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By R. D. Hancock

The complex responsible for the poisoning of anion-exchange resins is identified as the anionic cobaltic penta¬cyanide mono aquo species. It is shown that, at high concentration, this species polymerizes in solutions of pH less than 9. A mechanism for poisoning is presented that involves adsorption of anionic cobalt cyanide by a normal ion-exchange process, followed by polymerization within the resin matrix to form complexes that are too large to diffuse readily through the resin pores. The effects of resin structure and functionality on the extent of cobalt poisoning are examined, and the effect of cobalt poisoning on the kinetics and equilibrium loading of uranium is discussed.

Jan 1, 1979

By J. J. van Vuuren

Pipe-stick support in deep-level gold mines is first described and illustrated, a pipe-stick being a mine pole trimmed to the required size and sleeved by a pipe. An account is then given of an investigation into this form of support that involved load-compression tests in a 1000-ton press, tests in a rapid loading machine simulating rock-burst conditions, a study of the load-compression behaviour of pipesticks installed underground, and a cost evaluation. Pipe-stick support was found to be very effective on the face and to cost less than conventional matpacks.

Jan 1, 1979

By S. Venter, W. E. Stumpf

Some of the factors that govern the choice of a nuclear fuel are briefly discussed, special reference being made to the introduction of advanced carbide fuels into fast-breeder programmes. One of these factors, i.e. the compatibility of carbide fuels with stainless-steel cladding, is discussed in depth. A very sensitive technique for the study of compatibility interactions between fuel and cladding is described in respect to the effects of particle size, specific surface area and surface oxidation of the fuel,and microstructure of the cladding on the compatibility behaviour of the cladding with the fuels. Finally, the need for the development of modified or stabilized uranium carbide fuels is discussed, and some results are presented to show the effects of small amounts of sulphur in these fuels on their compatibility with stainless-steel cladding materials.

Jan 1, 1979

The Canadian Institute of Mining and Metallurgy. Milling practice in Canada. CIM Special Volume 16. 1978. The purpose of this volume is to up-date The Milling of Canadian Ores, which describes Canadian mineral. processing plants and gives other metallurgical information, and was published by the Sixth Commonwealth Mining and Metallurgical Congress in 1957. NIM reports Report no. 1874 Activation analysis and classification to soune of samples from the Kimberley Reef conglomerates. (10th Mar., 1977; released Jun. 1978). Report no. 1926 The analysis of anode sludges by X-ray-fluorescence spectrometry. (5th Jun., 1978). Report no. 1936 The analysis of mineralogical and metallurgical materials. A guide to the analytical techniques and instrumentation available at the National Institute for Metallurgy. Report no. 1959 The slag-metal equilibrium, and the activities of slag and metal components in the production of high-carbon ferromanganese. (15th May, 1978). Report no. 1965 Analyses, by several laboratories, of three ferromanganese slags. (22nd May, 1978). Report no. 1968 The influence of carbonaceous reducing agents on the rate of reduction of representative manganese and chromium ores. (28th May, 1978). Company Affiliates Guide To The Preparation Of Papers for Publication In The Journal Of The South African Institute Of Mining And Metallurgy The following notes have been compiled to assist authors in the preparation of papers for presentation to the Institute and for publication in the Journal.

Jan 1, 1979

The Annual General Meeting of the South African Institute of Mining and Metallurgy was held in Kelvin House on Wednesday, 23rd August, 1978. Mr P. A. von Wielligh (President) was in the chair and declared the meeting open at 16h00. Obituaries The President: It is my sad duty to announce the death of the following members of the Institute : T. K. Prentice and W. E. Gooday, Honorary Life Fellows and Past Presidents; B. S. Allen, J. A. Becking, L. H. Mellor, C. A. Pratt and W. T. Stobart, Life Fellows; J. P. Burls, E. Cameron, M. L. Fitzgerald, C. G. Hinds, A. J. Patrick, H. O. Reisener, N. D. Shuttleworth, N. Soldan and J. Whitehouse, Fellows; T. Gemmell, J. S. A. Oelofse, W. D. Rowe, R. L. J. Shearman and G. M. Thain, Associates. As a mark of respect to the memory of the deceased and in sympathy with the bereaved, I ask you to rise and observe a few moments' silence. Welcome The President: It is now my very pleasant duty to welcome our distinguished guests and visitors. We are pleased to have with us Mr D. A. Etheredge, Vice¬President of the Chamber of Mines of South Africa, and Mrs Etheredge. Mr Etheredge this afternoon represents the mining industry at our meeting. The importance of the close link that over the years has been maintained between the industry and our Institute speaks for itself. We are, therefore, grateful that he and Mrs Etheredge have managed to find the time to be with us this after¬noon.

