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By J. F. MacGregor, M. Hou, D. Hodouin

"RésuméDe nouvelles méthodes efficaces sont maintenant devenues nécessaires pour traiter les quantités massives de données en temps-réel que collectent les ordinateurs industriels modemes. Les méthodes statistiques multi variables comme l'analyse en composantes principales et la projection sur des structures latentes sont des méthodes analytiques bien adaptées aux données industrielles bruitées et mal conditionnées. L'efficacité de ces méthodes est illustrée sur des données historiques collectées dans une usine de broyage et de flottation. Trois cent cinquante observations de quarante quatre variables de procède ont été utilisées pour démontrer les aptitudes de ces méthodes pour l'analyse préliminaire de données, la classification des régimes opératoires, le contrôle de qualité et la modélisation empirique des precedes.AbstractBecause of the availability of powerful industrial computers which collect huge amounts of real-time data in mineral processing plants, there is a need for efficient methods to extract relevant information from them. Multivariate statistical techniques, such as principal components analysis (PCA) and projection to latent structures (PLS), are well suited to analyze these large sets of noisy and ill-conditioned data. The power of PCA and PLS is illustrated on historical data from a grinding and flotation plant. Three hundred and fifty observations of forty-four process variables are used to show the capacity of these techniques for preliminary data analysis, classification of operating regimes, process monitoring, and process empirical modelling."

Jan 1, 1993

By G. Nino de Guzman, L. C. Woollacott

The isotherms that are usually taken to represent the force 'driving' the adsorption in carbon-in-pulp processes may change from contactor to contactor. This paper reports on an investigation into the extent to which this Isotherm shift is Influenced by the changes in oxygen and cyanide concentration that occur in operating plants. The impact of the isotherm shift on the reliability of simulation results is examined.

Jan 1, 1993

By William A. Macaitis, Frank E. Dalton, Leo R. DiVita

The Metropolitan Water Reclamation District of Greater Chicago's Tunnel and Reservoir Plan (TARP) is a multi-purpose urban public works project with a total cost of $3.7 billion. Currently 51 miles of TARP tunnels are completed and operational and 34 miles are under construction. The excavated TARP tunnels have been constructed in rock utilizing 29 tunnel boring machines, ranging in size from 6.5 to 35.3 feet in diameter.

Jan 1, 1993

By B. R. Baldock

The converting of high-grade nickel matte for production of low-sulphur matte or nickel metal is a process which has eluded metallurgists in the past because of the limitations of conventional converting furnaces. The high temperatures required and the refractory nature of nickel oxide has prevented practical success in a process which has been known to be theoretically feasible for a long time. The Ausmelt top submerged lancing system is capable of operating under close control of the smelting conditions. High temperatures and both rapid oxidation and rapid reduction can be achieved. These features have provided the basis for successful pilot plant trials of the desulphurisation of high-grade matte from the Kalgoorlie Nickel Smelter. Sulphur level in product was lowered from 20 to 25% to as low as 0.2%, with iron levels in matte in the range of 1.0 to 3.5%. The theoretical background of matte desulphurisation is surveyed and the pilot plant operations described. The implications of the results in relation to commercial plants and possible refinery operations are summarised.

Jan 1, 1993

By C. A. Silva

Ladle change-over, during continuous casting of steel, initiates transient flow in the tundish which influences the inclusion content and degree of mixing between two consecutive batches of steel. The mixing behavior in the tundish during this period is determined by the casting rate and the ratios of: inflow to outflow during the refilling period; and, the low liquid level relative to the nominal level in the tundish during the transiency. A 3:10 scale water-model of a typical one strand slab caster was operated in conjunction with a tracer technique to characterize the velocity fields for several combinations of these parameters. Steady operation, a limiting case of the transiency, provided a basis for comparison. High-order moments -- skewness and kurtosis -- of the residence time density function have been utilized as signature elements associated with a particular residence-time distribution for the system. A simple mathematical model incorporating the above parameters as well as a characteristic Peclet Number was successful in simulating the features of the transient period.

Jan 1, 1993

By G. Kazonich

The high costs and environmental problems associated with making iron and steel in the United states is driving the development of new technologies to replace the blast furnace. A prototype reactor incorporating rocket technology was designed and built. This rapid rate reactor was operated successfully and consistently made iron metal. Minus 32s-mesh magnetite particles could be reduced to iron metal in less than 50 ms in a high temperature flow through reactor. Iron product was recovered inside the reactor and in a downstream cyclonic separator. The results of typical operation and how parametric changes affected the reduction of iron ore concentrates are discussed.

Jan 1, 1993

By Tullio Corsini

Scrap battery recovery process, developed by Engitec Impianti S.p.A., is improved transforming batches operations in continuous. Benefits expected: constant and better quality of the products; easier and more reliable control of the operating parameters, reduction of manpower requirements. Paste will content less sulfate, particularly in soluble form. Sodium sulphate is obtained with higher and constant purity.

