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By D. J. Frey

While costs of most commodities and services have increased markedly over the past 25 years, the cost of electricity has steadily declined. One of the reasons for this price decline is the improved efficiencies of generating plants which is shown in Fig. 1. 1,2 Another reason for this is the decline in coal production costs. Efficiencies for the best plant increased from about 32 percent in 1540 to about 40 percent in 1962 and then decreased slightly to 38 percent in 1965. The increase in efficiency for all plants (US average) has been even more notable, progressing from less than 15 percent in 1940 to about 32 percent in 1965. The chief reason for the improved efficiency is the change in operating steam temperatures. These increased about 12 F per year until 1200 F was reached in 1962. At this high temperature excessive corrosion of super-heater and reheater tubes was experienced and steam temperatures were dropped back to 1050 F and even 1000 F in some cases. To successfully compete against other energy sources for generating electricity, this corrosion problem must be solved so that operation at higher temperatures and thus, increased efficiencies will be possible.

Jan 1, 1967

By SAMUEL A. LOLON, ADITYA JUGANDA, JURGEN F. BRUNE, JR. GREGORY E. BOGIN

Historically, there have been many events of mine fires and explosions recorded in the United States and other countries that have demonstrated the existence of explosive methane-air mixtures, herein referred to as explosive gas zones (EGZs) [1]. The risk of mine explosions can increase if these EGZs migrate out from the gob into the surrounding mine entries — a phenomenon known as gob breathing. A number of 3D computational fluid dynamics (CFD) simulations using various magnitudes and periods of barometric pressure variation have indicated that the EGZ outgassing potentially occurs due to lags in pressure, which are strongly influenced by mine conditions and ventilation systems. Early-warning systems with real-time pressure monitoring and the application of gob ventilation boreholes are recommended to detect and mitigate explosion hazards from gob outgassing.

By Jürgen F. Brune, SAMUEL A. LOLON, ADITYA JUGANDA, Gregory E. Bogin Jr

Historically, there have been many occurrences ofmine fires and explosions recorded in the United States and other countries that have demonstrated the existence of explosivemethane–airmixtures, herein referred to as explosive gas zones (EGZs). The risk of mine explosions can increase if the EGZs migrate out from the gob into the surrounding mine entries. Fluctuating barometric pressure is the common cause for EGZs outflowing or outgassing from the gob. Numerical analysis using a 3D computational fluid dynamics method was developed to fully understand the outgassing phenomenon. A number of simulations using various magnitudes and periods of barometric pressure changes indicated that the EGZ outgassing potentially occurs due to lags in pressure, which are strongly influenced by mine conditions and ventilation systems. An early warning system with a real-time pressure monitoring and the application of gob ventilation boreholes are recommended to detect and mitigate explosion hazards from gob outgassing.

Aug 24, 2020

By Polezhaev S. Yu, I. V. Ukraintsev, Boduen A. Ya, Saburbayeva L. Yu

"Comparison studies of different technologies are performed when selecting optimum option for gold ore and concentrate processing. Methods of ultrafine grinding, oxidizing roasting, bacterial leaching and pressure oxidation are used to extract gold from refractory ores and concentrates. Refractory gold flotation concentrate produced from pyrite-arsenopyrite ores of Bestobe deposit is a case study in this paper. The results of the experimental tests of the direct leaching of flotation concentrate and pre-oxidation products using different methods (oxidizing roasting cinder, pressure oxidation and bacterial leaching cakes) are the following: - cyanidation of original flotation concentrate provides recovery of Au at 46.6 %; - oxidizing roasting increases gold recovery from 46.6 % to 85 %; - BIOX increases gold recovery up to 86 %; - preliminary pressure oxidation of flotation concentrate ensures steadily high Au extraction in the follow-up cyanidation at 94.9-96.5 %. Pressure oxidation and bio-oxidation has changed dramatically the strategy of refractory gold ore processing. These solutions provided for development of ore deposits that considered earlier non-commercial. However, refractory ore processing has a complex character in terms of developing process flowsheet and requires large amount of studies to be performed for each new project. Gold extraction is the basic but not the only criteria to technology selection for gold ore and concentrate processing. Opex and capex, ore reserves, regional geography, developed infrastructure and skill personnel should be considered. Process studies and feasibility study of the developed technology shall be provided for each specific gold ore deposit. INTRODUCTION Due to changes in available feedstock and depletion of easy-to-process ores, refractory ores containing finely disseminated gold and silver in sulphides (primarily, in pyrites and arsenopyrites) are more and more involved into processing. Experts say that such ores amount above 40 % of the world’s gold reserves. Conventional technologies of gold extraction from refractory ores include flotation, roasting and cinder cyanidation (Fraser etal., 1991). However, today’s best available practice for refractory gold ore processing are bacterial (BIOX) and pressure (POX) oxidation."