Jan 1, 1979

Bowen, R., and Gunatilaka, A. Copper, its Geology and economics. London, Applied Science Publishers, 1977. Miller, D. S. Internal flow systems. (Volume 4 in the BHRA Fluid Engineering Series). 1978. 288 pp. £21,50. MACH 80 The Machine Tool Trades Association of Great Britain (M.T.T.A.) announce that MACH 80 - The International Machine Tool Exhibition - will take place from Tuesday, 22nd April, to Friday, 2nd May, 1980, at the National Exhibition Centre, Birmingham.

Jan 1, 1979

Financial Times Mining International Year Book 1979. London, The Financial Times Limited, 1979. 712 pp. Price: airmail, U .S. $60,00; surface mail, U .S. $42,00. International Wrought Copper Council. Glossary of terms applicable to wrought products in copper and copper alloys. London, the Council (6 Bathurst Street, Sussex Square, London W2 2SD), 1978. 170 pp. 80 Swiss francs (approximately £25). Council of Mining and Metallurgical Institutions At a meeting of the Council of Commonwealth Mining and Metallurgical Institutions held on 15th January, 1979, it was unanimously agreed that the name of the Council should be changed.. Assaying and analytical techniques This year sees the Diamond Jubilee of the South African Institute of Assayers and Analysts, which held its first meeting on the 3rd of May, 1919.

Jan 1, 1979

The Annual General Meeting of the South African Institute of Mining and Metallurgy was held in Kelvin House on Wednesday, 22nd August, 1979. Dr M. G. Atmore (President) was in the chair and declared the meeting open at 16h00. Obituaries President: It is my sad duty to announce the death of the following Members of the Institute : Brigadier R. S. G. Stokes, Honorary Life Fellow and Past President ; J. A. Arthur, C. L. Cartwright, R. B. Greaves, A. A. Haynes, G. Ross, M. W. Richards, W. T. Stobart, E. Veres, G. V. White, and A. G. Williams, Life Fellows; A. J. H. Pole, D. T. McMurray, P. G. O. Pretorius, A. E. D. Rubidge, A. M. Seccombe, and R. R. Uren, Fellows; R. E. Oltman, R. B. Richardson, and G. P. Rundle, Members; S. F. Dench and S. van Wyk, Associates. As a mark of respect to the memory of the deceased, and in sympathy with the bereaved, please rise and observe a few moments' silence. Minutes President: May we confirm the minutes of our last Annual General Meeting, which was held on 23rd August, 1978, as published in the November issue of the Journal? Agreed.

Jan 1, 1979

By H. W. Glen

The use of a personal style (mainly active voice and first person) makes technical writing more pleasant to read, and helps the writer to express his meaning clearly and to avoid many of the stylistic errors normally encountered in that type of writing.

Jan 1, 1979

By P. A. Von Wielligh

Without minerals, man cannot possibly hope to maintain his present standard of living. Professional mining men throughout the world, particularly in mineral-exporting countries like South Africa, are faced with the increasingly difficult task of ensuring adequate supplies of minerals. The problems of gradually diminishing mineral reserves and rapidly rising mining costs can to a certain extent be overcome by the use of more-sophisticated technological techniques and by the improvement of efficiency wherever possible. However, there is growing concern in some quarters, that, despite the ingenuity of engineers, geologists, metallurgists, and scientists, the earth's mineral reserves will eventually become insufficient to meet man's needs. In order to ensure the continued well-being of the earth's population, it is therefore imperative that more attention should be paid to mineral research and the training of specialists in the field of mineral reclamation.

Jan 1, 1978

In Chapter 1 we mentioned that up to three components are considered to represent the variability of regionalized variables : a deterministic component, a correlated component, and a random component. In Chapter 2 we considered some of the models based on the assumption of randomly distributed values: the random component was assumed to be the only one present. In Chapters 3 to 11, more general but also more complex models were described, based on the assumption that the values were correlated with the possible presence of random noise. In this chapter we introduce a model used to analyse non- stationary data, for which a deterministic component (or drift) must be assumed. This model will be used for estimation purposes, and the corresponding optimal linear estimation procedure is known as universal kriging. The theory of universal kriging is much more complex than the theory of kriging. Fortunately, in the majority of mine valuation problems the drift can be ignored and the simpler form of kriging can be used.

