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By T. B. Counselman

PROBABLY the earliest concentration of iron ore in this country was carried on in the northeastern magnetite areas. Magnetic concentration was relatively simple and gave a concentrate that, after agglomeration, and in spite of being high in phosphorus because of the dry concentrating methods then in use, was satisfactory blast-furnace feed. Production from the northeastern magnetite area languished after the discovery and development of the Lake Superior ores, where there was seemingly an unlimited tonnage of high-grade ore, first the Michigan ores, and subsequently the still larger deposits of Minnesota. For years only the higher grade, direct shipping ores of the Lake Superior district were mined. Those of Michigan, and of the Vermilion Range in Minnesota, were hard ores and came principally from underground mines. The softer ores of the Mesabi came partly from underground mines, but mostly from the enormous deposits that could be worked by open-pit methods. The costs of ore from these open-pit deposits, even with the high initial cost of stripping, were so low that the underground mines of the Mesabi could hardly compete. The so-called Old Range ores, of Michigan and of the Vermilion Range of Minnesota, were hard and lumpy, and opened up the burden in the blast furnace, therefore making possible harder driving with greater output. Also, some of these ores were of such grade and physical characteristics that they were suitable for charge ore in the open hearth. These ores, therefore, commanded a price premium, and could compete with the softer, finer, but cheaper, Mesabi ores. The big tonnage reserves, however, are on the Mesabi, and it is these big open-pit deposits that constitute our stock pile of iron ore, from which we are drawing so heavily during this war period. On the western end of the Mesabi the ore was found to be high in silica, and not suitable as furnace feed. As early as 1902, attempts were made to concentrate this so-called wash ore and by 1910 the first washing plant was put into operation. The process was very simple, consisting essentially of a sizing and washing operation, with scalping screens, logwashers, and tables, which later were replaced by classifiers. Ore particles finer than 100 mesh were deliberately wasted, because these fines were undesirable in the furnace. Fortunately, these tailings were impounded, and already are being reworked. Before long some of the low-grade ores began to require more elaborate treatment than the simple washing operation and, tables having been discarded because of their low capacity, in favor of classifiers, jigs were next introduced. These were able to discard coarser pieces of tailing than classifiers. Jigs are in active use today, various improvements having been made in their design and application. Various other machines and methods of concentration have been tried from time to time, and have in turn been discarded for more improved processes. The latest and most important process that has been

Jan 1, 1943

By W. R. Davis

This paper presents a sunimary of the results of a study of the Dornick Hills-Springer sand reservoir of the Velma Pool. Stephens County, Oklahoma. The data are of interest because this type of reservoir is unusual in the mid-continent area. The reservoir is characterized by very steep dips and a relatively thick producing section. Its up-dip productive limit is defined by truncation of the productive sands, and the down-dip limit is defined by deterioration of sand quality rather than by the presence of an oil-water contact. The crude oil is of 29" API gravity, is relatively viscous and was saturated with dissolved gas at the original reservoir pressure. Consideratiqn of the physical characteristics of the reservoir indicates that natural water encroachment will be negligible, and that the producing mechanism will be a dissolved gas drive augmented by gravity drainage. Performance to date tends to confirm this. INTRODUCTION It is the purpose of this paper to present some of the features of the Dor-nick Hills - Springer sand reservoir which are unusual in mid-continent operations. The study was undertaken in an attempt to define the producing mechanism or mechanisms that will control reservoir performance, as an aid in determining well completion and production practices. GEOLOGY The reservoir under consideration is a series of sand bodies of Pennsylva-nian age found in the Lower Dornick Hills and/or Springer formations. For the purpose of this paper, the sand series is referred to as the Dornick Hills-Springer sand. This sand series lies on the northeast flank of the Velma anticline, and dips very sharply to the northeast in TWP 1S-5W, the average dip being about 45º. However, as shown in Fig. 1. the trend of the pool swings eastward in TWP 1S-4W with a coincident de- crease in dip angle. In this portion of the pool the average dip is about 25". Faults in Sections 30-1S-4W and 32-1S-4W are shown in Fig. 1. These faults show only minor displacements for the horizon contoured in Fig. 1, but they do show a pronounced displacement of the immediately overlying beds. Similar faults are thought to exist in TWP 1S-5W; however, since the detailed geological studies necessary to properly define these faults were not available to the author, no attempt to show them in Fig. 1 has been made. The up-dip productive limit throughout the pool is determined by the truncation of the Lower Dornick Hills-Springer sand. The down-dip productive limit does not appear to be defined by edge water, but by a gradual reduction in permeability of the sands. No dry hole has produced a significant volume of water from this sand section. There was a small gas cap in TWP 1S-5W. Most of the wells in TWP 1S-SW encountered an oil sand 70 ft to 150 ft thick, a shale 20 ft to 80 ft thick, and another oil sand 50 ft to 130 ft thick. A few scattered wells in this area encountered other and bodies below these

