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By R Steinhaus, D M. Frantois-Bongarton, P W. Cleary, G K. Robinson, M D. Sinnott

Multotec Process Equipment and Dominique Frantois-Bongarton have a patent for a mineral sampling device, which they call a æTrue-Belt SamplerÆ. This uses a plough, which is rotated about an axis parallel to a conveyor belt to throw material off the belt. A fixed sample cutter takes a sample from the material thrown off the belt.Discrete element modelling has been used to consider a range of plough designs, plough speeds, positions for the cutter relative to the plough, cutter apertures, cutter designs and frictional properties, prior to the building of a physical prototype. This modelling work will be discussed, both as an illustration of the role of modelling in the development of new materials-handling devices and in order to explain the likely strengths and weaknesses of this new type of sampling device.CITATION:Robinson, G K, Sinnott, M D, Cleary, P W, Steinhaus, R and Frantois-Bongarton, D M, 2012. Modelling of a ætrue-belt samplerÆ - A new device for sampling from a conveyor belt, in Proceedings Sampling 2012 , pp 33-40 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By M Goers, M Almond

"The use of reverse circulation (RC) drilling for grade control sample collection was selected by the Pueblo Viejo Mine Geology department at the recommencement of the operation in 2010. This method was selected because it allows: for multi-bench drilling (60 m hole depth, four benches of mining) to aid mine planning and provide a detailed close spaced drill data comparison with the reserve model angled drill holes to optimise the drill hole interception of the vertically controlled mineralisation dry sample collection in areas of excessive surface and groundwater mining operations to commence with the long assay return period (due to the need for the samples to be shipped overseas for analysis) until the on-site laboratory is operational.To date, 118 302 m of drilling has been completed throughout the operations of two open pits: Monte Negro and Moore. Two drill rigs (contractor and site-owned and operated) with three generations of sampling systems have been used to date. Throughout the drilling a 20 per cent quality assurance, quality control (QAQC) sample check (blanks, field duplicates and standards) have been used to check the drilling and laboratories performance. In addition, a total of 1104 fines samples were collected to compare the drill chip samples collected and the fines lost with two of the sample systems used.The drilling to date has highlighted the need for a complete and coordinated system to be used before sufficient confidence in the quality of the samples collected is achieved.The complete system must be set-up and coordinated to obtain the best quality sample possible. This complete package includes: drill bit size and shape for the rock being drilled and mineralisation targeted face sampling hammers with the correctly sized hammer shrouds sample hose routing to reduce sample flow turbulence and choking blow-down valves to eliminate drill hole water that has entered the drill string during rod changes correct drilling techniques targeting sample quality a sample system that captures the fines for inclusion into the sample.These improvements can be obtained without reducing the drilling rates.The measurements required to demonstrate the improvement in the sample quality will be the focus of future work within the department.CITATION:Goers, M and Almond, M, 2012. Bit to bag - The importance of a total coordinated system in reverse circulation drilling, in Proceedings Sampling 2012, pp 65-72 (The Australasian Institute of Mining and Metallurgy: Melbourne)."