Jan 1, 1978

By W. D. Grimsley, R. P. King, J. B. See

Samples (15 to 20 g) of pre-calcined Mamatwan manganese ore or pure Mn 304 smaller than 48 mesh were reacted at temperatures in the range 1000 to 1300°C with samples of spectrographically pure graphite smaller than 325 mesh. Samples (1 g) of ore or pure Mn02 smaller than 48 mesh were reacted at temperatures of 1000 and 1200°C with pure graphite fines in argon, with graphite in carbon, .'1onoxide, and with carbon monoxide alone. In each case, the loss of mass as a function of time was recorded with a hermobalance. The rate and degree of reduction were found to increase with additions of carbon and with increasing temperature up to 1300oC, when they reached their maximum. The shape of the reduction curves, together with the results obtained from examination of the products of reaction by microscopy and X-ray diffraction, were used as the basis for a postulated reduction mechanism. Some details are given of an initial kinetic model that was used to verify the proposed mechanism. It was found that the reduction of Mamatwan ore by graphite at temperatures in the range 1000 to 1300°C occurs in two stages: (i) an initial stage during which the higher oxides of manganese are rapidly reduced to MnO with concurrent formation of CaMn2O4 and (ii) a longer stage during which CaMn2O4 and MnO are reduced to carbides by carbon dissolved in the ferromanganese phase.

Jan 1, 1978

Branch Minutes of the General Meeting held at President Steyn Gold Mine canteen on Wednesday, 10th May, 1978, at 4.00 p.m. Erratum We apologize to Mr J. G. Taylor for the error in one of his qualifications. Bio-engineering monograph The selection of papers presented at the International Bio-engineering Conference at the University of Cape Town organized by the South African Institution of Mechanical Engineers and held in April 1977, and which are appearing in The South African Mechanic al Engineer during April to June this year, will shortly be available in book form. Mathematics The Institute of Mathematics and Its Applications is planning the following conferences and symposia: The Nand F Proposals in Relation to Mathematics, 1st July, 1978: London School of Pharmacy. NIM reports Report no. 1917 The instrumental neutron-activation analysis of granites from the Bushveld Complex. (31st Mar., 1978.) Report no. 1951 Potentialities and limitations of four-parameter equations for the correlation of formation constants of metal-ion complexes in aqueous solution.(15th May, 1978.) Report no. 1963 An evaluation of the methods used at the National Institute for Metallurgy for the analysis of base-metal concentrates. (28th Apr., 1978.) Report no. 1964 The separation, by anion exchange, of noble metals on substituted cellulose. (28th Apr., 1978.) Guide To The Preparation Of Papers For Publication In The Journal Of The South African Institute Of Mining And Metallurgy The following notes have been compiled to assist authors in the preparation of papers for presentation to the Institute and for publication in the Journal.

Jan 1, 1978

[The following notations will be used: O an ore body. W a sample of size w located in O; the size of this sample. W a block or a sample, of size W, located in O; the size of this block or sample. z' a point in W. W' a block or a sample, of size W' greater than or equal to W, located in O; the size of this block or sample. z" a point in W'. y (h) point semivariogram in O. s (h) point covariogram in O. In the previous chapter, we saw that the point semivariogram y (h) usually cannot be estimated directly from the data available. Rather, the values of samples of size w are available in O, and from these a regularized semivariogram y w (h) can be estimated. The following relationship has been proved (5.8): Y w(h) = Y (w;w+h) - Y (w;w). y (w;w+h) is the average value of y (z' z") when z' takes all possible positions in a sample w and z" all possible positions in a sample w+h of the same size, h being the distance between w and w+h. y (w;w) is the value of y (w;w+h) for h = 0, i.e. the average value of y (z' z") when z' and z" take all possible positions in w. We also saw that the regularized covariogram aw(h) is related to the point covariogram a (h) as follows (5.9): w(h) Gr In the following chapters, it will be shown that calculation of the average value y of y, or -a of a, in the general case relating to samples or blocks W and W' which need not be of the same size, plays a very important part in all the practical applications of geostatistical theory. The purpose of this chapter is to introduce various methods of calculating y and a-. Furthermore, mathematical equations and graphs are provided which can be used when the point semivariogram can be represented by one of the more common equations, and when the blocks W and W' are of simple shape. By definition (Fig. 6.1): [ ] Y (W;W) = WW f dz' f y (z' z") dz" (6.1) in W z" in W']

Jan 1, 1978

By A. Vogelzang

The paper describes how the level of the water-table was reduced as a result of increased pumping of water from the mine. Because such a condition in an area where there is compactable material above solid dolomite results In surface movement, steps were taken to restore the water-table to its former level. These included the return of water underground via a sinkhole and boreholes, and the piping of water from another mine.