Jan 1, 1951

By W. R. Davis

This paper presents a sunimary of the results of a study of the Dornick Hills-Springer sand reservoir of the Velma Pool. Stephens County, Oklahoma. The data are of interest because this type of reservoir is unusual in the mid-continent area. The reservoir is characterized by very steep dips and a relatively thick producing section. Its up-dip productive limit is defined by truncation of the productive sands, and the down-dip limit is defined by deterioration of sand quality rather than by the presence of an oil-water contact. The crude oil is of 29" API gravity, is relatively viscous and was saturated with dissolved gas at the original reservoir pressure. Consideratiqn of the physical characteristics of the reservoir indicates that natural water encroachment will be negligible, and that the producing mechanism will be a dissolved gas drive augmented by gravity drainage. Performance to date tends to confirm this. INTRODUCTION It is the purpose of this paper to present some of the features of the Dor-nick Hills - Springer sand reservoir which are unusual in mid-continent operations. The study was undertaken in an attempt to define the producing mechanism or mechanisms that will control reservoir performance, as an aid in determining well completion and production practices. GEOLOGY The reservoir under consideration is a series of sand bodies of Pennsylva-nian age found in the Lower Dornick Hills and/or Springer formations. For the purpose of this paper, the sand series is referred to as the Dornick Hills-Springer sand. This sand series lies on the northeast flank of the Velma anticline, and dips very sharply to the northeast in TWP 1S-5W, the average dip being about 45º. However, as shown in Fig. 1. the trend of the pool swings eastward in TWP 1S-4W with a coincident de- crease in dip angle. In this portion of the pool the average dip is about 25". Faults in Sections 30-1S-4W and 32-1S-4W are shown in Fig. 1. These faults show only minor displacements for the horizon contoured in Fig. 1, but they do show a pronounced displacement of the immediately overlying beds. Similar faults are thought to exist in TWP 1S-5W; however, since the detailed geological studies necessary to properly define these faults were not available to the author, no attempt to show them in Fig. 1 has been made. The up-dip productive limit throughout the pool is determined by the truncation of the Lower Dornick Hills-Springer sand. The down-dip productive limit does not appear to be defined by edge water, but by a gradual reduction in permeability of the sands. No dry hole has produced a significant volume of water from this sand section. There was a small gas cap in TWP 1S-5W. Most of the wells in TWP 1S-SW encountered an oil sand 70 ft to 150 ft thick, a shale 20 ft to 80 ft thick, and another oil sand 50 ft to 130 ft thick. A few scattered wells in this area encountered other and bodies below these

Jan 1, 1951

By J. E. Lawver, J. L. Wright, H. R. Kokat

Mesabi semitaconite and oxidized taconite ores that cannot be concentrated by froth flotation can be rendered amenable to flotation through partial concentration in a high-in tensity wet magnetic separator. Since 1964, a method for accomplishing this precon-centration has been under development at the Minnesota Mines Experiment Station, where several hundred tons of ore have been successfully processed. This paper is an analysis of the performance of the separators used at the Station. At present the United States is producing about 85 million tons of iron ore a year, and nearly 55 million tons of this comes from Minnesota. Nearly half of Minnesota's production is in the form of magnetite taconite pellets —the remainder being wash ore and gravity concentrates. As the demands of the blast furnace operators become more stringent - and they are becoming more so yearly — these demands are met by improved iron ore beneficiation technology. Furthermore, there is no doubt that as magnetite taconite, gravity ores, and wash ores are exhausted, new processes will be developed to produce a product comparable to magnetite taconite pellets from Minnesota's vast reserves of oxidized taconite and semitaconite. The magnetite taconite ores are rather easily bene-ficiated by conventional, low-intensity (500- to 1400-gauss) magnetic separators, followed, in some plants, by froth flotation of the magnetic concentrates.