Aug 21, 2012

By V Rasouli, G Cavanough, A Mokaramian

The sampling time, the costs and its quality are the three factors that determine the best method of drilling in mineral exploration. The two principal methods of reverse circulation (RC) and diamond core drilling are often used in combination by mine operators. RC is used for drilling shallow holes and in-pit grade control, and core drilling for deeper holes to identify future resources. The RC method is faster and more flexible than coring and provides virtually uncontaminated cuttings (ranges from dust to 25 mm chips) to the surface cyclone suitable for geochemical anomalies. The diamond coring produces core samples to increase the level of geological knowledge and the 3D extension and distribution of the orebody. However, both of these methods are subjected to certain limitations and inefficiencies in reaching deeper depths and drilling complex hole geometries. Examples of such shortcomings include the inability to provide enough air pressure for RC drilling and high friction between drill pipe and the hole wall in diamond core drilling.Considering that delivering large volume of reliable samples from deep zones to the surface in shortest possible time is of paramount importance in mineral exploration, and assuming that obtaining core samples over whole overburden is not always essential, then drilling small size holes as fast as possible and delivering the small chip samples to the surface would be a good alternative with several advantages over conventional drilling methods for deep hard rocks mineral exploration. As a result, the use of coiled tube (CT) drilling technology has been proposed recently for such applications. CT is a continuous length of ductile steel or composite tube stored and transported on a large reel; and allows fast drilling by eliminating the connection time and providing continuous circulation during drilling. This enables quick access to the zone of interest to collect the cuttings or obtain core samples. CT is advantageous particularly in drilling directional boreholes and multi-laterals. In this paper, feasibility of using CT delivering reliable samples is discussed for deep mineral exploration. In addition, recent developments and practices are presented that make CT a reliable drilling technology to drill cheaper, faster and deeper and to deliver more continuous and reliable data and samples from deep formations.CITATION:Mokaramian, A, Rasouli, V and Cavanough, G, 2012. Quality sampling using coiled tubing drilling in deep mineral exploration, in Proceedings Sampling 2012 , pp 73-80 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By D M. Frantois-Bongarton

Variograms can be powerful tools for the analysis and control of process streams and their sampling. Their uses and proper utilisation have been described somewhat unclearly to date, and their limitations and precautions of use are too rarely mentioned. The general meaning and properties of the variogram tool and its use in geostatistics are therefore reviewed in details to derive a critical view of its proper use for process control: what to expect from it and what it cannot deliver and which uses are illusory or potentially misleading. A summary of GyÆs seminal work accompanies this essay to put the concepts into historical perspective.CITATION:Frantois-Bongarton, D M, 2012. Review of variogram properties and remarks on its use in process control, in Proceedings Sampling 2012 , pp 175-180 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By C R. Stanley, D Lawie

The measurement of error in assays collected as part of a mineral exploration program or mining operation, including errors introduced during sampling, sample preparation, or geochemical analysis, historically has been undertaken in a variety of ways. Different parameters have been used to describe the magnitude of relative error and each of these parameters is related to the standard measure of relative error, the coefficient of variation. Calculation of the coefficient of variation can be undertaken in a variety of ways; however, only one produces unbiased estimates of measurement error: the root mean square coefficient of variation calculated from the individual coefficients of variation. CITATION:Lawie, D and Stanley, C R, 2012. Average relative error in geochemical determinations - Clarification, calculation and a plea for consistency, in Proceedings Sampling 2012 , pp 181-184 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By C D. Rose

"The primary objective of this paper is to demonstrate a different approach to predicting and verifying mechanical sampling system precision. Early in the year 2011 an experiment was conducted to evaluate the sampling precision being obtained by a three-stage falling-stream mechanical sampling system for coal owned and operated by Peabody Energy. This system collects samples from lots averaging approximately 14000 t being loaded onto rail cars at a flow rate averaging about 9000 t/h. In phase 1 of the experiment, a total of 60 increments were collected in a two day period at preassigned intervals using a cross-belt sampler located on a conveyor belt feeding a silo upstream of the sampling system under evaluation. Coal variability parameters were calculated from the resulting laboratory analysis data using the gauge-invariant fractal model developed by the author.Estimates of precision of the three-stage system as a function of the number of increments were calculated using the variability parameters determined in phase 1. In phase 2 of the experiment, duplicate samples of 30 lots of coal were taken by the three-stage sampling system, enabling calculations of the precision being achieved by the system. Phase 2 precision estimates are in reasonable agreement with those of phase 1. Conclusions drawn from the experiment include the following: Experimental variograms or the equivalent correlograms are essential in understanding sampling issues and for designing a sampling system to meet specific precision requirements. Consensus coal sampling standards provided by ISO and ASTM may be improved by treating all stages of a mechanical sampling system as æsamplingÆ rather than considering downstream sampling stages as æsample preparationÆ, to be treated in a separate part of the document. The coal industry would profit from use of methodology for routinely monitoring the overall measurement precision and the precision of the individual components of measurement: sampling, sample preparation and laboratory testing. This would not only give necessary credence to the measurement results but would also no doubt, lead to more efficient sampling system designs.CITATION:Rose, C D, 2012. Evaluation of precision being obtained by a three-stage sampling system for coal, in Proceedings Sampling 2012, pp 115-124 (The Australasian Institute of Mining and Metallurgy: Melbourne)."

