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By Benjamin W. Haynes

Analytical procedures are described for the quantitative determination of 16 elements (As, Ba, Be, Cd, Co, Cr, Cu, Fe, Mn, Mo, Ni, Pb, Sb, Se, TI, and Zn) and 7 ionic species (NH4, C032-, CI-, F-, NO3-, P043-, SO42-), identification of major and minor mineral components, and measurement of physical properties associated with manganese nodules and nodule processing reject waste materials. Compound identification methods discussed include X-ray diffraction, infrared spectroscopy, scanning and transmission electron microscopy, selective area electron diffraction, and optical and reflected light microscopy. Methods for elemental analysis include atomic absorption spectrophotometry, inductively coupled plasma emission spectroscopy, neutron activation analysis, fluorescent X-ray spectrography, and ion chromatography. Thermal gravimetric analysis, ultraviolet-visible spectrophotometry, ion specific electrodes, and standard wet chemical procedures are briefly discussed. Physical properties determined in manganese nodule materials include grain size distribution, specific gravity, triaxial shear, permeability, maximum density, Atterberg limits, and slurry density. The results of a round-robin analysis of an ammonia process waste material and manganese nodule standards demonstrate the applicability of the discussed methods. Tests discussed for the evaluation of the waste materials for disposal options include the Environmental Protection Agency (EPA) EP toxicity test, the ASTM shake extraction test, and the U.S. Army Corps of Engineers EPA seawater elutriant test.

Jan 1, 1983

By Harrison R. Cooper

Approximately 40 concentrators throughout the world have successfully adopted computer control for flotation circuit operation since 1969. Successful use of flotation control, gaining up to 2% efficiencies, has largely derived from effective employment of on-stream slurry analyzers and integration of key measurement data through digital processors. Requirements for reliable measurement have also led to improved functional reliability in magnetic flow meters, pH, reagent feed, and other key elements. Methods used in computer control of flotation will be reviewed and variations in operating philosophies will be described with reference to the approaches taken to flotation automation.

Jan 1, 1979

By Owen Matthews

Introduction For the past year and a half, the mill of Cochenour Willans Gold Mines, Limited, McKenzie Island, Ontario has been roasting arsenopyrite-gold concentrates, prior to cyanidation, by means of a roaster employing techniques that are new and novel. The roaster is known as the Dorrco 'fluo-solids reactor', and the technique as 'fluidization'. The reactor has demonstrated its ability to roast a flotation concentrate containing arsenopyrite, pyrite, stibnite, small quantities of other sulphides, and some lime silicates and carbonates, yielding a calcine consisting mainly of porous iron oxide, plus the gold values. This calcine is readily amenable to cyanidation. Bulk shipments of concentrates to a distant custom smelter, as practised prior to this installation, has thus been eliminated, with appreciable savings in smelting charges, freight costs, and interest losses during shipment and smelting. This is the pioneer installation of fluo-solids roasting at a Canadian mill and up to the present performance results have not been published. It is the purpose of this paper to present the information now available for the benefit of other millmen who may be confronted with identical or similar problems to those encountered and solved at Cochenour Willans.

Jan 1, 1949

By N Guresin, A Cooper, L Lorenzen, H Muller, S C. Dominy

Sampling and metallurgical test work during various phases of engineering?studies?is of?paramount importance for a robust processing plant design. When developing a process flow sheet, risks in achieving desirable financial outcomes are minimised by ensuring appropriate sampling and adequate metallurgical test work supports the engineering and cost estimation at each phase of project development.The quality and type of samples used for metallurgical test work are just as important as the metallurgical test work itself. The key characteristic required of any sample is that it represents some defined portion of a mineral deposit. Representivity should take into account the spatial orientation, lithology, alteration, degree of oxidation, mineralogy and competency of the ore such as hardness and abrasiveness. Statistically representative sampling procedures and an appropriate metallurgical test work program should be designed to bring metallurgical understanding up to feasibility study standard and to give a basis for process plant design.Snowden has observed that the quality of sampling and quantity of metallurgical test work carried out during the various phases of engineering studies are often insufficient to truly support a robust plant design. Some designs are often the result of the plant design based on benchmarks of apparently similar orebodies or buoyant metal prices supporting cash flows until rectifications can be implemented.The paper will discuss important aspects of sampling and test work required for engineering studies in designing process plants based on industrial case studies.CITATION:Guresin, N, Lorenzen, L, Dominy, S C, Muller, H and Cooper, A, 2012. Importance of effective sampling and test work protocols for process plant design, in Proceedings Sampling 2012 , pp 95-108 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By C. S. Ek

