of sustaining high loads and, at the same time, they have to be flexible and accommodate large deformation. A dynamic support system is therefore a system capable of absorbing a high quantity of energy. Ground support systems are composed of rock reinforcement (rock bolts or cable bolts) and surface support (mesh or shotcrete). In terms of surface support, fibre-reinforced shotcrete is increasingly seen as the industry preferred solution when difficult ground conditions are experienced, including areas of high seismic hazard. A thick layer of shotcrete is certainly strong but it is by no means flexible. Normal weld-mesh has some flexibility, but it is not very strong. The Australian Centre for Geomechanics (ACG), in collaboration with Onesteel Reinforcing Pty Ltd, is currently working on a new high-energy absorption mesh that combines strength and flexibility. The new mesh can be installed with a jumbo, in a similar way as the widely used sheet of weld-mesh. This paper describes the development of this new mesh system.

Jan 1, 2008

By Paul Tyler

THE extensive employment of nonmetallic minerals antedates the use of metals, but only within the last two decades has the production of nonmetals begun actually to keep pace with the complicated activities which characterize the so-called Machine Age. The economic changes ushered in by the Industrial Revolution were reflected first in an increased demand for metals and for fuels. In the modern sense, therefore, the nonmetallic mineral industries are new and afford new opportunities for engineer and economist alike. A certain amount of caution is indicated, therefore, before attempting to apply ready-made formulas to the problems of these industries. Economics is not an exact science. In the field of production technology where the number of variables is fairly well known, the principles of economics are readily applicable, but as the student proceeds through the province of marketing into the unexplored regions of psychology and sociology he must distinguish carefully between scientific reasoning and purely metaphysical speculation, even when the latter masquerades as economics. The present paper attempts to prove no preconceived theorems and is designed primarily to stimulate careful thinking on sundry neglected phases of these industries. An attempt is made to differentiate the general problems into single aspects which afford promise of being comprehended separately; also, some fundamental statistical data are presented, but merely to indicate a method of scientific approach applicable to more intensive studies.

Jan 1, 1933

By Joseph C. Zelanko, Anthony T. Iannacchione

One of the most difficult and longstanding engineering problems associated with coal mining is the catastrophic failure phenomenon known as coal mine bursts (known in the United States as bumps). For more than 70 years, researchers and practitioners have attempted to determine whether this destruction observed underground is caused by stress conditions within the coal pillar or from distant seismic sources in the mine roof and floor strata. The role of confinement and the extent of failure in solid pillars and panels have also proven difficult to define. These are important issues, since control solutions need to be based on a fundamental understanding of the problem. Obsenations by U.S. Bureau of Mines researchers over the last decade have helped to clarify certain aspects of these issues. Microseismic sensors and geomechanic field measurements have located areas of excess energy release, identified stress conditions in coalbeds close to failure, and recorded the response of mine structures prone to bursts. In the present study, data available for a range of U.S. bursts were considered in an effort to evaluate both common and distinctive features. Although the attempt revealed little commonality, encouraging results were produced by categorizing coal bursts by source mechanisms. When a coal burst is thus categorized, differences in environmental factors-such as geology, stress fields, and mining methods-are highlighted, and viable control strategies are readily recognized.

By Mills KW

Coal mine pillar design formulae available to mine planners are typically based on relationships determined for specific site conditions. Application of these methods is difficult when other factors, relating to mining or geological conditions, not specifically addressed in these relationships are encountered. A review of pillar design methods, coal strength properties and relevant field monitoring of pillar behaviour has shown pillar strength and deformational characteristics are extremely sensitive to in situ behaviour of the rock and other material components that make up the coal pillar system. A method has been developed that has been found to provide excellent correlation between existing field data using the strength and deformational characteristics of materials determined in selected laboratory tests. This method is based on definition of the loading conditions, accurate modelling of the strength, confining conditions and deformation occuring in the roof, floor and coal seam and definition of the in situ strength of coal based on underground monitoring of appropriately sized coal pillar. The design method is considered to provide an accurate and rigorous pillar design method that will give mine planners a more rational mine design capability which is based on the mine geometry and geological setting of the operation. It is envisaged that availability of such a method will allow significant optimisation of pillar layouts and more closely define the geological and mining issues that relate to pillar design optimisation.