Aug 21, 2012

By D M. Frantois-Bongarton

"A few situations are first reviewed where practical shortcuts lead to acceptable solutions where none seemed to be possible. These include: The solving of many complex sampling optimisation problems with the simple approach of the worst case policy (WCP). A simple approach to single-stage sampling problems will be mentioned at continuation. In the plants, minimising the impact of border effects in incorrect samplers, so that the resulting samples are approximately correct and acceptable in practice because the bias risk attached to them is controlled. Examples are given, as well as practical tools and a general methodology.Finally, some sources of undue conservatism are reviewed with general recommendations aiming at eliminating them.CITATION:Frantois-Bongarton, D M, 2012. Practical considerations and shortcuts in sampling, in Proceedings Sampling 2012, pp 171-174 (The Australasian Institute of Mining and Metallurgy: Melbourne)."

Aug 21, 2012

By I M. Platten, Y Xie, R-M F. Bell, S C. Dominy, L E. Howard, R C. A Minnitt

For any resource evaluation program, the collection and processing of representative samples for assaying is critical. Sampling, sample preparation and assay protocols must be designed to suit the style of orebody in question. The a priori need is for the characterisation of mineralisation type(s) and domain definition. The proportion and size of gold particles has a direct impact on the effectiveness of sampling protocols employed. Mineralogical studies focusing on gold particle deportment, size and distribution are required. Key issues are the presence of gold particle clustering and proportion of coarse versus fine gold. High-resolution X-ray computed tomography (HRXCT) is a radiographic technique that produces high-resolution 3D computerised models of in situ objects based on density distribution. The ævirtualÆ specimens are made up of voxels, the 3D equivalent of pixels each assigned a grey value based on X-ray absorption. This paper presents the results of recent research on the imaging of in situ particles in coarse gold-bearing ore samples from the Nalunaq mine, southern Greenland. The samples used were previously well-characterised through mineralogical and metallurgical testing, and serve to test the HRXCT methodology. Gold particle size and distribution in the context of the sampling liberation diameter was investigated.CITATION:Dominy, S C, Platten, I M, Howard, L E, Xie, Y, Bell, R-M F and Minnitt, R C A, 2012. Determination of the sampling liberation diameter in a high-grade coarse gold ore by high-resolution x-ray computed tomography, in Proceedings Sampling 2012 , pp 161-170 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By P W. Cleary, G K. Robinson, M D. Sinnott

Discrete element modelling (DEM) is a research tool that involves numerically solving the equations of motion of large numbers of particles. It can be very useful for investigating mechanisms that can lead to bias when extracting samples from material as it is carried on a conveyor belt or as it falls from the end of a conveyor belt. DEM is more realistic than conceptual models and mathematical models; but it is not as realistic as physical experimentation. Its primary advantages over physical experimentation are that it is cheaper and that it allows many factors to be varied while keeping other factors unchanged.This paper reviews our investigations of the performance of sampling systems by using DEM. The sampling systems investigated include falling-stream cutters, cross-belt cutters, Vezins and a device called a ætrue-beltÆ cutter, which is being developed. The purpose of the review is to explain what DEM has contributed to the theory and practice of sampling, and to indicate what it is likely to be able to contribute in the future.CITATION:Robinson, G K, Cleary, P W and Sinnott, M D, 2012. How discrete element modelling is influencing the theory and practice of sampling, in Proceedings Sampling 2012 , pp 15-20 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By S C. Dominy, R C. A Minnitt

