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By Wilbur I. Duvall, Thomas C. Atchison, David E. Fogelson

The breakage of rock by explosives depends largely on the ability of an explosive to transfer its stored potential energy to the rock as strain en- ergy. Therefore, the relative rock-breaking abilities of explosives can be determined indirectly by determining the relative amounts of strain energy transferred to the rock at the time of detonation. This report presents experimental data on the strain energy contained in explosion-generated strain pulses in a granite gneiss. Six explosives were tested. The scaled total radial strain energy E/W flowing outward through a spherical shell of scaled radius R/W1/3 surrounding the point of detonation was found to follow an exponential decay propagation law of the form Analysis of the data showed that the intercept parameter H depended upon the type of explosive used but that the absorption coefficient B was practi- cally independent of the type of explosive. Comparison of the intercept pa- rameter H and the calculated energy of the explosive showed that the percent- age of explosive energy transferred to the rock increased linearly as the ratio of the characteristic impedance (product of density and propagation velocity) of the explosive to that of the rock increased toward unity. From 5 to 9 percent of the calculated total energy released by the explosive was transferred to the rock as radial strain energy.

Dec 1, 1959

By S. E. Khalafalla

The extremely sluggish oxidation of steel scrap was appreciably accelerated when the charge was pretreated in aqueous solutions of sodium metavanadate or sodium molybdate. The degree of oxidation acceleration was inversely correlated with the melting point of the promoter oxide possessing the highest valency. The magnitude of oxidation enhancement exhibited a systematic inverse dependence on the duration of pickling processes; mere dipping of the oxidizable charge in the vanadate bath was most effective. In general, the rate of steel scrap oxidation increased with increasing concentration of the pickling reagent. The results are explained on the basis of the hydrolytic decomposition of the pickling agent with subsequent slow interaction with the metal surface, coupled with the tendency of vanadium to form polyanions in alkaline media. The data not only served to elucidate the mechanism by which catastrophic oxidation takes place, but also showed that the accelerating species need not be alloyed with the oxidizable metal; surface impregnation by minute amounts of the accelerating species can still produce catastrophic effects.

Jan 1, 1970

By F. C. Gregory

"Introduction.The third annual mine-rescue maneuvers of the Globe-Miami District First Aid and Mine Rescue Association were held at Globe, Ariz., on November 5 and 6, 1923. The first demonstration was held in October 1922, and the results** from that experiment, both in the practical training and the interest aroused in the apparatus men, were so much more satisfactory than those from the ordinary smoke-chamber training, that Orr Woodburn, director of the Association, decided to hold similar maneuvers at frequent intervals. The second test was held on March 21-22, 1923, in connection with the meeting of the Southwest Mining Section of the National Safety Council at Globe.Place and Organization.The recent maneuvers were held in the same mine and conducted in the same general manner as the first, and the points of interest not brought out previously are described below. By studying the accompanying map the movement of the teams can be better understood.Thirty-three apparatus men were out on the first day and thirty-two on the second day, a total of forty-three men being trained.Mr. Woodburn was aided in directing the work by his two assistants from the mine-rescue station, two local safety engineers, and an engineer from the Bureau of Mines. Local mine superintendents and the State deputy mine inspector were interested spectators."

Jan 1, 1924

By J. J. Demeter

Anthracite from the four producing regions in Pennsylvania was both ashed in the laboratory and burned on a chain-grate stoker to determine the sulfur-retention properties of its ash. The retention of sulfur in laboratory-prepared anthracite ash was shown to be related to ashing temperature and to the amounts of sulfur and calcium present in the coal. At the usual laboratory ashing temperature of 750° C sulfur retention ranged from 0.8 to 13.2 percent of the total coal sulfur. Sulfur retention in the ash was negligible, o to 0.3 percent, at 1,200° C, which is the thermal decomposition temperature of calcium sulfate; thus calcium sulfate does not form and cannot serve as a sulfur-retaining agent. In several tests the anthracite was mixed with 6 or 10 percent dolomite prior to firing in the chain-grate stoker. The dolomite did not improve sulfur retention owing to the high temperature in the fuel bed. Sulfur retention was, however, related to the unburned carbon in the ash. The relationship of the percentage of original coal sulfur retained in the ash (Y) to the percentage of the original carbon in the coal remaining in the ash (X) is expressed by Y = -0.579 + 0.914X. The percentage of sulfur retained is almost directly proportionate to the percentage of original coal carbon in the ash.