As a continuation of previous work, further tests have been carried out to recover silver from the residues obtained in a zinc jarosite process. Selective flotation has been performed with different reagents, and ?cleaning steps have been introduced to upgrade the silver concentrate. Leaching of crude residues, as well as flotation tailings, has been carried out with cyanide and thiourea. Finally, the different beneficiation methods are compared, and the industrial aspects? of their application are reviewed.

Jan 1, 1990

By James D. Hall

THE Dome ore-bodies are more or less isolated and are mined. by shrinkage stoping. An interwoven system of veins is mined at Hollinger '.1.nd requires close filling. Deep mining is the problem at McIntyre. Dome ore contains a large amount of free gold, which is recovered on blankets. An all-cyanide flow-sheet is \lSed in the Hollinger mill. Flotation concentration is an important feature of McIntyre mill operation. Therefore, these three mines afford an unusual opportunity to compare gold mining and milling methods. The purpose of this paper is to describe the conditions existing at the Dome, Hollinger, and McIntyre mines and to outline the mining and milling practice at each property. Figures 3, 4, 5, and 7 are reproduced from the Canadian Mining ]011rna/, September, 1935 (Young, A. W., Mining at Hollinger), and Figures 8 to 11 from the Engineering and Mining Journal, November, 1933 (Keeley, D. E., Development and Mining at McIntyre). The photographs (Figures 6, 12, and 13) are by The Canadian Government Motion Picture Bureau. Diagrams of the several mill flow-sheets, which formed a part of the original paper, are not reproduced here. They will be found in Dorr's Cyanidation and Concentration of Gold and Silver Ores.

Jan 1, 1938

As the high-grade copper deposits in the world become depleted, there is an increasing focus on developing lower-grade ores which contain problematic impurities such as arsenic. Indeed, many high-arsenic ore bodies remain undeveloped because of their high arsenic levels. Separation of arsenic from copper at the beneficiation stage is difficult using the current processing techniques and invariably copper concentrates produced from these ores contain high arsenic levels, sometimes so high as to make them unacceptable to copper smelters. New, sustainable approaches are needed to allow development of high-arsenic copper ores while at the same time minimizing arsenic dispersion into the biosphere. The most promising route for separating arsenic from copper at the flotation stage centers on the use of pulp potential control. In recent years CSIRO has demonstrated at laboratory scale, for a number of high-arsenic copper ores, that crude flotation separation between arsenic-bearing minerals and copper-bearing minerals can be made. The differences in specific minerals responses to changes in pulp potential and pulp pH are exploited for this separation. Such separations nominally produce a low-arsenic high-copper concentrate and a low-copper high-arsenic concentrate. The former can be smelted without penalty, while the latter requires further treatment to capture and stabilize the arsenic and to recover the residual copper. Consideration has now been given to treatment options for the high-arsenic low-copper product. A pyrometallurgical option, involving a low temperature roast to selectively fume off the arsenic and leave a high-copper calcine, coupled with an arsenic stabilization step, has been demonstrated in the laboratory, and a preliminary techno-economic evaluation shows the process to be economically favorable. These results were recently published. CSIRO has now investigated an alternate hydrometallurgical option, involving atmospheric alkaline sulphide leaching of the high-arsenic product, where the arsenic is selectively dissolved leaving a copper-rich leach residue. The leaching testwork was carried at on the same high-arsenic low-copper material used in the roasting studies, enabling a techno-economic comparison of the alternate roasting and leaching treatment options to be made. The alkaline leaching work is briefly described and the results of the process option comparison presented and discussed. Keywords: arsenic, copper, economics, enargite, ore flotation, tennantite INTRODUCTION