Determination of the sampling constant and liberation diameter are of importance when applying the Fundamental Sampling Error (FSE) equation to optimise sampling protocols. The method for the direct determination of the sampling constant is based on the æGy 50-pieceÆ experiment and variants thereof, which is generally known as the heterogeneity test. In the coarse gold environment, the heterogeneity test is prone to poor repeatability and bias due to the very heterogeneity that it aims to quantify. A key issue is the large sample mass that can be required in the coarse gold environment, which may reach 1 t or more. The heterogeneity test often provides an evaluation of the background gold grade heterogeneity, but understates that of the high-grade coarse-gold component. This is because the total mass of fragments is usually too small to represent the mineralisation. Despite this relatively well-known problem, heterogeneity tests are often undertaken on deposits where the presence of coarse gold is ignored, not fully realised or vastly understated. Sampling types and protocol designs are frequently based on poor quality data that do not match the characteristics of the orebody. For this style of mineralisation, an empirical approach to define ore characteristics is recommended.CITATION:Dominy, S C and Minnitt, R C A, 2012. Application of heterogeneity testing to coarse gold ores, in Proceedings Sampling 2012 , pp 143-160 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By N Guresin, A Cooper, L Lorenzen, H Muller, S C. Dominy

Sampling and metallurgical test work during various phases of engineering?studies?is of?paramount importance for a robust processing plant design. When developing a process flow sheet, risks in achieving desirable financial outcomes are minimised by ensuring appropriate sampling and adequate metallurgical test work supports the engineering and cost estimation at each phase of project development.The quality and type of samples used for metallurgical test work are just as important as the metallurgical test work itself. The key characteristic required of any sample is that it represents some defined portion of a mineral deposit. Representivity should take into account the spatial orientation, lithology, alteration, degree of oxidation, mineralogy and competency of the ore such as hardness and abrasiveness. Statistically representative sampling procedures and an appropriate metallurgical test work program should be designed to bring metallurgical understanding up to feasibility study standard and to give a basis for process plant design.Snowden has observed that the quality of sampling and quantity of metallurgical test work carried out during the various phases of engineering studies are often insufficient to truly support a robust plant design. Some designs are often the result of the plant design based on benchmarks of apparently similar orebodies or buoyant metal prices supporting cash flows until rectifications can be implemented.The paper will discuss important aspects of sampling and test work required for engineering studies in designing process plants based on industrial case studies.CITATION:Guresin, N, Lorenzen, L, Dominy, S C, Muller, H and Cooper, A, 2012. Importance of effective sampling and test work protocols for process plant design, in Proceedings Sampling 2012 , pp 95-108 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By P Cleary, G K. Robinson, J Hilton, P Wilson

Concern has been expressed that Vezins can be biased when used for sampling fine materials if the cutter speed is as high as the 0.6 m/s which is often used. Using modelling techniques that consider airflow as well as particles, we have endeavoured to investigate sampling bias as a function of the size of fine particles, cutter aperture, cutter speed, shape of cutter blades, and the size of the gap between the inlet pipe and the cutter blades. Using crude estimates of the rate of airflow and a simple model of a single particle moving through air led to an approximate rule that bias will not occur due to mechanisms related to airflow for particles larger than about 200 microns; and bias will always occur for particles smaller than about 40 microns. For particles between these size limits, the extent of bias depends on particle density, cutter speed and cutter geometry as well as particle size.CITATION:Robinson, G K, Wilson, P, Hilton, J and Cleary, P, 2012. Avoiding bias when using vezins for sampling dusty materials, in Proceedings Sampling 2012 , pp 109-114 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By C D. Rose

A review and summary of the results of 120 coal sampling system bias tests is presented. This review supports new methodology using multivariate statistics currently being considered by ISO TC27 SC4. The current difficulties with ISO 13909-8 are explained and the logic behind the current new working draft is discussed in detail. Bias was detected in nearly 36 per cent of tests reviewed, suggesting that much improvement is needed in designing, maintaining and monitoring the performance of sampling systems in order to avoid sampling bias.CITATION:Rose, C D, 2012. Bias testing of mechanical sampling systems for coal - A review of test results and call for use of multivariate statistical analyses, in Proceedings Sampling 2012 , pp 185-192 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By P Hofmeyr, D Pretorius