Jan 1, 1968

Use instantaneous sampling to pinpoint dust sources and to Improve dust control on longwalls. Approach Use a dust monitor developed under a Bureau contract. How It Works Sampling can be done by either a moving or a stationary method. In the "moving' method, the dust monitor is carried by a survey engineer walking at the midpoint of the shearer Dust levels and face position (support number) are taken during all phases of the mining cycle while the shearer is cutting. These measurements can show how changes in airflow along the face, face specific; (rock partings) and cutting sequence (cutting the wedge) variables affect dust levels. In the "stationary sampling" method, the survey engineer stands with the RAM at a fixed location on the face. As the shearer approaches, the dust level and the distance to the shearer are recorded at 10-second intervals. Typically measurements start when the shearer is 20 feet from the sampling position and continue as the shearer passes the position until it is 20 feet away on the other side. Dust profiles around the machine are obtained at several fixed locations along the face only while the shearer is cutting.

Jan 1, 1982

By Fun-Den Wang

Finite-element structural analyses were performed to determine the stress distribution and displacements around a single rectangular coal mine opening in a multilayered rock system. The effects of changes in mechanical properties of roof and coal layers, roof layer and mine opening geometry, horizontal-to-vertical load ratio, and structural geologic features on the stress distribution about the opening were studied. Variability in the stiffness and relative thickness of the immediate roof layers can produce a considerable difference in the stress distribution about the opening as compared with that of a homogeneous material. Changes in opening width and horizontal-to-vertical load ratio have different effects on the stress distribution about the opening depending on the composition of the roof layers. In general, where a stiff layer exists in the roof at the surface of the opening, the stresses are higher in the roof and ribs around the opening. Horizontal changes in facies in the roof layers produced by structural geologic features can also greatly alter the stress distribution about the opening compared with the simple layered cases.

Jan 1, 1974

By E. P. Youngman

The Ottoman law, which was in force in Palestine before the British con- quest of the country (1917-18), still forms the basis of the legal system. Nevertheless, with respect to mining, legislation has been considerably re- vised since the British occupation and mandate, some of the Ottoman laws having been either radically altered or wholly abolished, in order that the legal status of Palestine might be more in harmony with that of western States. Legal transition is still far from being complete; however, no further mining legislation is pending at the present time (March, 1931). Revisions during the British military occupation (1917-20) took the form of proclamations of the commander in chief. After the establishment of the civil administration (1920) changes in the legal system were a decided de- parture from the Turkish laws. In 1922 the practice was begun of giving con- secutive numbers and short titles to the ordinances. The basic mining law is the mining ordinance of 1925, No. 19 (amended by mining ordinance No. 10 of 1926), an "ordinance to make provision regarding the winning of minerals, and the conditions under which minerals may be gotten, and to replace the existing Ottoman laws relating thereto." The chief regu- latory provisions are embodied in regulations (A) and (B)--mining ordinance, 1925. This mining legislation of 1925 repealed the following laws:

Nov 1, 1931

By John B. Goodman

This report presents a study of a modification of the precision laboratory carbonization-assay apparatus that renders the unit capable of performance at low-, medium-, and high-temperature assay levels and permits, under controlled conditions, evaluation of the relationship between carbonization temperature and the yield of pyrolysis products. Second, the interest and value derived from the temperature study data directly apply to the particular semiplant carbonization processes and techniques currently being investigated in this laboratory. Data obtained with the assay apparatus enables the fuel technologist to predict the probable yields of carbonization products from pilot-plant operations under various carbonizing conditions. Data obtained with the assay apparatus has been used to predict the product yields of industrial carbonization plants at Kemmerer, Wyo., and Rockdale, Tex. The assay provides a useful tool in detecting, from the carbonized plant product, the degree of effectiveness of pilot-plant operation. Third, the residual volatile matter in some industrial carbons has broad significance. Evaluation of the volatile material remaining with or in the carbon may be assessed through the high-temperature-assay technique. The low-temperature carbonization assay devised by the writers has proved to be a versatile tool in predicting the probable product yields from pilot-scale carbonization processes. The apparatus described in previous publications has been modified to extend the range of testing above 500° C. without impairing the accuracy and reproducibility obtained in the low-temperature range. Results presented here include product yields from a typical Texas lignite and Wyoming subbituminous-B-rank coal over the temperature range 150° to 1,000° C.

Jan 1, 1958

By R. A. Cattell

The Bureau of Mines recently observed its fortieth anniversary, and with the close of the fiscal year 1950 it completed 36 years of close cooperation with and helpfulness to the petroleum and natural-gas industries, whose technical problems it studies. Petroleum people likewise observed the ninetieth anniversary of the start of this truly American industry when "Colonel" Drake drilled the first well at Titusville, Pa., in 1859 (see fig. 1). Throughout the period, during which there have been many changes in the fuel and related economy of the country, this work has been carried on systematically by an organized entity of the Bureau first known as the Petroleum Division and in recent years as the Petroleum and Natural Gas Branch. Changes in the industries have been brought about partly by economic forces, partly by advances in technology, and in some measure by the impact of two world wars. As the needs of industry and the Nation have changed, so have the studies of the Bureau changed to meet these needs. Consistently, Bureau technologists and scientists have tried to keep in step with progressive movements; frequently, in fact, have taken the lead. Wherever possible, they have looked far ahead in their program of research, at the same time recognizing the needs of the hour.

Jan 1, 1951

By H. M. Lawrence

The recovery of phosphate rack from the ores in the land-pebble district of Florida is a simple washing and screening operation. In the gashing plants coarse phosphate only is saved. Log-Washer overflows and screen-undersize products containing an appreciable content of fine phosphate are discarded. The phosphate grains in the material discharged to waste are generally finer in size than the mesh--14 to 20 mesh or 0.346 to 0.03 inch--of the finest screen in the washer. The operators state that the washers ordinarily recover from 50 to 60 per cent of the phosphate content of the matrix mined. Any increase that can be effected in the recovery of phosphate would be of advantage to the industry and would conserve the mineral resources of the country. In considering possible methods that might increase the recovery obtained in phosphate-washing plants the application of flotation, if it could be successfully developed, seemed to warrant investigation.

Jan 1, 1928

By S. J. Schatzel, J. Cervik, A. A. Campoli

The cross-measure borehole technique is being studied by the Bureau of Mines as an alternative to the use of surface gob boreholes as a means of controlling methane in gobs during longwall mining. Small-diameter holes are drilled from underground locations into strata overlying the mined coalbed. When the roof strata are fractured by the mining opera- tion, a partial vacuum applied to the boreholes draws the methane out of the fractured strata and prevents it from entering the mine ventilation system. Tests in the Upper Kittanning Coalbed showed that 50 pct of the methane produced by the longwall mining operation was captured by the cross-measure boreholes. Borehole inclination and penetration into the gob are two important borehole parameters that affect the performance of the cross-measure borehole system.

Jan 1, 1983

By Stephen Utter

This report summarizes the procedure and results of an investigation to determine the stresses in the rock around an underground opening in the Climax molybdenum mine, Climax, Colo. This study is part of an overall investigation conducted by the Bureau of Mines to determine the stresses induced by block-caving mining. The purpose of this study is to obtain estimates of the magnitudes and directions of the principal stresses, the location of the maximum stress concentrations, and the effect of topography on the stresses.