Sep 1, 2012

By J. V. Thompson

The Powderhorn complex as a source of perovskite (calcium titanate) containing about 1.5% rare earths has been examined in several recent feasibility studies. Much promising exploration and process research has been done in recent years. This paper is presented with cautious optimism and with the acknowledgment that there may be some technical and economic areas yet to be explored. The Powderhorn carbonatite and alkalic stock in Gunnison County, Colorado, lies about 203 airlines km southwest of Denver at an elevation of 2450 to 2750 m (see Figures land 2). All of the mineable ore bodies are owned by Buttes Resources Company of Houston, Texas.

Jan 1, 1990

"Canada Centre for Mineral and Energy Technology (CANMET)Natural Resources CanadaMining and Mineral Sciences LaboratoriesA. Address and Contact Information555 Booth StreetOttawa, Ontario, Canada, KIA OGlWebsite: http://www.nrcan.gc.ca/Contact: Philippe Dauphin, Manager, Business DevelopmentTel.: (613) 947-0798Fax: (613) 947-0984E-mail: pdauphin@NRCan.gc.caB. Type and Size of FacilityScope of facilitiesCrushing from minus 4 in. to 10 mesh; grinding - rod, ball, vibration, SAG and impact mills; classification- screening, cycloning, mechanical, hydraulic and dry centrifugal classifiers; froth flotation - automated, column, and frothless flotation; gravity separation- wet and dry; magnetic separation - high gradient, high and low intensity, wet and dry; electrostatic separation; heavy-media separation; calcining; cyanidation; thickening; filtration; drying - fluid bed and freeze drying; pelletizing; microwave.SpecialtiesMineral beneficiation research and development; flotation of sulphides - flowsheet improvement, selectivity, reagent selection; novel flotation techniques; analysis of thiosalts formation; use of mineral processing techniques for recycling.Specialized equipmentHigh gradient magnetic separation, Denver XRF on-stream analyzer, automated flotation cell.Complementary support servicesElectron microprobe; SEM; STEM; X-ray diffraction; particle size analyzer; mineralogical and analytical chemistry services; physical chemistry; hydrometallurgy; pyrometallurgy; engineering and economic evaluation; mechanical shops; technical information services and library integrated with the National Library System of the National Research Council."

Jan 1, 2000

By Brian Raymond

This paper will outline the problems and solutions of the new generation washeries, as well as the recent technological advances which are being considered for future coal preparation plants. The subjects to be covered will include: - reasons for considering coal preparation plants; - raw coal crushing and handling systems; - types of coal cleaning equipment being used versus new equipment being considered; - fine coal circuit sizing; - clean coal centrifuging and dewatering; - thermal dryer problems and changes; - fine refuse dewatering systems; - clean coal storage problems and changes; - materials handling within the plants; and - control systems for preparation plants. The design and integration of the various circuits that form a modern coal preparation plant have led to the creation of an exciting new field of industrial research. As the need for energy sources increases, efficient methods of preparing coals for specific markets will become more important.

Jan 1, 1979

By Wei Sun, Ruolin Wang, Jianjun Wang, Xiaodong Li, Honghu Tang, Yuehua Hu, Anh V. Nguyen, Haisheng Han, Kefeng Chen, Zhao Wei