Iron ore, which is transported by rail from the iron ore mines at Sishen in the Northern Cape, to the Saldanha Iron Ore Terminal in the Western Cape, needs to be analysed while loading to be exported. Every shipment will be sampled and an average analysis of the ore will be produced which is required by the purchaser at the receiving port. On arrival at the iron ore terminal at Saldanha, the ore is tipped from the rail trucks onto conveyor belts to be either stockpiled or direct-loaded. The conveyor belts run under the sampling plant and the ore is sampled periodically by means of an automated cross-belt sampler. This is the first iron ore port sampling facility in which the automated sampler is situated above the conveyor belts and not adjacent to them. A portion of the primary sample taken off the belt is moved to the dedicated sampling laboratory situated behind the cross-belt sampler and over the conveyor belt lines. The sample is split in the laboratory, one split being used for moisture and particle size determination and the other part is dried and then analysed by means of X-ray fluorescence spectrometry (XRFS) on fusion beads for major and minor elements. Particular care is taken to obtain high quality data for penalty elements.This sampling plant is completely automated and from the primary cross-belt sampler to final analysis by XRFS no manual steps are involved. This has meant that some processes are used which are suitable for automation and are ISO compliant but not necessarily ISO-certificated. The ISO manuals were developed with manual laboratory processes in mind. Precautions are also taken to maintain the integrity and representativity of the samples. This paper is a case study?describing?the automated sampling systems used at the Saldanha Iron Ore Terminal sampling facility and laboratory from conveyor belt to analysis.CITATION:Hofmeyr, P and Pretorius, D, 2012. Automated sampling of iron ore for analysis at the Saldanha Iron Ore Terminal in South Africa, in Proceedings Sampling 2012 , pp 25-32 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By S Brochot

In cases where coarse gold is present in a deposit, it is usual to use the screen fire assay (SFA) method to analyse the samples. There is no doubt that this method is more accurate than the standard fire assay (FA) and reduces the risk to have a systematic bias. Nevertheless, the difference between the analytical errors of both methods can be glossed over when the overall sampling error is added to obtain the measurement error. In that case, the advantage of the SFA cannot justify its higher cost.The current paper attempts to address this question in the case of a gold ore deposit with visible coarse gold in various sampling situations (drill core sampling in exploration, blasthole or chip sampling in mining exploitation). The overall measurement error is estimated taking into account the analytical error and all the sampling error components following the Pierre GyÆs theory of sampling.Firstly, only the last sampling stage is considered when the pulverised sample is processed either to obtain one analysis sample for a FA or to be screened and subsampled for a SFA. The calculated measurement error clearly shows the advantage of the SFA specifically in presence of coarse gold. Secondly, the half core sampling is studied to explain the observed discrepancies when controlling the second half core. Finally, the blasthole sampling is treated using in situ heterogeneity models to show that the relative advantage of the SFA is hidden by the large overall sampling error.In conclusion, the choice of the assaying method is discussed at the light of the overall measurement error and in accordance to the analysis objective.CITATION:Brochot, S, 2012. Standard fire assay or screen fire assay? Application of the overall measurement error approach to choose the most appropriate method, in Proceedings Sampling 2012 , pp 135-142 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By Z-Y Pi, B Zhang, S Wen