Jan 1, 2018

By S. Tuylu, D. Adiguzel, A. Bascetin, E. G. Savas, O. Ozdemir

"Paste Technology has some advantages comparing to other surface disposal methods. With this method, it is possible to pump high concentrated solid materials to very long distances without segregation problem. However, it is known from Literature that pumpability of materials is completely related to rheological properties of the materials. For this reason, in this study, the rheological parameters (e.g. yield stress and viscosity values) of the paste material prepared from Pb-Zn tailings at various solid ratios (60-85%) were obtained in order to determine the pumpability of the paste material. Additionally, slump tests, which are usually used in mining industry, was carried out. Finally, regression analysis was made between the slump values and rheological parameters of the paste material to find a correlation between two independent parameters. The results showed that there is a great correlation between the slump values and the yield stress of the material. On the other hand, there was no correlation with viscosity: ty=430.28-16.877Sv (R2= 0,94; ty: Yield Stress (Pa), Sv: Slump Value (cm)). Based on the results obtained from this study, it can be clearly concluded that the slump values obtained from a simple test can be used to predict yield stress values of paste materials. INTRODUCTION Recently, surface disposal of mining tailings has become one of the biggest problems in mining industry in terms of environmental issues. Therefore, several researches have been focused on this subject in order to find a best solution or method for this problem. These studies showed that paste technology has some advantages compared to other conventional methods. Tailings thickened to the extent show no segregation of particles during transportation, and relatively small amount of settling occur post-deposition which are often called “paste” (Cincilla et al. 1997). Paste tailing technology has two applications in the industrial area as underground paste fill and surface paste disposal. Paste tailing technology was first started to be used in Grund mine, Germany in the late 1970s (Grice, 1998). Process tailing material, water and - if needed - cement materials, which are the components of the paste, must be blended to obtain a homogenous mixture suitable for pumpability. Consistency behavior of the paste material is determined using a conventional sedimentation cone concrete test (slump). Meanwhile, the slump value of the paste must be between 200 and 250 mm for surface applications (Newman et al., 2001). Additionally, in the case of underground paste system, the optimum slump value must be between 150 and 200 mm. On the other hand, the water content and density of paste at certain slump value change depending on the amount of fine particles in the tailing sample. While moisture of the material will be high, its density will be low because of surface area of particles which increases with decrease in particle size (Meggyes and Debreczeni, 2006). For pumpability of the paste to long distances, slump value of the paste must be good enough to be accepted for use of surface paste disposal. Paste material has a yield stress because they show non-Newtonian behavior and generally is classified as a Bingham plastic fluid. (Cooke, 2008; Theriault, 2003). In addition, the appropriate viscosity value of the paste along with the yield stress must be between 100 and 250 Pa (Bascetin et al., 2013; Bascetin et al., 2014; Bascetin et al., 2015)."