Jan 1, 1978

By J. Meintjes

The measures taken by Rand Carbide Limited from the 1950s to 1976 to control dust emission from the electric furnaces at its Witbank factory are described. A new design of furnace for calcium carbide followed by a dry-fabric filtration plant for the furnace gases was not successful in arresting the dust. A 131 m chimney commissioned in 1968 effectively dispersed the dust-laden gases from both carbide and ferrosilicon production and so brought considerable alleviation. In 1974 a bag-filter dust-collecting plant was successfully commissioned on a 6 MV.A carbide furnace, and this was followed in 1976 by a bag-filter plant on a 46,5 MV.A ferrosilicon furnace. The company has spent considerable effort and money over two decades in trying to combat dust emission, but eventual success had to await technological development.

Jan 1, 1978

Council and Standing Committees, 1976-1977 President: Dr M. D. G. Salamon. Vice-Presidents: P. A. von Wielligh and Dr M. G. Atmore. Honorary Treasurer: J. K. E. Douglas. Immediate Past President: Dr R. E. Robinson. Members of Council: J. D. Austin, E. Collier, C. T. Fenton, J. A. Holmes, Dr P. R. Jochens, Prof. R. P. King, Dr D. G. Krige, Prof. F. Q. P. Leiding, D. G. Malan, C. T. Shaw, D. A. Viljoen, R. A. von Maltitz. Chairman, Witbank-Middelburg Branch: E. J. Jackson. Chairman, Orange Free StatelKlerksdorp Branch: A. N. Shand. B. Past Presidents Serving on Council: R. J. Adamson, H. Britten, J. K. E. Douglas, R. C. J. Goode, Prof. D. D. Howat, Dr J. P. Hugo, D. G. Maxwell, Prof. R. P. Plewman, V. C. Robinson, P. W. J. van Rensburg. Ten Council meetings were held during the year, and the standing and sub-committees held seventy-one meetings. Standing Committee Chairmen: Membership, Dr M. G. Atmore; Technical Programme - Metallurgy, J. A. Holmes ; Technical Programme - Mining, C. T. Shaw; Vacation School - Metallurgy, Prof. R. P. King ; Vacation School - Mining, Dr D. G. Krige ; Awards, Dr R. E. Robinson; Excursions, C. T. Fenton; Adjudi¬cation, Dr R. E. Robinson; Constitution, Rules and Policy, Dr R. E. Robinson; Mines and Works, C. T. Shaw; Education, Dr R. E. Robinson; Pyrometallurgical Discussion Group (Convenor), Dr J. B. See; Phoenix National Committee, Dr R. E. Robinson.

Jan 1, 1978

By D. W. Boydell, E. B. Viljoen

A flowsheet incorporating rotary-drum filtration for the solid-liquid separation step, followed by solvent extraction for uranium purification, is used as a standard against which four flowsheets are compared. These flowsheets employ either counter current decantation or belt filtration for solid-liquid separation, and either solvent extraction or continuous ion exchange plus solvent extraction for the purification step. Sales revenue, taxation, capital expenditure, and operating costs are estimated. These factors are taken into account in the calculation of an incremental net present value for each circuit by the discounting of cash flows at 25 per cent per year over a projected life of 15 years. For the material used in these examples, the highest net present value results from the circuit that employs belt filtration followed by continuous ion exchange and solvent extraction.

Jan 1, 1978

By E. Barnea

This paper simplifies and provides a strict mathematical proof for an equation developed by R. J. Woody for the c alculation of solute recoveries in countercurrent decantation. The equation offers a convenient method for the optimization of flowsheets involving a simple countercurrent-decantation circuit.

Jan 1, 1978

By R. G. Jurd

This paper considers the introduction of large-scale longwall mining into South African coal mining, instead of the conventional mechanized bord-and-plllar mining that is widely practised at present. The two methods are compared, and longwall mining is found to have the advantage in several respects in some seams. The most cogent reasons for the introduction of the longwall method In some seams are associated with safety strata control and increased labour costs.

Jan 1, 1978