"The paper introduces the structure and work processes of outside auger hollow claw tipped mechanical sampler for coal. Twenty sets of claw tipped sampler performance tests show that: The design of inner hollow cylinder-type (?180 mm) can ensure to take a coal sample with nominal top size of 60 mm. Built-in self-cleaning piston pusher ensures no adherence and blocking of the sample. The operation practices show that the mechanical sampler can operate in order for taking coal sample with up to 16 per cent of total moisture. Claw closing design can avoid sample leaking or spilling during the claw lifting and ensure the integrity of primary increment. Ultrasonic positioning device makes the sampler capture the materials no less than 10 cm from the bottom of the wagons, basically meeting the requirement taking full depth of the sample. The precision and bias test indicates that the moisture and ash have no relative bias under the sampling process; the sampling precision is in accordance with the requirement in IS013909.At present, the spiral mechanical sampler is widely used for coal sampling but there are many limitations during application, for example: It is difficult to capture a large size sample, so the size range of a coal sample taken is limited. There is easy adhering or blocking for high moisture coal, which will result in the mixture of different increments, wear of sampler and the difficulties for cleaning and maintenance of sampler. It is difficult to capture the coal sample at lower than 30 cm from the bottom of the wagons, in order to avoid damage of the vehicle. It is possible for coal sample loss and spilling during the sampler lifting, due to the unsealed sampler.For the outside auger hollow claw tipped mechanical sampler designed for solving the above problems, the opening distance of the claw is the opening size of the sampler and makes the size range of the coal sample to be taken wide. During sampling, the two pieces of claws open and the sampler rotates vertically downward to capture an adequate coal sample after reaching the specific point. Then the two pieces of claws close tight automatically to ensure there is no coal leaking or spilling. The inner pusher of the sampler will prevent from the adherence and blocking of the coal sample effectively.CITATION:Zhang, B, Pi, Z-Y and Wen, S, 2012. Outside auger hollow claw tipped mechanical sampler for coal, in Proceedings Sampling 2012, pp 41-44 (The Australasian Institute of Mining and Metallurgy: Melbourne)."

Aug 21, 2012

By I T. Ross

Sampling drawpoints in block cave mines has been a contentious issue for many years. Doubts have been expressed as to the validity of the process used at most mines. This paper outlines the sampling practice commonly in use, discusses the resulting issues associated with reconciliation and drawpoint closure decisions. The paper also looks to the future and highlights issues for some block cave mining operations currently planned to have in the order of one thousand active drawpoints. It is likely that these operations will require a new approach to drawpoint sampling. There are several potential technologies currently available although some appear to be better suited than others to replace the current approaches. CITATION:Ross, I T, 2012. Sampling in block cave mines, in Proceedings Sampling 2012 , pp 81-86 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 21, 2012

By Julián Pérez Falcón

El mineral que se procesa en la planta concentradora de Mesapata-Cátac de la Compañía Minera Toma la mano S.A. presenta comportamientos complejos puesto que el mineral es oxidado y polimetálico. En ese sentido, el presente texto busca recuperar los minerales oxidados polimetálicos complejos a través de la tecnología limpia de dicha empresa que consiste en eliminar reactivos nocivos al medio ambiente y sustituir o reducir a otros por reactivos orgánicos.

Aug 1, 2012

By Osvaldo Aduvire

El presente texto describe las mejores técnicas preventiva que permitan predecir la generación ácida permitan a partir de ensayos de laboratorio denominados ensayos ácido/ base que simulan las reacciones que experimentarán los materiales excavados cuando entran en contacto con la atmósfera y agua de lluvia e inicien un complejo mecanismo de oxidación que termine generando drenajes ácidos.

Aug 1, 2012

By Pedro Hugo Tumialán de la Cruz

Dado que el Perú ocupa el segundo lugar en la producción de plata a nivel mundial, el presente estudio describe la metalogenia de este metal. Respecto de su fisiografía y geología, se tienen rezagos de la Cordillera con rocas metamórficas del Pre-cámbrico, rocas metamórficas y sedimentarias del Paleozoico y Mesozoico en el suroeste del Perú y noroste del Perú en Paita, Illescas y Amotape. Mineralización de platacomo un subproducto se encuentra en los siguientes yacimientos: exhalación volcánica marina, yacimientos relacionados a diques de inyección magmática félsica, yacimientos tipo pórfidos de cobre, yacimientos tipo skarn, yacimientos de reemplazamiento y relleno en calizas, yacimientos de oro y plata en areniscas-cuarcitas-pizarras, yacimientos tipo cordillerano, yacimientos de oro y plata de baja ley de alta sulfuración y yacimientos tipo Mississippi Valley.

Aug 1, 2012