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By L. W. Kempf, K. R. Van Horn

DURING the recent development of aluminum alloys for free-cutting screw-machine rod, it became desirable to know something of the solubility of lead and bismuth in liquid aluminum and in some aluminum alloys. The literature is not particularly helpful in supplying this information. These portions, therefore, of the constitutional relationships of aluminum-bismuth and aluminum-lead alloys were investigated by thermal analysis and by chemical analysis of samples taken from aluminum-rich melts in equilibrium with precipitated lead or bismuth. The solubility of lead and bismuth in some liquid aluminum-copper alloys was also investigated. Some consideration was also given to the solubility of these elements in solid aluminum. Among the earliest investigators of the aluminum-lead and aluminum-bismuth systems was Wright,1 who reported that melts of aluminum and lead formed two layers indicating limited liquid solubility. Under his conditions, the aluminum-rich layer was reported to contain 1.91 per cent Pb and the lead-rich layer, 0.07 per. cent Al. Subsequently, Pecheau2 found that in aluminum-rich alloy melts with more than 10 per cent Pb three layers were distinguishable. He reported that the middle layer contained from 3 to 10 per cent Pb. He also found that the melting point of aluminum appeared to be lowered slightly by the addition of lead. Gwyer3 investigated these alloys and found evidence of a slight lowering of the freezing point of aluminum by the addition of either lead or bismuth. He found no evidence of solid solubility in either case and made no attempt to determine the liquidus curves. Hansen and Blumenthal4 reported that the addition of lead distinctly lowered the solidification point of aluminum. They also found that bismuth lowered the melting point of aluminum. Guillet5 reported almost complete mutual immiscibility for the aluminum-bismuth alloys in the liquid state. Bohner6 examined the effect of various concentrations of lead and bismuth on the electrical conductivity of aluminum. He found decreases in conductivity on annealing at 500° C. as compared with the conductivity of the same alloys on annealing at 300° C.

Jan 1, 1938

By Charles Barrett

THE experiments reported in this paper have been fruitful in disclosing the mechanism of the deformation of iron in compression. They have established the nature of "deformation bands," "etch bands," or "X-bands," that have been a recognized but little understood feature in the structure of cold-worked metals since the early days of metal-lography, and have shown the role of the bands in the development of preferred orientations by cold-working. The work has also shown the relation of the orientation of individual grains to the preferred orientation of the aggregate. Some of the methods previously used in the determination of the indices of slip planes and slip directions are shown to be untrustworthy in the presence of deformation bands. The conclusion is reached that many slip planes and slip directions must operate during each stage in the compression of a single crystal, and that theories failing to take account of this require revision. In conducting the experiments a method f compression has been used by which extreme reductions can easily be reached, even to the limit set by the metal's capacity to deform with-out fracture. The work is a portion of a research program on the plastic properties of iron and steel. It is being used as a foundation for studies of orienta-tions resulting from recrystallization and is being extended to other metals and other types of deformation.

Jan 1, 1938

By Mark Sheppard

This paper is the second of a series recording the results of tests made at various quarries throughout the United States to determine, (1) the relation between the size gradation of feed to, and product from, primary crushers; (2) the particle shape of crushed product; (3) the differences in gradation and particle shape produced by different tries of primary crushers; and ( 4) the differences in gradation and particle shape caused by crushing different kinds of stone. Primary crushing has received comparatively little attention in the technical literature in spite of tine fact that the design of the whole crushing plant should be correlated to the performance of the primary crusher.

Jan 1, 1938

By John B. Hodgeson

AMMONIA is an essential constituent in the production of the ammonium-sulphate and ammonium-phosohate soil fertilizers manufactured by the Consolidated Mining and Smelting Company of Canada, Limited. The fertilizer plant, built in 1930 at Warfield, near Trail, provides a means of utilizing the large amount of sulphuric acid produced from the sulphur dioxide which is removed from the smelter smoke. The plant has an avail-able source of cheap power which makes the production of fertilizer economically possible. The fundamental operations involved in the production of ammonia at the Warfield plant are, first, the manufacture of hydrogen by the electrolytic dissociation of water; next, the recovery of nitrogen by the fractional distillation of liquid air; and finally, the combination of hydrogen and nitrogen in proper proportions and under suitable conditions to form ammonia.