Jan 1, 2016

By J Zhou, X Bi, Y Yan, W Peng, H Yang, D Weng, P Li

Fortescue Metals Group (FMG) fines from Western Australia is a hematite and limonite mix characterised by high crystal water content. Due to its higher supply capacity and lower prices, the Wuhan Iron and Steel Corporation (Group) intended to use more FMG fines in the sinter mix. It is understood that sinter quality is closely related to its microstructure featured by the hardness and brittleness of different mineral phases, the content of micro pores, and trans-cracks. In order to maintain sinter qualities such as tumble index, reducibility and so on at higher FMG fines blend ratios, a research project was initiated to study the effects of the FMG fines blending ratio on sinter microstructure. Research results showed that at higher FMG fines ratios, the hardness of hematite and magnetite were both decreased while the hardness of calcium ferrite showed a tendency to decrease. The number of cracks that were generated during Vickers hardness measurement in various mineral phases decreased, but their length was shortened, and the variation of crack lengths increased. The contents of hematite and magnetite were also reduced and the reduction of magnetite was clearer. Also the content of calcium ferrite and pores rose and the magnitude of the increase of pores was greater. Among all the mineral phases in sinter cakes, the Vickers hardness of hematite was highest within the range of 879 N/mm2 ~ 942 N/mm2, and therefore the decrease of its content in sinter and the enhancement of its brittleness, ie the number of cracks increased, were harmful to sinter strength. In addition, the excessive increase in pores content is also not favourable to sinter strength.CITATION:Bi, X, Yan, Y, Zhou, J, Peng, W, Li, P, Yang, H and Weng, D, 2013. Study of sinter microstructure with various blend ratios of Fortescue Metals Group fines, in Proceedings Iron Ore 2013 , pp 331-336 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 12, 2013

By A. Koizhanova

Kumistinskoye gold- and silver bearing ores (Republic of Kazakhstan) as well as standardized test solutions containing gold, silver, copper, zinc and iron were studied. The best results in silver and gold recovery from Kumistinskoye gold- and silver bearing ores were achieved through use of complex cyanide-thiosulfate solutions as compared to individual cyanide solutions and thiosulfate solutions. It was found that such complex solutions substantially step up leaching process herewith increasing precious metals recovery rates. Thermodynamics of studied chemical processes was calculated. Reaction order, kinetic constant and activation energy of gold leaching process through use of cyanide-thiosulfate solutions were identified. We managed to prove that the sorption rates and holding capacity in process of gold anions recovery with anionite AM-2B are comparable to sorption characteristics for cyanide solutions. Keywords: gold, silver, copper, zinc, iron, cyanide-thiosulfate solutions, anionite AM-2B

Sep 1, 2012

By D. M. Wyslouzil

"This paper was prepared for presentation at the 16th Canadian Mineral Processor's Annual Meeting, Ottawa, Ontario, Jan. 17 to Jan. 19, 1984.This paper gives an account of the development of treatment procedures for the differential flotation of refractory copper-zinc ores. Special references are made to the effectiveness of various zinc depressants and their combinations.Studies carried out on refractory copper-zinc ores demonstrated that conventional zinc depressants such as cyanide and zinc sulphate were not particularly effective when secondary copper minerals were present in the ore; the flotation activity of sphalerite was enhanced in the presence of cyanide.Among the various zinc depressants evaluated, the following depressant combinations were found most effective: Zn(OH) 2-S02 , 802-CaO, Na2S-Na2S03-S02, Na 2 S-S02 and Na 2S-S0rDS22.The practical application of any of these systems depends on the type of ore treated and other conditions such as pH, levels and points of collector and depressant additions.In this paper the effect of each depressant combination on different ores is described with reference to the selection of collectors."

Jan 1, 1984

By Guolin Zheng, Jian Pan, Deqing Zhu, Xianlin Zhou

"In ferronickel production, nickel oxide and part of the iron oxide are reduced to metal by agglomeration and smelting in blast furnace. Due to the physical and chemical properties of the laterite ores, a large fraction of fines is generated during the pre-treatment stages and the strength of agglomeration is weakened, which results in low productivity and bad quality. In this paper, the process of pelletization of nickel laterite was developed, and some parameters to strengthen the pelletization of nickel laterite have been optimized. The results show that the compressive strength of fired nickel laterite pellet can reach over 2000 Newton per pellet while firing at the temperature of 1220 °C~1250 °C in 12 min. The product pellet can be used as high-quality burden for blast furnace to manufacture ferronickel.IntroductionIn recent years, the global stainless steel market was developed exuberantly, which greatly promoted the needs of the basic raw material of stainless steel smelting - metal nickel. Currently nickel sulfide ores are only 40% of global nickel reserves, but offer 60% of all the nickel production. However, with the deficit of resources, the nickel sulfide ore (high grade ore) is depleting, so there is an increasing focus on the utilization of low-grade nickel laterite. Recent research has focused on the wet treatment process to utilize nickel laterite, and less on the use of other technologies [1-8]. The economical and efficient technology relies on the reduction of nickel oxide and part of the iron oxide metal by agglomeration and smelting in blast furnace in China. Some domestic steel companies have adopted this process [9, 10]. Unfortunately a large fraction of fines is generated during the pre-treatment stages and the strength of agglomeration is weakened, which results in low productivity and bad quality of fired pellets. In this study, the process of pelletization of nickel laterite was developed firstly, and some parameters to strengthen the pelletization of nickel laterite have been optimized, and the product pellet can be used to produce stainless steel and ferronickel alloy by blast furnace."