Jan 1, 1962

By B. W. Gandrud

[The meaning of the term "bauxite' has always been somewhat vague and indefinite, and the term has been used in various applications to denote sometimes a rock, sometimes a mineral, but more frequently an ore. It seems logical to think of bauxite as an ore, however, because a very large part (probably at least 85 per cent) of the entire world's production of bauxite is at present being used as a source of aluminum and aluminum chemicals. In the United States there are two districts that, produce bauxite - the Arkansas district and the Alabama-Georgia-Tennessee-Mississippi district. The deposits in Mississippi have been discovered recently and are riot as yet productive but it seems reasonable to consider them as apart of the-district hat includes the deposits of Alabama, Georgia, and Tennessee. The, two districts are often referred to as the Arkansas field and the Appalachian field. Of these two the Arkansas field has been by far the largest producer, and at present over 90 per cent of the bauxite production of they United States comes from the Arkansas field. The bauxite industry in the Appalachian field had its beginning in 1889, and since that time the total production of the states of Alabama, Georgia, and Tennessee has been, nearly a million tons. The production of bauxite in this field has languished in the last five, or six, years, and In 1927 its production was only about 14,000 tons, according to Harder4. The recent decrease in production is due mainly to the fact that many .of the known deposits of commercial-grade ore have become exhausted. There are, however, considerable quantities of low-grade bauxite in the Appalachian field, but these have not been available because there has been no satisfactory way of concentrating low-grade bauxite. The quantity, of low-grade material in the Appalachian field is probably, fully as large as the tonnage of commercial ore which the field has already produced.]

Jan 1, 1928

By W. E. Robinson

Oil-shale samples selected from a core of the Green River Basin (Wyoming) were studied to ascertain differences in the composition and/or chemical structure of the organic material in the samples relative to stratigraphic position within the Green River Formation. This involved a systematic study of the soluble organic material and the insoluble kerogen present in the samples. Emphasis was placed upon the distribution of the alkanes (normal and isoprenoid compounds) in the soluble extract and upon the aromaticity of the kerogen. In general, it was concluded that significant differences exist in the chemical structure of the oil-shale organic material from various strata within the Green River Formation of Wyoming. Most of the compositional and structural changes were not related to burial depth but were related to source material variations, environmental differences, or other factors.

By I. N. Beall

The present survey indicates 'that the average volatility of motor gasoline now being marketed throughout the country falls well within the limits of Federal Specifications. As would be expected, there is a slight decrease in volatility as compared with the gasoline marketed last wine:., but on the average the gasoline sold today is about the same as that sold last summer. During the past five years the Bureau of Mines has made semi-annual surveys of the gasoline marketed in the United States. To obtain a sample of each gasoline sold is obviously impracticable, but the cities in which samples have been collected have been so chosen as to be representative of the more important marketing territories. It is believed, therefore, that the samples obtained are indicative of the quality of gasoline marketed throughout the country.

Jan 1, 1925

By E. C. Lane

The motor gasoline that is being marketed in the United States this winter is practically the same 'as that sold a year ago. In fact, there has been little char sin this commodity during the year, as the gasoline sold last summer was almost as volatile as that marketed last winter. Boring the past eight years, the Bureau of Mine's has made semi-annual surveys of the gasoline marketed in the United States, the survey just completed being the fifteenth in the series. The cities in which samples have been collected have been chosen as representative of the more important marketing territories as it is obviously impracticable to obtain a sample of every gasoline sold in the entire country.