Jan 1, 1938

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Jan 1, 1938

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Jan 1, 1938

CHAIRMAN I. N. BAYLESS: Will you come to order, gentlemen? They told me that you had a very interesting meeting yesterday and a good time last night. Our program is rather long this morning, and I am not going to take up any of your time, as we got started a little late. I will ask Mr. Marchant to make a few announcements. (Announcements.) SECRETARY MARCHANT: I just noticed in this morning's paper a rather serious accident at Hobbs, New Mexico, in which George Kaseman, a former President of the Institute, and a loyal member ever since its organization, was killed. I think that this meeting should go on record and prepare a resolution of condolence, etc., and with your per- mission we will have the Committee on Resolutions do that. I assume that will be all right. CHAIRMAN BAYLESS: Our first paper and discussion this morning will be Education of the Miner, by Thomas Allen, Chief Coal Mine Inspector of Colorado. Mr. Allen.

Jan 1, 1938

By W. A. Knoll

THE sinking of a new shaft at the Newport mine, Ironwood, Mich., was started in May 1931 and completed on Aug. 3, 1932. During this period, 2665 ft. of shaft in granite was completed, at, an average advance of 6 ft. per 24 hr. In November of 1930, experimental work was con-ducted oil 65 ft. of shaft through 22 ft. of overburden where ledge was encountered, and this work convinced the operators that all drilling could be clone with vertical holes with the blasting relief to a 4 ½ -in. hole drilled vertically in the center of the cut. The reason for not adopting the conventional V-cut was to get away from damaging the shaft steel. The blasting in a V-cut naturally tends to throw the broken material upward, but with the cut as adopted the relief was in a horizontal direction to a large extent. The scheme of mucking employed made it necessary to keep the steel shaft sets within 511 ft. of the bottom at all times. This could not be clone without serious damage with a V-cut when blasting in granite. The cut as drilled also broke 10.53 ft. per round of drilling, which was considerably more than the experience with a V-cut in the sane material. The extended cut reduced proportionately the delays for charging, blowing smoke and handling drilling equipment in the shaft. Another advantage was the ease in drilling vertical over inclined holes, and the preservation of the proper spacing of the drill holes at the bottom of the cut.

Jan 1, 1938

By Howard N. Eavenson

From the Pittsburgh coal bed in the four states of Pennsylvania, Ohio, Maryland and West Virginia has been produced an output that, at mine prices, represents a greater value than any other single mineral deposit in the world has yielded.12 While this distinction may in a few years pass to the gold reef of the Witwatersrand, it is possible that eventually, owing to the tremendous reserves still remaining, the ultimate yield of the Pittsburgh bed will be greater than that of any other known single deposit. Considering its importance, not a great deal has been written of its early history and development as a whole; most of the accounts have been of limited localities, or, at the most, of the area within a single state. In "Coal through the Ages" the writer mentioned some references to its early history, but this study will deal not only with its history but with the character of the bed, where and why it was first developed, and its effect upon the states in which it is found. It has not been the intention to write a detailed history of the development of the seam in each locality, as neither time nor inclination were available for doing such work, but only to show the influences that tended to hasten or retard such development. In general the historical matter ends about 1830, when geological surveys began to be made. Some of the maps show data available only since that time, and the sections about coal preparation and coking have been extended to the present time to show the changing conditions. It is believed that the early history includes all published records, and many more sources than those shown in the bibliography were consulted. It is quite likely that some references to coal in this area may be found in the unpublished papers of some of our early soldiers and colonizers, which exist in several libraries, and it is hoped that some future * Dedicated to Dr. Thomas S. Baker, President Emeritus, Carnegie Institute of Technology, whose labors in promoting the International Coal Conferences and in establishing the Coal Research Laboratory have done much in showing the industry how science can be of help to it. Manuscript received at the office of the Institute Feb. 15, 1938.