Jan 1, 2011

By Patricia Negrini Siqueira Poveda, Leonardo G. A. Silva

Thermoplastic materials are sensitive to ultraviolet radiation (UV), which can cause structural changes, causing variation in mechanical properties and appearance. UV range between 250 and 400 nm is considered the most aggressive to polymers, and prolonged exposure to it results in breakage and/or crosslinking chains. Light stabilizer additives, blockers or absorbers are added to the polymers for protection in order to extend the life of the final product. The choice of the adequate light stabilizer additive system depends on factors such as resin final application, thickness, geographic location of exposure, presence of fillers in the composition, contact with chemicals, among others. This study evaluates different additive systems: conventional organic, inorganic nanotechnologyc base and the synergy between them when applied to polyethylene considering carbonyl index and UV/VIS results after aging by QUV chamber.

Mar 1, 2017

By Cleusa Cristina Bueno Martha de Souza

Hydrometallurgical techniques for processing metals are becoming an efficient method for recovering metals. Although batteries' manufacturers have got rid of mercury content, some efforts have been made for recovering other metals enclosed in the battery formula. This paper discusses the bench scale experiments in the purification process of leached solutions from alkaline spent batteries. After leaching process using sulfuric acid as leachant, the solutions containing Fe, Cd, Pb, MIl, Zn and K were neutralized to precipitate iron hydroxide. In a second step, the purification experiments were carried out with excess of zinc dust to try to remove Cd while Mn and Zn still remain in the solution to be recovered in an electrolysis stage. The purification experiments procedures were conducted at different temperatures and times to find out properly conditions from the viewpoint of metals removal After filtration the solutions were submitted to chemical analysis to certify the metals content extracted.

Jan 1, 2001

By S. M. Geerts, M. T. Wild

In this paper the performance effects of various shaped charge liner designs will be discussed. Several different charges will be tested and the liner design will be reviewed based on the performance in testing. The first type of shaped charge to be tested is a conical charge with dual confinement. For the purpose of this paper, dual confinement is a shaped charge with two liners but containing one explosive charge. Several charges with different dual confinement designs will be tested. Variations in configuration include charges with similar angle and similar diameter. The second type is a double conical shaped charge configuration. A double shaped charge will be considered to be two complete charges formed into a single cone. The goal of the project is to determine if any of the designs increase the efficiency and/or effectiveness of the shaped charge in comparison to the standard conical shaped charge. A standard conical charge will be detonated against a witness plate to get a standard depth of penetration or a baseline. All charges will have a seven cone diameter standoff, allowing the data to be compared to the control charge. Computer modeling will be used to predict the results of the testing that will be conducted. The actual results will be compared to the computer simulation for validation.

Jan 1, 2010

Under the AMIRA P9 project the three-product cyclone-an off-shoot of the conventional hydro-cyclone-that produces three distinct products has been developed. The three-product cyclone shows great promise as a classifier in mineral processing. Industrial and pilot plant trials performed to assess its performance in the classification of the UG2 platinum ore, indicate that the presence of an extra overflow product stream that captures the mid-sized particles, provides improved classification efficiency. To assess the split on component density, samples from the feed and product streams were screened and assays by size for chromite (? = 4.8) and silica (? = 2.65) were obtained. Results from tests performed using this type of hydrocyclone in a number of applications indicates that it can be applied successfully in circuit configurations where the conventional hydrocyc-lone is not suitable. Utilising the three-product cyclone to classify the UG2 platinum ore resulted in an intermediate overflow product stream containing the mid-sized low density silicates and relatively fine high density chromite particles while the finer overflow contained mostly fine silicates and chromite particles. The coarse chromite and silicates reported to the underflow. Due to the increased number of products, the method of using efficiency curves was extended to cater for the increased number of products in the three-product cyclone. Although significant differences in the classification performance of the three-product cyclone were noticed with variations in machine variables a consistent method of assessing the performance was applied. The efficiency curve was adopted and applied and separate efficiency curve properties were obtained for each product stream. The methodology was applied to the component data, and efficiency curve proper-ties for each key component were obtained and compared. This paper discusses the application of the efficiency curve to cyclones producing more than two products and extending the methodology to the different components in the feed.