Jan 1, 1969

By T. E. Scott, O. G. Koepke

DURING research currently in progress the need arose for interplanar angles and planar spacings to analyze crystallographic data obtained from hcp yttrium. In the absence of such existing information, a program was written in Fortran-11 language and processed on an IBM 7074 computer. The program and results have been assembled in report form to make them generally available.' Of the possible combinations of, only those most frequently encountered were employed. The ranges of h, k, and 1 involved were: However, not all combinations and permutations of the above appear in the tabulation because redundancies occur in several cases. Nevertheless, fifteen types of planes and all their equivalent planes have been included, giving a total of 109 sets of Miller-Bravais indices.

Jan 1, 1967

By C. C. Wright, R. J. Day

Although data on the exact tonnage of recoverable coal silt are not known, the quantity produced in 1943 was estimated to be over five million tons for the anthracite region of Pennsylvania alone. Since that time the recovery of the No. 5 buckwheat size previously included in silt estimates has increased greatly thus reducing the total silt tonnage. As a compensating factor, however, the methods of recovering silt previously escaping into the rivers and streams have been markedly improved so that the net figure may not have changed materially. Comparable estimates for bituminous coal are lacking, but undoubtedly the silt represents a significant tonnage. With the trend toward increased wet cleaning of the smaller sizes of bituminous coal, it is to be expected that even greater quantities of silt will be available in the future. The raw silt from anthracite collieries usually contains a high mineral matter content, but technological developments in fine coal cleaning have been making rapid advances and it appears probable that more extensive use of these methods will be employed in the near future. Bituminous coal silt in many instances contains a similar high mineral matter content. As with anthracite silt, however, the cleaning of this material, where necessary, appears both technologically and economically feasible. With a view to upgrading the size and value of silt, considerable laboratory and pilot plant work has been conducted by a number of organizations on what is commonly known as pelletization. Actually the process is one of extrusion in which the moist silt is extruded from a die in the form of rods, which usually break into relatively short lengths—a few inches long—as they fall from the die. Fig I is a photograph of some extruded 3/8-in. diam pellets and of the anthracite silt from which they were produced This technique of producing larger sized material from fines is by no means new, having been used extensively by the industrial carbon and clay industries for years.' The application of the process to coal silt appears, however, to be relatively new. The first major program of investigation dates back only to July 1945, when a group of engineers representing the Anthracite Institute, The Pennsylvania State College and the J. F. Pritchard and Co. conducted preliminary tests on the extrusion of anthracite silt at the Floridin Co. plant at Warren, Pa. Since that time these three organiza-tions—individually, together, and in cooperation with other interested groups— have actively pursued work on various phases of the problem. Much of the early history and details of the laboratory and pilot plant work by the Anthracite Institute, has been reported by Mulcey and Eckerd.2 It is the purpose of this paper to report additional information on the process, especially with respect to the factors influencing the quality and use properties of the product, and the current develop-

Jan 1, 1949

By Robert Sisselman

If we are lucky," says Hollis M. Dole, Assistant Secretary of the Interior, "coal, uranium and hydropower will provide us with maybe a third of the energy we require in 1985. The other two- thirds will have to be made available in liquid and gaseous form." Luck, however, may have run out, for if the facts and figures relating to supply and demand of natural gas over the next 20 years prove accurate, the United States may fall short in its attempts to bring the energy crisis under control. By the year 1990 the world will need to consume a minimum 150 quadrillion Btu of energy with gas requirements running as high as 42-43 trillion cu ft. By 1990, the U.S. alone will require 45-46 trillion cu ft. To meet anticipated demand, this country will have to overcome a deficiency of about 20 trillion cu ft since, by all pragmatic estimates, it will produce only 15-20 trillion cu ft of gas. The importation of natural gas into the U.S. will help but will not solve the problem. Adequate gas supplies will have to be supplied domestically. The Arctic, with its predicted huge reserves of gas, combined with imports of liquid natural gas (LNG) may provide as much as 15% of the 45-46 trillion figure, however, such reserves will not come into play as quickly as originally thought. The Alaskan gas fields, for instance, will provide a substantial supplement to domestic gas needs, but only after 1976.