Jan 1, 1938

By L. E. Porter

El Segundo field is about 14 miles southwest of the central portion of the city of Los Angeles, immediately adjacent to the town of El Segundo and the Standard Oil Company's El Segundo refinery site. The field is served and bisected by several major highways connecting the beach cities on the west side of the Los Angeles Basin. The exact location of the field and its position with respect to other producing areas is shown on the map covering this portion of the Basin (Fig. I). The Republic Petroleum Co. discovered the first commercial production in the area when it completed its El Segundo No. 1 (sec. 18, T. 3 S. R. 14 W.) at a depth of 7402 ft. on Aug. 24, 1935, flowing at the rate of about 400 bbl. per day, 28" gravity oil. The producing horizon in this well consists of about 72 ft. of conglomerate and schist conglomerate situated below the nodular shale (Miocene). The true (or solid) schist (Franciscan) was encountered and penetrated some 20 ft. in the bottom of the hole. This paper gives a report on the history of development and oil production to date, and also submits the writer's interpretation of structural conditions as determined from such development. The limited development, together with the complex and variable nature of the producing horizon, makes any interpretation of the structure at present only tentative, and any forecast for a given well extremely hazardous. History of Oil and Gas Production The El Segundo field has produced approximately 1,920,000 bbl. of oil. It has 27 producing wells and 14 drilling wells or locations. The present daily rate of production is about 13,400 bbl. The production history of the field to date is shown in Table 1. The principal companies operating or owning leases in this field are: Caminol Company, Geo. F. Getty, Inc., Ohio Oil Co., Republic Petroleum Co., Pacific Western Oil Corporation, Royalty Service Corporation, Richfield Oil Corporation, Standard Oil Company of California, The Texas Company, Union Oil Company.

Jan 1, 1938

By A. A. Millar

THE output of coal from the Province of Alberta reached its peak; in the year 1928, when 7,334,179 tons were produced. Following this, a steady decline was recorded, and in 1930 a low mark of 4,564, 290 tons was made. Since that time, however, the tendency has been upward, and this year (1937) 5,551,682 tons were produced, compared with 5,696, 375 tons in 1936 and 5,462,973 tons in 1935. The value of the output in 1937 was $14,434,969, against $14, 720,004 in 1936. The coals of Alberta have been classed under three heads, viz., domestic, sub-bituminous, and bituminous The domestic (or lignite) and the sub-bituminous coals are used chiefly for domestic purposes, with the possible exception of the smaller sizes and the output of the two stripping pits at Stereo and Coal Valley The bituminous output is used mainly by the railways, for locomotive purposes, which, in 1937, accounted for 80.6 per? cenr of the total sales of bituminous coal. A fair proportion is sold for stationary engine and steam purposes and, in 1937, 25,000 tons were used in making briquettes at plants operated by the Canmore Coal Company, Limited, and Brazeau Collieries, Limited. The International Coal & Coke Company, Limited, used 99,500 tons in their plant at Coleman, for making coke. The bulk of the 66,000 tons of coke produced was sold for use at the smelter at Trail, B.C.