Jan 1, 2014

By S. N. Monteiro, E. B. Zanelato, J. Alexandre, M. T. Marvila, A. R. G. Azevedo, G. C. Xavier

The incorporation of industrial waste into ceramic tiles is a major trend in the search for alternative raw materials, and also in the search for environmentally correct disposal of waste. In order to evaluate the effect of the incorporation of residues from the ornamental stone industries, in the properties of ceramic tiles, incorporations of up to 40% by weight of the residue in ceramic mass were studied. It is noteworthy that this residue is constituted basically by limestone and its characterization was performed by grain size analysis, Atterberg boundaries, grain density and chemical analysis by X-ray fluorescence. The specimens were burned at 800 °C and the following properties were evaluated: linear retraction, water absorption and bending rupture stress. The results indicated that the residue of ornamental rocks is a material with potential to be used as a component in the mass of red ceramic tiles.

Mar 1, 2018

By Maria das Graças da Silva-Valenzuela, Mathilde Julienne Gisele Champeau Ferreira, Simeão Lopes Ferreira, Francisco Rolando Valenzuela-Díaz

The use of clays to formulate powder coating can improve physical properties, besides a final product with more sustainable characteristics due to the elimination of some additives, which may be substituted for the clay. We investigate the use of a modified smectite clay to formulate powder coating based on polyester resin. Four compositions of incorporated claywere evaluated (0, 4, 7, and 10wt%). Powder coating were prepared in a twin-screw extruder at 105 °C, and characterized by XRD, FTIR and SEM. Tests of flexibility, adhesion and impact strength in accordance to ASTM standards were performed. Diffractograms of the samples showed the characteristic peak of the modified smectite in d(001) * 37°(2h), indicating exfoliation of the clay. Micrographs by SEM showed the presence of lamellar structure for the clay-based powder coating.Mechanical assays were found for all analyzed coatings, indicating that sample containing 7% of clay presents the best performance.

Mar 1, 2018

By Zhihe Dou, Jiang Liu, Ting-an ZHANG, Yukun Huang

The paper aimed to propose that mixed rare earth concentrate was decomposed by pressurized calcification where mechanical milling was applied simultaneously (also known as mechanochemical calcification). The bastnaesite and monazite were both decomposed by OH−, where released rare earth formed RE (OH)3, released fluorine and phosphorus formed CaF2 and Ca2P2O7. Then, the calcified slag was leached by diluted hydrochloric acid to extract rare earth and both recover fluorine and phosphorus. The phase transformation regularity, the behavioral trends of rare earth, fluorine and phosphorus were investigated. Results showed under the optimal conditions of ball to material weight 80:1, the calcification temperature 250 °C, the liquid-solid ratio 5:1, the leaching yield of rare earth reached to 92.16%, Ce was 86.47%, La was 97.58%, Nd was 99.99% and the mass fraction of F, P entering into calcified liquor were 8.27, 0.21% respectively. The micromorphology of the mineral has a transition from dense to fluffy, and then became dense again.

Mar 1, 2018

By Jorge Alberto Soares Tenório, Denise Crocce Romano Espinosa, Beatriz Peralta Oruê

Manganese, a toxic mineral, related to manganism may have high added value for the steel industry. The difficulty in obtaining manganese encourages the exploration of new secondary sources such as the lateritic nickel effluent. In Brazil, nickel reserves are predominantly lateritic, making the country a potential producer. For the tests, a synthetic solution was used which simulates the lateritic nickel effluent from leaching. The oxidative precipitation with ozone occurred at the oxygen flow rates: 0.5; 1.0 and 2.5L/min, at the original pH 1.5 at 21°C in a 500 mL bubble column reactor. O3 was produced in the benchtop generator feed by 99% oxygen. The ozonation time was determined by the oxidation potential1.55V. The ozonated solution was centrifuged and filtered. The filtrate and collected samples were characterized in ICP-OES. Optimization tests with ultracentrifuge were performed. The best precipitation reached 97% at 0.5L/min O2 at 6.07 ± 0.045mg/min of O3 dosage and resulted in a solution 10-15mg/L Mn+2, above 1mg/L, maximum value acceptable by Conama 2011, to be retreated before being discharged into the water body or being reused as a manganese source.