Jan 10, 1972

By James B. Austin

Growth of the Society When the Institute was born in May, 1871, it was given the name American Institute of Mining Engineers. Yet from its conception a few months earlier, its genetic code clearly carried the message that metallurgy was equal in importance to mining. Thus, the "call" for the initial meeting, which was sent out in April of that year by three mining engineers, Eckley B. Coxe, R. P. Rothwell and Martin Coryell, gave this first objective of the proposed organization as: "the more economic production of the useful minerals and metals." And this call concluded: "Anyone who may have devoted himself to a particular subject connected with either mining or metallurgy, and who may be possessed of new facts in reference to it, would greatly aid in furthering the objects of the proposed association by preparing a paper giving the results of his experience." In response to this call, a group of 22 men assembled in Wilkes-Barre, Pa., for a 3-day meeting beginning May 16, 1871. On the first day, a set of 20 "Rules" was adopted, of which Number 8 read, in part: "The words mining engineers in these rules comprehend engineers connected with mining and metallurgy." On the second day, 18 officers were elected, of whom nine were not present. Moreover, as if to emphasize that the words about metallurgists were to be taken seriously, one of those elected in absentia was the president, David Thomas, a Welshman who had founded the Thomas Iron Co. and who built the first anthracite-fired, hot-blast furnace in this country. The second meeting of the Institute, held in Bethlehem, Pa., in August, had a more metallurgical flavor, and the third meeting, in November, was held in what was then one of the great steel-making centers of the country - Troy, N. Y. This was the home of the Albany and Rensselaer Iron and Steel Co., which held the American rights to Bessemer7s machinery patents. And it was here that the great American steel master, Alexander L. Holley, carried out a series of experiments that led to improvements in the design and method of operation of the Bessemer vessels. It was at this meeting that Holley and Henry Marion Howe, then a "student" at the Albany and Rensselaer plant, were admitted to membership. Four years later, Holley was elected president of the Institute. Clearly, metallurgy

Jan 1, 1971

By Jasper Johnson

TAKEN in all its bearings there is, perhaps, no more interesting coal-field than that locally known and designated as " Wilmington," both on account of the superior qualities of its product as a house- hold and steam fuel, when compared with other Illinois coal, and its geological position. The territory underlaid with coal, to which this name was originally given, embraced a very small area, including only the south half of sections 31 and 32 (township 33 north, range 9 east) in Wilmington township, and sections 5, 6, 7, 8, 17, 18, 19, 30, and 31, with occasional outliers in sections 3, 4, and 9, and, possibly, in sections 20, 28, 29,30, and 32 (township 32 north, range 9 east) of Reed township, in Will County, comprising eleven square miles of workable coal within the known basin. Borings indicate the presence of coal on sections 30 and 33 in Wilmington

Jan 1, 1875

University of Alabama University, Alabama Mining and Metallurgical Society WILLIAM R. HIGGS, President ROBERT E. MEAD, Secretary J. R. CUDWORTH, Faculty Sponsor MILTON H. FIBS, Counselor University of Arizona Tucson, Arizona Miners' Society LEE BLESSING, President R. W. CORY, Secretary E. P. MATHEWSON, Faculty Sponsor B. R. HATCHER, Counselor University of California at Los Angeles Los Angeles, California Student Chapter, A.I.M.E. ARCHER WARNE, President ROBERT JOHNSTON, Secretary E. K. SOPER, Faculty Sponsor EMILE HUGUENIN, Counselor Colorado School of Mines Golden, Colorado Student Chapter, A.I.M.E. J. Ross REED, President ANDREW PERRY, JR., Secretary J. BURNS READ, Faculty Sponsor A. W. NEWBERRY, Counselor