It is difficult to separate scheelite especially from fluorite with fatty acid collectors because the adsorption mechanism of these collectors occurs through chemisorption of the oleate ion onto the mineral surface. A simplified flotation process using Pb-BHA complexes was developed to replace the energy-inefficient Petrov’s process of using a fatty acid, increasing the recovery of scheelite and reducing the cost. The relationship between surface chemical properties (crystal chemistry, solubility, and Zeta potential) of minerals and flotation by using a fatty acid or Pb-BHA complexes was studied in detail to provide new insights into the selective separation mechanism. The results indicate that the scheelite surface exposes more O atoms than Ca and that they are negatively charged due to the anisometric dissolution of Ca and WO4, which provides the possibility for separation using selective interfacial reaction. The FTIR and Zeta potential results indicate that both chemical and electrostatic adsorption play an important role in the adsorption of Pb-BHA complexes on the scheelite surface. The XPS results of the atomic composition and binding energies confirmed the presence of the adsorbed Pb-BHA complexes and that O and Ca may be the active adsorption sites. Therefore, scheelite was able to be collected by forming either a Ca-O-Pbcollector or W-O-Pb-collector (BHA). However, fluorite was only able to be collected by a fatty acid collector and colloidal [H2SiO3]n -, and a high temperature was needed improve the selective desorption of the adsorbed fatty acid collector by forming Ca-[H2SiO3]n - on the fluorite surface, resulting in serious problems in industry. However, the Pb-BHA complexes significantly contribute to improving the recovery of scheelite minerals, simplifying the flotation process, and circulation of the residual reagents and water. The new process has been applied in Shizhuyuan Mine, and improved the recovery by almost 10%.

Jan 1, 2018

By John Hillman

The reconstruction of the British mining industry which began shortly after nationalisation in 1947 continued until well into the 1950s with the support of the Government. This support diminished as plentiful supplies of cheap oil from the middle East made many coalmines un¬economic. The planned rundown which followed was foreshadowed in the 1965 White Paper which outlined the financial measures to speed the closure of uneconomic collieries. The decline appeared likely to continue into the 21st century as the role of coal in UK energy requirements became less and less significant. This policy was well on course in 1973 when the oil crisis led to a complete reappraisal of the position. A Government examination in 1974 of the coal industry then supported the National Coal Board's general strategy of major capital investment as set out in its 'Plan for Coal' (1). Plan for Coal aimed at halting the intended decline in the industry's capacity and restoring it to 120 million tons of deep mined output in 1985. The Plan proposed action along the following lines (a) increase output by major Investment in construction at existing collieries with sufficient reserves to give 13 million tons per annum extra output (b) invest in extending the life of existing collieries by gaining access to additional reserves, to give 12 million tons per annum extra output © by sinking new mines, produce an extra 20 million tons per annum. Figure 1 shows the contribution (2) expected from each of the three sources up to 1990/1. The measures taken were expected to offset the inevitable exhaustion of existing pits and provide the additional 40-42 million tons capacity needed to restore annual output in 1985 to 120 million tons. Parallel to this programme for expansion of deep mined output, opencast mining was to produce 10-15 million tons per annum. A recent review however, indicates that new mines are likely to yield only 10 million tons per annum by 1985, mainly owing to the need for public inquiries into proposals for new mining and the resultant fact that planning approval takes 'much longer than originally expected. Nevertheless the objective of 120 million tons deep mined output by 1985 is still considered achievable of means of a greater contribution from existing mines. This programme was originally estimated to cost 2,-56 million dollars at March 1974 prices, out revised estimates of the cost of Plan for Coal indicate that it may now exceed 6,960 million dollars at mid-1977 prices. Plan for Coal includes a substantial investment in new and reconstructed coal preparation plaints. At mid-1977 prices more than 322 million dollars Ls so be invested in coal preparation projects in the UK, at the rate of, about 70 million dollars a year. This rate 3f capital expenditure has been maintained over the past three years and covers investment in a wide range of coal preparation coals for the power station, coking and domestic markets.