Jan 1, 1993

By P. Peczak

A Monte Carlo simulation technique has been used to study dynamic recrystallization in polycrystals. A continuum microstructure of the polycrystal is modeled employing a discrete lattice. The response of the material to hot deformation is simulated by adding stored energy and recrystallization nuclei continuously with time. The experimentally observed nonuniform character of deformation substructures is modeled by employing a phenomenological expression for inhomogeneous distribution of the stored energy. All simulations were performed on HP-Apollo 9000 Series 700 workstations. A program written in FORTRAN with use of PHIGS graphics library calls was used to interactively monitor the current state of the matrix and all relevant parameters: deformation stress, average grain size and effective nucleation rate. Visual analysis of the simulated microstructure allows a better understanding of the data developed by averaging over a number of very long Monte Carlo runs. Since the essential features of dynamic recrystallization are accurately reproduced by the model, it is used to discuss the role of the controlling mechanisms of the dynamic recrystallization in real polycrystal.

Jan 1, 1993

The Tom, East and West zone, stratiform Zn-Pb-Ag deposits at Macmillan Pass, Yukon, Canada were discovered by Hudson Bay Mining and Smelting Co Ltd prospectors in 1951. Further exploration, including two phases of underground exploration produced an HBM&S calculated reserve of 9.28 Mt of 7.5 per cent Pb, 6.2 per cent Zn and 69.4 g/T Ag for these zones. Cominco Ltd optioned the property in 1988. Deep, surface drilling extended the West and Southeast zones downward 200 - 300 m, indicating an additional potential resource of several million tonnes of good grade. The magnitude of the controlling syndepositional setting suggests that mineralisation continues to greater depth but with increased drilling and possibly mining costs. The 30 x 60 km Macmillan Fold belt trends WNW across the NW Selwyn Basin and Cordilleran trend. Within the fold belt, the Central Block - a complex, rift controlled basin of Devonian siliciclastics, hosts seven zones of Pb-Zn-Ag mineralisation clustered about four hydrothermal centres. The centres, distributed over 24 km, are coincident with small syndepositionally active structural sub-basins. The Tom deposits, in one such sub-basin, are localised by a third order structure consisting of two palaeobathymetric troughs flanking a syndepositional horst. This structure caused drastic facies and thickness changes over 600 metres of strata and focussed the venting of hydrothermal fluids through permeable conglomerates in the horst and its flanking growth faults. Mineral facies are zoned, with Pb-Ag contents rapidly diminishing outward from the vent resulting in restricted areas of high grade Pb-Zn-Ag-Ba ore within more extensive, sub-economic, Ba-Zn mineralisation. Widespread iron carbonate alteration of the footwall and high Si, B and Zn values in the hangingwall 'fingerprint' the deposit and along with the distinct facies variations provide aids to exploring the Tom and like deposits.

Jan 1, 1993

By Guarascio M, Massacci P

In process simulation, more reliable prediction of industrial results and evaluation of data for design purposes and process optimisation may be attained by the combined use of: the modelling and simulation of ore characteristics, and 2. the modelling and simulation of the process. It is well known that geostatistical methods allow the defining of models of orebodies in which the variables considered are the grades of the valuable components. These models are proper for reserve estimation, geostatistical contouring, design and simulation of the exploitation method, and, in addition, for evaluating the variability of the ROM which is expected to be fed to the processing plant. However, no data are normally incorporated in the orebody model in order to evaluate the ore characteristics relevant for a reliable process simulation. The procedure for process simulation aimed at predicting plant results normally used so far consists in collecting samples from different orebody sites and building up a so-called 'representative sample'. On this sample, the ore characteristics (eg liberation, washability, grindability, etc) and the processing tests are referred to as the 'average behaviour in the orebody', assumed constant. A more reliable methodology consists in collecting samples from different orebody sites, in performing tests to characterise the samples from the point of view of the process (ore patterns), and in using synthetic parameters (process features). The values of the parameters are processed using geostatistical methods in order to develop a model for simulating the feed to the process. The estimation may thus be referred to the amount of recoverable minerals instead of to the existing minerals. Furthermore, the selection of the processes, the sizing of equipment and the design of control devices, as well as the prediction of results, become more accurate and reliable.

Jan 1, 1993

By Marcelo Jimenez Bustos

The Chagres Smelter was the first in Chile to follow environmental regulations to control sulfur dioxide emissions. Because of this, the operation and development plans have had to incorporate environmental planning as part of its policies for almost three decades. The present article shows the development of the environmental standards applied to its operations, investments and operational improvements carried out to meet the regulations and improve competitiveness. Results to-date and future plans are outlined, as well as their impact on operations and the environment.

Jan 1, 1993

By Don Rapp, Rufus Flinchum

Air blast and flyrock are two of the most critical concerns facing the blaster of today. This paper will provide the blaster with proven procedures for recognizing open face and bench surface problems, explain various surveying methods, and provide the mathematical formulas for calculating and designing proper hole placement and explosive load configuration. A concept called "Pattern Footage" is utilized in conjunction with a USBM study to develop blast designs aimed at minimizing air blast and flyrock. In addition to this main focus, this concept can be used in shot displacement and cast blasting design.