Oct 3, 2019

By K. Wu, X. Yuan, R. Du, C. Chao

"Lump coals are currently employed to replace part of coke in the COREX melter-gasifier for ironmaking. In order to optimize the process, the pyrolysis kinetics of Datong coal used in the COREX process was studied. A sectioning method is proposed to overcome certain shortcomings of traditional methods for studying the pyrolysis of coal. Based on the sectioning method and the characteristics of the coal pyrolysis process, the temperature range was divided into three intervals. In the first, the adsorbed gas and water of crystallization were removed; in the second, the coal was transformed into semi-coke; and finally, the semi-coke was further coked. Three models of reaction were then established to study the different stages of the pyrolysis process: an interfacial chemical reaction model, a random pore model, and internal diffusion with shrinking volume. The results showed that the experimental data fitted the models well, with all correlation coefficients (r2) exceeding 0.97. Finally, the mechanisms of reaction and kinetic parameters for each temperature range were derived, which laid a necessary foundation for optimizing the usage of non-coking coal in the COREX process. IntroductionIn view of environmental concerns and the shortage of good-quality coking coal, the COREX process was designed as a new ironmaking technology, attracting wide attention (Fang et al., 2005). In this process, lump coal and a small quantity of coke are directly charged into the melter-gasifier, where a high-quality reducing gas is generated for the reduction of the iron ore (Kumar et al., 2009). In contrast to the conventional blast furnace (BF) process, non-coking lump coal is used as the reducing agent and as the energy source, and the iron charge consists of lump ore and/or pellets, which results in the elimination of the coke oven and sintering plant as well as a decrease in investment (Kumar et al., 2009; Liu et al., 2012).Although the COREX process has made great progress, in current production practice the energy consumption greatly exceeds that of the BF, and it requires a certain amount of coke to maintain permeability of the semi-coke bed (Wang et al., 2008). In addition, the process consumes a lot of good-quality lump ore and lump coal. The pyrolysis of coal is the first step in most coal conversion processes, such as carbonization, gasification, and combustion (Aboyade et al., 2013). The reaction behaviour of lump coals in the COREX melter-gasifier is crucial, as it determines energy utilization and gas composition, as well as the metallurgical properties and particle size of the semi-coke produced (Prachethan et al., 2011; Zhang et al., 2014). In order to optimize the process and improve its competitiveness, the pyrolysis kinetics of Datong coal used in Baosteel’s COREX C-3000 facility was studied."

Jan 1, 2016

By Jefferson Caponero

The tire is an expressive component of Municipal Solid Waste, manly when its occupied volume is considered. Its treatment by pyrolysis stands for a list of advantages, such as: landfill releasing and a production of a high quality fuel. The exploitation of new natural resources is becoming more difficult each day, basically due to the environmental damages caused by this type of activity. This work presents a study on the thermal behaviour of Brazilian tires using thermogravimetric analysis and differential thermal analysis, in order to optimise the pyrolysis process of tires. Samples of I to 2 mm were investigated at atmospheres of nitrogen, argon, oxygen and mixtures of these gases at temperatures up to 1273K, under heating rates between 1 to 50 Klmin . The results showed that the behaviour of each sample is related to both the atmosphere composition and the heating rate.

Jan 1, 2001

By Sayan Sarkar

HAMR (Hydrogen Assisted Magnesiothermic Reduction) process is a promising alternative route of titanium production, which is convenient due to reduction at relatively lower temperatures below 750 °C and usage of cost-efficient TiO2 as the starting material. A crucial step involved in this process requires the Mg reduction of TiO2 subjected to H2 atmosphere which produces porous TiH2 along with residual magnesium impurities. Before the final heat treatment and deoxygenation steps for consolidation of the Ti powder, leaching plays a significant role in the removal of Mg impurities. In this report, we present a systematic study on the role of acid concentration (HCl), temperature and the kinetics of MgO dissolution. In addition, we also report the controlling mechanism during kinetics of MgO dissolution in acid. This parametric study will provide a platform to ensure very low Mg content that meets with ASTM standards during production of Ti in the HAMR process.