Jan 1, 1936

By Kenneth C. Vincent, A. M. Gaudin

TEN years ago Taggart, Taylor and Ince1 described a workable, convenient apparatus for the measurement of contact angles between cleaved, ground or polished particles and captive bubbles. Wark and Cox2 and Wark and Sutherland3 have done an immense amount of experimental work with this apparatus. Their work has had as principal object the determination of "contact curves." Contact curves are cartesian charts in which pH (or some other variable) is plotted against quantity of modifying agent. The rectangular area is broken into two or more curvilinear areas separated by the contact curve. The curve indicates that a sharp demarcation exists between conditions that bring about sticking of particles to bubbles and conditions that do not produce sticking. The type curve appears in the TRANSACTIONS as Fig. 1, page 248, volume 112. Wark and Cox offer data to show that the contact angle has a value determined by and characteristic of the agent used. Wark and Cox also make the statement that they believe this value is independent of concentration (ref. 2a, p. 209). They say: It is suspected that, given sufficient time and provided that there are no disturbing factors, the full ethyl xanthate angle (corresponding to a complete xanthate film) would be obtained in every case where contact occurs. Such a conclusion, if correct, would tend to substantiate the hypothesis of flotation collection by metathesis championed by Taggart and his associates4-8 and would argue against the adsorption hypothesis now adopted by Wark7 and by one of us.8 However, the data of Wark and Cox do not bear out the conclusion that there is a sharp passage from conditions of contact to conditions of noncontact. Rather, they indicate the existence of a transition zone of reagent concentration across which the contact angle varies with changes in reagent concentration from zero to a value near the maximum. This may be seen, for example, from Fig. 195 in the new text by one of us (ref. 8, p. 380), which presents the data of Wark and Cox in graphical form. The object of this study has been to explore the nature of the transition from conditions of contact to conditions of noncontact. The data of Wark and Cox to which reference has been made as showing that a gradual transition exists are marred by the fact that the region of critical-agent concentration is at an extremely small concentration. This condition suggests that diffusion may have played such a preponderant role that equilibrium was not reached within the time alloted. In the Wark and Cox data, the critical concentration was at about one part of xanthate per million parts of water. To form a monolayer of xanthate on the mineral surface would therefore require depletion of xanthate in the liquid to a depth of the order of

Jan 1, 1940

By G. Ostberg

OXYGEN has frequently been considered responsible for phenomena in the metallurgy of cast iron which are not sufficiently explained by the presence of other elements. Oxygen and oxides have been regarded as critical factors, particularly for the solidification process, and specifically in the formation of graphite. However, the evidence for an influence of oxygen has mostly only been indirect or qualitative. Furthermore, quantitative data on the oxygen content of cast iron presented in the literature have often been less conclusive as being apparently determined with insufficient regard for the difficulties associated with the sampling and analysis. These problems, experimental and theoretical, have been studied in this investigation. An attempt is made to bring the views on the soluble amount of oxygen in cast iron on a level with the present understanding of the thermodynamics of these types of alloys. Although there are no experimental data on the complete multicomponent cast-iron alloys some conclusions have been drawn from investigations on simpler systems. The order of magnitude of the solubility of oxygen in cast iron is considered in the first part of the paper. The second part deals with the oxygen content actually present under practical conditions. First the possible sources of errors in sampling and analyzing methods are examined. Finally some observations on the oxygen and oxide content of malleable iron during the production process are made. THERMODYNAMICS OF OXYGEN SOLUBILITY When cast iron is saturated with oxygen the saturation phase is essentially carbon monoxide or silicon dioxide depending upon the composition of the iron, the temperature, and the rates of formation of the oxides.* The latter occurs accordiw to the O + C = CO, Kc0 - a COa J 20 + Si = SiO2, Activities are used here instead of weight pct concentrations, since activities are believed to show more sensitively the effects of the interaction of all the alloying elements. Calculations involving activities are, however, seriously hampered by lack of experimental data on the interactions between the components encountered in the multi component cast-iron system Fe-O-C-Si-Mn-P-S- and so on. In order to make an estimate of the oxygen solubility reason-

Jan 1, 1959

By Robert H. Richards

During tile summer of 1870, I had an opportunity to visit the laboratory of the late David Forbes, Esq., in London, and was much interested in a labor-saving device which he had attached to his agate mortar. The mortar was placed in the centre of a small table, and about ten inches to the right of the mortar, a post, perhaps two