Jan 1, 1927

As part of the overall development of a borehole mining system -develop backfilling techniques to reduce possible damage to the environment caused by either the cavities or the piles of sand tailings that result from in-borehole hydraulic mining. (Borehole mining is described in technology News No. 56.) Approach Water filled cavities at the bottom of boreholes are rapidly and economically backfilled by jetting a sand-tailings slurry underwater. How It Works The Bureau of Mines borehole mining system creates a cavity having a horizontal diameter of more than 50 feet. (See photograph). This cavity can be backfilled with much of the sand previously mined. The sand tailings or similar backfill material is dumped by a front end loader into a slurry mixing tank at the rate of about one ton every three minutes. Enough water is added to give a thick, but pumpable slurry. The slurry is pumped down the borehole through a string of 4-inch pipe to the cavity. After passing through a right elbow at the end of the pipe, the slurry is ejected through a nozzle. The resulting slurry jet emplaces the backfill at the outer wall of the cavity. To obtain an even distribution of fill in the cavity, the nozzle is slowly rotated. The nozzle and pipe assembly is supported from a turntable on the surface. See diagram.

Jan 1, 1981

By John C. Edwards

The Bureau of Mines has developed a time-dependent droplet vaporization model (in the absence of forced convection) that can be applied to the vaporization of liquid Halon 1301 droplets (vapor pressure at 300 K = 14 atm) sprayed from an extinguisher. It was found that rapid surface vaporization quickly lowers the droplets' surface temperature very near to the boiling temperature, and the vaporization becomes diffusion controlled. Although the lifetime of the droplet is proportional to the square of the initial radius of the droplet, the elapsed time prior to complete droplet vaporization is not proportional to the square of the droplet radius, as an equilibrium model would indicate.

Jan 1, 1982

By T. G. Carnahan

The Bureau of Mines conducted research to simulate in situ leaching of a porphyry copper sulfide ore. The purpose was to determine the effects on copper leaching of additions of NaCI to a conventional sulfate leach system and to analyze the oxidant requirements and the oxidation products that resulted from leaching of the sulfide minerals in the ore. Baseline sulfate and sulfate plus 2-pct-NaCl-leach-solution experiments employing 167-kg (367-lb) and 152-kg (333-lb) charges, respectively, were conducted. The minus 25.4-cm (10-inch) ore was leached at 90° C under flooded conditions with 2.8 MPa (400 psig) of oxygen bubbling through the system. Sixty-seven pct of the copper was extracted in 1,236 days of leaching in the NaCI experiment, whereas 47 pct of the copper was extracted in 913 days of leaching in the baseline experiment. Diffusion into and out of the ore fragments controlled the rate of leaching, which precluded enhancement of the leach rate by the chloride ions. The calculated oxygen consumption was 3.17 kg/kg of copper extracted in the baseline experiment and 3.46 kg/kg of copper extracted in the experiment to determine the effect of chloride ions.

Jan 1, 1982

Reduce longwall shearer operators' dust exposures by more effectively suppressing the dust generated by the upwind cutting drum. Approach Direct more of the shearer water supply to the upwind drum, thus reducing the shearer operator's exposure to respirable dust while making more efficient use of water. How Proportioning Permits More Efficient Use of Water On most longwall mining operations, the cutting action of the shearer drums is the primary source of dust. Al-though the amount of dust generated is directly related to the amount of coal and rock cut by the drum, the exposure or the shearer operators to dust depends more on their work position relative to the upwind drum. When cutting with the airflow, the upwind drum, cutting bottom coal and floor rock, is the primary generator of dust reaching the operators. The lead drum is downwind of both shearer operators and is thus of less concern. (See diagram). When cutting against the airflow, the lead drum is upwind-taking a full cut, including roof rock-and both shearer operators may be exposed to very high levels of respirable dust. Currently, water sprays mounted on the cutting drum provide the most effective method of controlling dust from longwall shearer drums, and all longwall mining operations use some type of bit flushing or cavity filling water spray system on the cutting drums. Bureau surveys of longwall operations, conducted as part of its research program to reduce respirable dust, have indicated that six longwalls with better than average compliance records use higher than normal water flowrates to the cutting drums. The average water flow to the shearers at these six operations was approximately 60 gpm-about 50 percent more water than is normally supplied to double-drum longwall shearers.

Jan 1, 1982