Jan 1, 1938

By A. G. Roach

MILLING of Nova Scotia gold ores began in 1862 with arrastras and wooden stamps and has progressed to heavier stamps followed by tables and other forms of concentration for the recovery of the sulphides. Chlorination and cyanide leaching of the concentrates has been practised, and in 1936 the combined amalgamation and all-sliming cyanidation plant of Seal Harbor Gold Mines was built. It has since been found that it is not necessary to cyanide the full tonnage and now only the concentrates are being so treated. From his experience in this enterprise, the writer presents the accompanying flow-sheet and supporting comments. While he has not the temerity to maintain that it is the best or only flow-sheet for Nova Scotia gold ores, he feels that it warrants thoughtful consideration by members of the milling fraternity of the Province. THE ORE The gold in Nova Scotia ores occurs both free and intimately associated with sulphides-chiefly arsenopyrite. Much of the free gold is quite coarse and crystalline. This is especially true when it occurs in white quartz. When in the slate, it is usually in thin plates and scales, frequently coated and discoloured. The values bound up in the sulphides are not amenable to amalgamation and must be recovered by other methods-concentration, followed by smelting or fine grinding and cyanidation. While high freight and treatment charges apply on concentrates shipped from the Province to smelters, a considerable quantity has been so disposed of in the past. However, it is hoped that a customs cyanidation plant will soon become available to producers of these auriferous concentrates in Nova Scotia.

Jan 1, 1938

By Herbert Johnson

DURING the past 10 or 12 years very little information has been made generally available concerning the commercial possibilities of separating materials by means of static electricity; and yet during that same period important improvements have been made in various branches of the science of electricity, which, when taken together, and applied to electro-static separation, have resulted in important improvements in that art as well. For example, much improvement has been made in high-voltage electrical equipment such as full-wave vacuum-tube rectification and improved mechanical rectification. Great strides have likewise been made in the development of insulators for high-voltage work, not only in the materials used but also in the design of the insulators themselves. Again, in another field, the development of air-conditioning equipment has improved the technique of controlling the surface condition, through drying or humidifying, of the various materials that are passed through the electrostatic separator. In many authoritative publications and textbooks, the electrostatic separation process is declared to require a balance far too sensitive for general commercial application. For example, one publication1 in the past has referred to an unfavorable effect on the process caused by varying atmospheric conditions such as humidity. Some2 have even gone so far as to state that sunlight and shadows may seriously affect the separating efficiency of the process. Such statements may have been true in the early development of the art, when the source of static elec-tricity was derived from a friction disk machine, such as the Wimshurst. The Blake Mosher equipment and the work of Huff in applying motor-generator sets, transformers and mechanical rectification overcame much of this kind of objection to the commercial application of the elec-trostatic separating process.

Jan 1, 1938

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Jan 1, 1938

By C. B. Foraker

THE Magma mine, of the Magma Copper Co., at Superior, Pinal County, Arizona, is 68 miles east of Phoenix and 21 miles west of Miami, Arizona, on highway U. S. 180. TEMPERATURES AND UNDERGROUND WATERS Surface Temperatures.-The average surface dry-bulb temperature at Superior is 72.4°; wet-bulb, 57.4°; with an indicated relative humidity of 38 per cent. The average yearly rainfall from 1921 to 1936, inclusive, was 18.74 in. The maximum condition of the atmosphere is in June, July and August, and the minimum is in January and February. The surface temperatures, of course, influence the temperatures of the down-cast shafts; however, the variation between winter and summer causes a difference of only 2° to 3° in the stopes and working places that are not close to the intake shafts. Average atmospheric conditions are shown in Fig. 1. Rock Temperatures.-Rock temperatures on the deeper levels of tile mine are as follows: LEVEL DEGREES LEVEL DEGREES 2000 109 3200 127 2250 112.5 3400 130 2550 116 3600 134 2800 120 3800 137 3000 124 4000 140 There appears to be no difference in rock temperature for any particu-lar horizon of the various formations or in the vein. Water encountered is always the same temperature as the rock from which it flows, and for this reason it is thought that the water is heated by the rock; not the rock by the water. The country rock apparently has been heated by the various intrusions, perhaps the vein itself, and has not yet had time to cool off. The geothermal gradient (Fig. 2) as indicated by the rock tem-peratures given above is 1 1/2 ° per 100 feet.