Jan 1, 1879

By Ezequiel Ordoñez

The two mining districts of Pachuca and Real del Monte, well known for their antiquity and the extraordinary richness of their veins, are situated, 3 miles apart, only 62 miles north of the City of Mexico—the first being on the western, and the second on the eastern slope of the Pachuca range of mountains which bounds the great valley of Mexico. Close to the celebrated mining region of Pachuca is located the city of the same name, capital of the State of Hidalgo, at 2460 meters above sea-level and 20° 07' 35" North latitude, with 35,000 inhabitants, the majority of whom work in the mines; the remainder being Government employees, merchants, and a small number engaged in less important industries. The city extends along both sides of the canada which carries the waters of the river called "Avenidas de Pachuca," the banks of which are united by four bridges at regular intervals. The attention of the traveler approaching the city is first attracted by the appearance of the mountains, barren of vegetation, bounding the city with rocky cliffs and steep declivities, the grades of which serve as foundations to the irregular and varied groups of houses. Above these are the dumps, and, close by them, the mouths of the shafts, covered with conical tile roofs. The smoke of the chimneys, the noise of the mills and the appearance of some of the constructions reveal at first glance the industrial character of the place. At the left of the entrance to the canada, the mountain of San Cristobal, celebrated for the famous vein of Xacal, one of the richest and earliest exploited in the district, rises 450 meters above the city.

Jan 1, 1902

By R. G. Hall

An article on the subject of electrolytic zinc no longer needs to be preceded by an apology. The production of zinc by electrolysis is past the laboratory stage and has become an economic factor of considerable importance in the total production of zinc in the United States. The various methods of procedure to be followed fa the greatest economy of manufacture are fairly well known, consequently a detailed description of any method is no longer necessary or desirable. In this paper I shall endeavor to lay down some of the governing conditions in this industry, the relation of methods to ore deposits, freight rates, and sources of power supply. Power Points Assuming for a moment that, for the present at least, the electrolytic production of zinc will be confined to Those localities having developed water power, a glance at these powers so developed in the United States, with their relation to known zinc orebodies of economic size, will not be without interest. Northwest In the Northwest we have water powers, developed and undeveloped, . in Washington and Montana. These must, of course, bear a close relation to the rapidly growing zinc production of the Coeur d'Alenes and of the Butte districts. In general, the power of the territory in question is relatively low-priced, at least as compared with the cost of developing power from coal, and the near neighborhood of large bodies of more or less complex zinc ores makes these water powers of more than usual interest. The same remarks may be applied equally to the developed water powers of the Canadian side of the line in the Northwest, where we have again commercially available complex ore deposits such as are being exploited today at and near Trail. California One of the large complex ore deposits of the far West is to be found in Shasta County in the immediate neighborhood of the territory of the

Jan 1, 1918

The fifth convention of the National Foreign Trade Council was held in Cincinnati, Apr. 18, 19 and 20. More than one thousand accepted delegates were registered, the American Institute of Mining Engineers being represented by W. L. Saunders and W. N. Thayer. The convention was called to order Thursday morning, Apr. 18, in the convention hall of the Hotel Gibson; by the Chairman, Mr. James .A. Farrel, president of the U. S. Steel Corporation, and was in continuous session for two clays, several group sessions being held simultaneously. The convention adjourned Saturday morning after receiving the report of the central committee. The dominant themes of the convention were: First, "Win the War" and second, "Establish Foreign Trade on a. Firmer Basis." The discussions included textiles, lumber, chemicals, automobiles, finance, and agriculture, and also those things in which mining engineers are particularly interested, metals, oil, and coal. The report of the central committee, which was adopted, recommended the stimulation' of production of all materials required for war purposes; the subordination of all trade that will not impose new and heavy penalties on our adversaries; the maintenance of such foreign trade as will support national credit and supply materials required for military and naval purposes; the continued interchange so far as possible of merchandise and products between the United States and. Latin-America, Asia and Oceania; the immediate increase of tonnage in the north Atlantic; the cheerful and whole-hearted cooperation of importers