Jan 1, 1978

By Ray Holmes

This paper describes one approach in our search for greater stope efficiency and lower costs. The uppers technique with wagon drills in cut-and-fill stopes was commenced, on an experimental basis, in our Sudbury mines in 1961. To date, the method has developed into an accept-ed production operation. This technique minimizes the intermittent aspects of the drilling, blasting, mucking and filling operations associated with other cut-and-fill methods. However, studies show that not all cut-and-fill stopes are suitable for uppers, the governing factors being ore width, dip of the orebody, and ground conditions where large areas of unsupported back remain stable for ex-tended periods of time until rockbolting can be accomplished. Introduction F ALCONBRIDGE Nickel Mines Limited operates seven mines within a radius of 30 miles of the city of Sudbury, Ontario. These mines extend in depth from 1,500 to 6,300 ft. The ore consists of brecciated, massive and disseminated sulphides, and the ore minerals consist primarily of pentlandite, pyrrhotite and chalcopyrite. Widths are generally irregular and vary up to 150 ft. The ore dips at between 35 and 90 degrees.

Jan 1, 1965

By David Sutherland

The treatment of a complex orebody requires a thorough understanding of its mineralogy. If there is a poor appreciation of the mineralogy involved, difficulties can emerge with the efficient exploitation of the resource. Recently, there has been a lot of interest in automated image analysis systems, which aim to improve the reliability and accuracy of the data, which can be gathered. In this sense, the paper point out the process mineraloggy for complex ores. Mineral modal analysis a description of texture and liberation studies are the basis of these measurements. They have been applied to a wide range of mineral systems including copper, lead, zinc, silver and gold.

Sep 13, 2001

By W. M. G. Heeley

In the province of Alberta the coal measures dip at so many different angles, between the horizontal and the vertical, that many different systems of haulage are in use. I will, however, only touch briefly upon the general -systems in use, and devote the major portion of this paper to a discussion of endless-rope haulage and its adaptibility to various conditions in coal mines; dealing in particular with the endless-rope haulage that was installed at Brule during the month of August 1923. In coal seams that are approximately level, and newly opened, hand-putting or tramming from the face is the cheapest, but when the mine is further developed tramming is out of the question, and the use of ponies is the next consideration. The time arrives, however, when mining reaches a point where the economical haulage of coal by horses cannot be done profitably, and then some system of mechanical haulage must be installed. The installation of any system should be carefully considered before any particular type of haulage is adopted, because a great deal depends upon the grade or dip of the seam. Motor haulage is impossible to operate profitably on a grade of over 6 per cent and, while it is possible to use ponies, on short runs, up to 9 per cent, some other means of main and secondary haulage must be installed when a 9 per cent grade, is exceeded. I will, therefore, deal first with secondary haulage, because even though a main haulage is established, secondary haulage can be used to feed the main haulage.

Jan 1, 1925

By D. C. Dahlin

The Bureau of Mines investigated the Ketchem Dome tin prospect in east-central Alaska to evaluate the tin resource. The studies included field investigations, mineralogical characterization, and concentration of the tin-bearing minerals. The tin mineralization consists of cassiterite (Sn02), which occurs as grains disseminated in a greisen (quartz-mica) matrixo A bulk sample from the largest and best-developed greisen vein exposed at Ketchem Dome contained 0.51 pct Sn. Concentration of the cassiterite by gravity table methods resulted in a product that contained 56 pct of the tin at a grade of 41.4 pct Sn. The mineralization exposed at Ketchem Dome is typical of greisen found in the area and elsewhere in interior Alaska.

Jan 1, 1987

By George A. Komadina

From its modest beginning in 1957 with one mill grinding section handling 3000 tpd Pima has steadily expanded. In July 1966, work was completed that allowed the concentrator to treat in excess of 18,000 tpd. Almost immediately Pima embarked on another expansion program that will increase plant capacity to 30,000 tpd during the summer of 1967. This repeated expansion has corresponded with the development of additional low-grade ore deposits and with the improved operating economics realized by handling larger masses of material. Early in the life of Pima it was known that a mineralized area was present on the flanks of the high-grade orebody which systematic drilling had shown to be a low-grade copper orebody. Many months of engineering studies revealed that this was sufficient to allow Pima to compete with other large scale, low-grade copper operations in the Southwest.