Jan 1, 1938

The production of Rumania for 1937 amounted to 54.142.600 bbl., which is a decrease of 10.319.636 bbl., or 15.9 per cent over that of 1936. In all. 1.300.000 ft. were drilled during the year— an increase of 220.000 ft. over 1936.

Jan 1, 1938

By Norman A. M Macleod

FOR the past seven years, all flotation at the Britannia mill has been done in Forrester Air-Lift cells. Prior to 1931, the roughing and part of the cleaning operation had been performed in four 21-cell and two 14-cell M.S. machines. The resulting economies in reagent, power, maintenance, and general operating costs, and the increased recovery, more than justified the exclusive use of the Forrester machine. About three years ago, the possibility of still further improving the efficiency of the flotation section was the subject of considerable discussion and experiment. Arising from these experiments, tests were made of the practicability of using a cell of greater depth than that of any pneumatic or mechanically-agitated machine in common use. Cells were constructed with depths of 7 .5 feet, 10 feet, and 15 feet, and, in all cases, a very definite improvement in operation was indicated. The cell now being used in the mill treats from 5,500 to 6,200 tons of dry feed per day. It is 100 ft. long by 5 ft. wide by 8 ft. deep, and has replaced a total length of over 500 feet of standard Forrester machine. The choice of a depth of 8 feet was governed by the type of blower which was available-in this case, a Roots-Connersville blower, driven by a synchronous motor and delivering 6,000 c.f.m. of free air at 4.0 pounds per square inch. At the Chelan Division of the Howe Sound Company, where a new mill was recently built, all flotation is carried on in cells 10 feet deep, with good results.

Jan 1, 1938

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Jan 1, 1938

By Charles E. Reed

With the increasing importance of clay in drilling operations which demand more precise and exacting control over its behavior, there has come the realization that most of our present methods of control over many of its important properties still represent more of an art than a science. Such a situation with respect to a material of such industrial significance is unfortunate, and naturally many investigations have been conducted to improve our knowledge. In general, these investigations have revealed the complex nature of clay behavior and while sometimes they may not have seemed to contribute directly to a solution of the field operator's problems they have been of inestimable importance in bringing to light the broad fundamental scientific principles upon which must be based any effective working theory correlating the known facts of clay behavior and predicting profitable new lines of attack for its improvement. Major Facts Concerning Behavior of Clays In the study of clays, as in that of most other colloidal materials, it has been impossible to make progress by the study of isolated facts. On the other hand, analysis of large groups of facts, many of which seem at first completely unrelated, can lead to a deeper insight into the structure of clays and the mechanism of their behavior. It will be well to list the major facts on which the analysis here presented is based, starting with those that have emerged repeatedly from past investigations and which thereby constitute an impregnable foundation upon which must rest any comprehensive theory of clay behavior: 1. Clays consist of hydrated aluminosilicates of extremely fine and variable particle size. 2. Suspended in water, clays exhibit variable degrees of swelling, depending upon their origin and upon the chemical and colloidal nature of any other substances present. The magnitude of the swelling is a direct indication of the extent to which the clay has become dispersed.

Jan 1, 1938

By W. M. Deaton

[Knowledge of the ten?erat~rre to wkich n gas ullder3atur~ted xith re- srplc t to water vapor may be cooled before the water p?f 11 3egin to condense 8 is desirable .and frec-uently iq neceTsarp in nWy resenrch c~d industri~J activities. This tenperrture, the dew point, i s 2 nrrticulnrly innortmt factor in high-pressure gas transmission, PS water cox?-ensate any interfere i with the flow of gos in the line. Sonetimes this interfexnce is due only to the yresence of the liquid water. At other tfncs, under certain condi- tions of pressure and teriperature, the cogdense;? water cn!nhines with the 93 to farm solid .y2: hydrctes. These solid coar~ouncis ma:/ ccllect in sufficient quantit;. to rehce materially the c~xrying cap.citg of the pipe line or ever, to ply thc line coimletelp. ]

Jan 1, 1938