Jan 1, 1992

By L. B. Slichter

After statement of the principles of similitude which apply to electromagnetic modeling, charts showing the inductive response of conducting spheres as dependent upon frequency, conductivity, and size are exhibited in this paper. The shape of the curve which relates intensity of response to frequency is significant in indicating the advisability of low frequencies in the exploration for conducting bodies, when consistent with the securing of a large percentage of the ideally possible response. Comparisons of theoretical response and that observed with models are shown, and relationships with the subject of applied electromagnetic prospecting are indicated. Maxwell Field Equations The Maxwell field equations summarize the physical laws that govern electrical field phenomena; they are the basis for the solution of electromagnetic problems. These concise equations, with adequately formulated boundary conditions, specify the complete electrical condition of continuous media, and the development of their solution amounts merely to a more convenient re-expression of phenomena already completely described. Thus, the immediate content of the field equations themselves is sufficient and sometimes convenient for the treating of certain questions (such as those relating to electromagnetic models) which are independent of the special factors of geometry, or the nature of an impressed field. The four Maxwell field equations are written below, in c.g.s. gaussian units: curl E = -B/c [21 div eE = 4pp [31 div B = 0 [41

Jan 1, 1932

By Raja V. Ramani, Wilson Miola

The potential health effects of quartz-bearing airborne dust in mine and mill atmospheres point to the need for the quantification of quartz content in the source material for determining the source-sink relationships and for choosing applicable control measures. While a standard method exists from a regulatory point of view for the sampling of coal mine atmospheres for determining (i) respirable dust concentrations and (i) the amount of quartz in thesamples, there is no generally accepted standard method for quartz analysis in bulk samples of coal and host rocks. Generally, the bulk sample is reduced to a powder for producing quartz analysis samples. Extensive controls are necessary to ensure representativeness of the analysis samples when these are very minute fractions of the bulk samples. Since the amount of analysis sample is not limited, alternative methods for quartz analysis may also be tried. It is, however, necessary to adopt a procedure which will satisfy several statistical requirements to guarantee representativeness of the quartz analysis samples. In this paper, the important factors in the preparation of quartz analysis samples from the host rocks and bulk samples are discussed. The method developed to prepare the analysis samples is outlined. The results of application of the procedures are presented. The procedure developed for quartz analysis sample preparation is based on sound statistical foundations. The procedure has been validated for reproducibility and homogeneity.

Jan 1, 1991

Minimize the effects of underground mine conveyor belt fires by developing methods to prevent automatic fire suppression system failures. The Problem Fire protection is achieved by prevention, early detection, and planned fire-fighting response. Automatic fire suppression systems are one form of planned fire-fighting response. When these systems are properly designed, installed, and maintained they can effectively control fires. Conveyor belt fires account for about 20% of underground coal mine fires. Fire protection requirements have been established for underground locations because of potential for start and spread of fire and the restricted personnel egress in a fire situation. Belt conveyor systems arc potentially dangerous because of the high fire incidence rate, high temperatures, dense smoke, toxic gases, and rapid flame-spread rate. While investigating the conveyor fire suppression problem, the Bureau identified automatic fire suppression system reliability as a potentially serious deficiency within the mining industry. Table 1 lists common failure modes fur three Fire suppression system types. This table summarizes findings of Mine Safety and Health Administration electrical inspectors responsible for inspection of belt protection automatic fire suppression systems. Batteries, contact points, control wires, and electric servocontrols are all prone to failure. Figure 1 shows rock-dust-contaminated relay contact points. This condition is dangerous because of the chance of intermittent failures, which might allow systems to pass annual functional testing, yet fail during actual fire emergencies.

Jan 1, 1989