Jan 6, 1918

By B. W. Gonser

SOFT solders are used principally in the automotive, can-making, building construction and electrical industries, but their field of usefulness extends well beyond these principal users to a vast list of miscellaneous applications where metal joints are required. The most common soft solders and the only ones considered in this discussion are those com-posed of lead and tin, with or without various relatively small percentages of impurities or additions. A small amount of antimony is often pur-posely added. As an indication of the importance of these lead-tin solders, 8620 long tons were consumed in 1934 in the U.S., and during most of 1935 from 900 to 1000 long tons were used each month. A great many factors influence the properties of joints made with soft solders. Fluxes and the fluxing procedure used to prepare the surfaces to be joined in order to give a true metal-to-metal contact are among the most important of these factors. The temperatures used, cleanliness of the work and general soldering technique have their effect, but when results are unsatisfactory they are usually attributed to the metallic solder itself and the raw materials from which it is made. Some-times criticism of the solder is justified. The wrong composition may be chosen for a given job, impurities may be present that ruin certain desired qualities, or uniformity may be lacking. A solder may even be looked upon with suspicion because of its ancestry, regardless of its true composition and behavior. To clarify the effect of slight differences in composition as found in commercially refined solders, a comparison of properties of solders grouped according to their origin has been undertaken. This investigation seeks to give practical information on the proper-ties of tin-lead solders produced from virgin metals, from commercially

Jan 1, 1936

By S. K. Kawatra

The paper describes a system for on-line analysis of ash in solids in coal slurries for coal cleaning operations. The system consists of two sensors: 1) gama density gauge, and 2) ash sensor. The operational characteristics of each sensor are discussed.

Jan 1, 1980

NORMAN B. PILLING (author's reply to discussion *).-The discussion by Mr, Bassett raised one or two points that deserve further discussion. The printed figure for the lead content of the copper used was 0.015 per cent. and not 0.15 per cent., upon which his comment was based. A copper having the latter figure would, of course, be quite unusual. Mr. Bassett takes exception to the writer's statement regarding the distribution of cuprous oxide in wrought copper and states that "the FIG. 1.--ROLLED AND ANNEALED SHEET. ETCHED WITH AMMONIA AND HYDROGEN PEROXIDE. X 75. eutectic of copper with cuprous oxide is usually found between the crystals of pure copper, whether in the cast or the wrought form." While it is very well known that during the solidification of cast copper the cuprous oxide is segregated completely as an envelope of cuprous oxide-copper eutectic around the crystals of copper free from oxide, it is the writer's opinion that, as a result of repeated rolling, this eutectic structure is quite destroyed and the small particles of cuprous oxide become widely scattered, and in the recrystallization following, during annealing, the rearrangement of the grain boundaries takes place with much indifference to the actual distribution of these particles. In the accompanying micrograph, taken from a rolled and annealed sheet, the random distribution of the small cuprous-oxide particles with reference to the location of the grain boundaries may be seen.

Jan 3, 1919

By Robert F. Mehl, Gerhard Derge

The gamma-alpha transformation in iron and iron-rich alloys is of such practical and theoretical importance that many papers have been published upon the subject relating to critical temperatures, transformation rates and accompanying property changes. Although crystallo-graphic studies are of less immediate practical usefulness, the opportunities which these offer to furnish data on the basic atomic movements which characterize the transformation are not to be neglected1. The early work on the crystallography of this transformation has been reviewed in the fourth paper of this series2; since then several important papers have appeared. Our present knowledge may be briefly summarized as follows. Kurdjumow and Sachs, working with a 1.4 per cent carbon steel3, established the orientation relationships subsisting between the face-centered gamma and the metastable tetragonal lattices in freshly quenched martensite, and between the face-centered gamma and the body-centered alpha lattices in tempered martensite. The orientation relationship observed in the latter case may be stated in terms of planes and directions observed to lie parallel in the two lattices: {111} ?//{110}a [110] ?// [111]a (This notation is used throughout as the most descriptive means of expressing the fact that any (111) plane of the gamma phase may be parallel to any (110) plane of the alpha phase, and that a [110] direction in a particular (111)? plane is parallel to a [Ill] direction in the corresponding (110)a plane.) From these relationships the atomic movements that transform the gamma lattice into the alpha may be inferred. In the present experiment these may be considered as consisting primarily in a shear of the atoms parallel to the {111} planes in [110]? Directions

Jan 1, 1937