Jan 11, 1967

By H. M. Breza

Recovery of phosphate concentrate has received increased attention as the existing mine and plant production capacity limitations of the Texasgulf Inc. Aurora, North Carolina Mine are reached. Improved mining techniques and mineral processing of waste streams offer a potential to increase overall phosphate production without major expansion of the Mining facility. Innovative processes have been or are being identified to maximize pit mining recovery and to minimize losses in waste streams, resulting in more effective use of the valuable phosphate natural resource. This paper will describe the various continuous recovery improvement programs being implemented to achieve this goal.

Jan 1, 1994

By V. A. Ignatkina, V. A. Bocharov, T. I. Yushina, I. M. Petrov, A. A. Kayumov

"The purpose of this research was aimed at increasing recovery of metals from rebellious sulfide polymetallic ores of nonferrous and rare metal deposits. The ores under consideration have common processing features, including textural and structural complex characteristics, irregularity of impregnation and wide range of grain size, up to nanoparticle size, variable complex mineral composition, low content of precious metals etc. This all predetermines the need for advanced processing schemes with deep selective liberation and separation of minerals with intercycle release into rough concentrate and fractional products with the use of multi-stage cycles of individual dressing, based on an optimum combination of various integrated beneficiation and hydrometallurgical processes. The application of existing standard processes does not enable the production of high-grade selective concentrates without reducing the recovery rate due to incomplete separation of fine mineral intergrowths and overgrinding of brittle ore and rock minerals.The combined beneficiation processes for such type of resources, aimed at increasing recovery of nonferrous, rare, and precious metals are based on flotation methods in combination with gravity concentration to produce rich rough collective or selective concentrates, comprising readily floatable mineral fractions. At the same time, hardly recoverable and non-separable mineral associations are released into separate concentrated products for following dressing by individual processes. The proposed combined process provides for successive selective liberation of minerals with release of rich readily recoverable mineral fractions at the preparation and ore beneficiation stages. The hardly recoverable mineral associations shall be released in subsequent operations with the use of dressing, based on a combination of beneficiation and pyro- and hydrometallurgical methods."

Jan 1, 2018

By W. D. Eddy

Topaz is a fluorine-bearing aluminosilicate mineral of the kyanite-sillimanite group. The formula has been given as Al2SiO4(F,OH)2, [Al(F, OH)]2SiO4, or 2Al2O3?2Al(F, OH)3SiO2. Topaz is generally considered a semiprecious-to-precious gem mineral, but it is a fairly common minor constituent of granites. In 1937 the U.s. Geological Survey reported an occurrence of massive topaz in the 3 Brewer gold mine, Chesterfield County, S.C. Over the next 8 years considerable research was done on topaz to establish its properties and to determine possible end uses The first reported shipment of ore was in 1939 Peak production was reached in 194412, and output then began declining until the mine closed in 194913? During World War II topaz was used in refractories, as a flux in steel mills, and in the manufacture of borosilicate glass 14. The main advantage of using topaz over kyanite and sillimanite in refractory use was that calcined topaz converted to over 95 percent mullite (3A1203 .2Si02) while calcined kyanite or sillimanite contained only 88 percent mullite15. However, a major draw-back to utilization of topaz is the evolution of fluorides during calcination. In 1973 the Geological Survey reported that topaz occurred in probable commercial quantities in at least two domestic locationsl6: the Brewer area of South Carolina and a location in Colorado. The literature also indicated that progress had been made in controlling fluorine-bearing fumes. This research has progressed to the state where valuable fluorine compounds are being recovered on a commercial scale 17. Thus, a major obstacle to utilization of topaz appears to have been resolved. The Bureau of Mines under its program of advancing minerals technology initiated a project to study techniques for the concentration of topaz from disseminated materials. The objective of the study was to determine those techniques that would be used to produce topaz concentrates that could be utilized as a source of fluorine and mullite.

Jan 1, 1977