Jan 1, 1993

Prevent the explosion of methane gas or coal dust by replacing air with inert gas inside highwall mine excavations. Approach Use combustion gases as a source of inert gas with low oxygen content to blanket the cutting, head of highwall mining machines. This gas is placed strategically at the collar of the excavation where it enters the hole to replace the mined coal volume. The elimination of oxygen from the hole prevents explosions of gas or dust. How It Works Highwall mining methods arc used when surface mining becomes uneconomical. One method of highwall mining involves use of a horizontal auger to enter the coalbed from a surface mine bench. The coal is mined in a series of horizontal, parallel, and large-diameter holes. Historically, little methane has been associated with auger mining. However, mining technology has extended the reach of auger mining, which can increase the occurrence of methane. Methane explosions at auger mining operations have been increasing. Methane has been the primary fuel source of these ignitions, but coal dust also may have been involved.

Jan 1, 1993

By Joel L. Morrison

The preparation of coal-water slurry fuel (CWSF) has the potential to be a commercially viable technology for the coal industry. The technology base required to prepare stable CWSF using grinding circuits has been developed over the past decade and is now being applied to the preparation of CWSF from wet coal fines which are generated during coal beneficiation. When preparing CWSF, the optimum CWSF formulation must be determined to ensure that the fuel will be stable while having acceptable atomization and combustion properties, and the production run must be monitored closely to ensure that the CWSF quality is maintained. This paper describes the CWSF formulation process, CWSF preparation circuits, and some of typical problems encountered in, and solutions to, the transportation and storage of CWSF.

Jan 1, 1993

By A. S. Rao

In the original roast-leach-electrowin (RLE) circuit at the Chambishi Cobalt Plant, commissioned in 1978, the separation of nickel and zinc from cobalt in aqueous streams was achieved by successive stages of precipitation using lime. However, this technique was not able to meet the increasingly stringent metal quality requirements of customers whilst maintaining acceptable process recoveries. Intensive process development work was carried out and, in July 1988, an ion exchange circuit for nickel removal was commissioned using DOW XFS 4195 resin and for the first time Z.C.C.M. produced high purity cobalt metal containing less than 0.10% nickel. Following further work, a solvent extraction circuit for zinc removal, using DZEHPA, was commissioned in February 1991 in order to enhance cobalt recovery by reducing co-precipitated cobalt losses. This paper outlines the process development, design, commissioning and subsequent operation of these nickel ion exchange and zinc solvent extraction circuits.

Jan 1, 1993

By Ximena Diaz

Mercury is one of the most undesirable contaminants in gold bearing ores. During cyanidation mercury cyanide compounds accompany gold in all the extraction and recovery processes. Of course mercury in the carbon eluates creates environmental problems in subsequent refining steps. One possible process alternative for the separation of gold from mercury in such concentrated alkaline cyanide solutions is the selective solvent extraction of gold by undiluted Dibutyl Butyl Phosphonate (DBBP). In order to describe the behavior of mercury during extraction by DBBP, the results from a preliminary research program are presented. In this study, temperature and cyanide concentration have been found to be the most significant variables which influence the separation of gold from mercury by solvent extraction using DBBP. It was found, using plant eluate from a carbon strip, that excellent separation of gold from mercury can be obtained at 60' C with 98% gold recovery and complete mercury rejection in a single stage of extraction. The influence of pH is also discussed in terms of the extraction chemistry. These results complement previous research which described the DBBP solvation extraction of an aurocyanide ion pair. In addition, these results extend our understanding of the alkyl phosphorous ester extraction systems by illustrating that neutral ionic species such as Hg(cN)02sq, can be extracted at low cyanide concentrations, a phenomenon which had not been observed previously for other cyanoanions.

Jan 1, 1993

By D. W. Fuerstenau

One of the more energy-efficient methods for size reduction, namely particle-bed comminution under high compressive loads, was employed to grind eight minerals and ores, using up to 250 MPa pressure. A new approach based on the self-preserving character of the ground product size distributions and a linear energy-reduction ratio relationship is proposed for analyzing this mode of size reduction. The grind ability of the material when comminuted in a particle bed is about one-half that of the single-particle crushing mode, which is in agreement with previous estimates of the relative efficiencies of energy utilization based on direct measurements of surface area produced. The loss of efficiency may be attributed to energy dissipation by particle interaction phenomena in compressed beds.

Jan 1, 1993

By Charles J. Zablocki, Robert J. Kamilli

"Abstract - Buried, possibly mineralized granite cupolas at the Silsilah tin deposit in Saudi Arabia (lat. 26°06' N, long. 42°40' E) have been successfully located using a closely spaced electric-field-ratio profiling technique. In this study, electrical fields at 27 and 270 Hz across grounded electrodes spaced 50 m apart were measured along six traverses. This method is interpretable by inspection, unlike the dipole-dipole technique, which requires mathematical modeling for interpretation.In the study area, the technique allowed the authors to identify and distinguish among unroofed granite cupolas, cupolas with their aplite-pegmatite apical contact zones intact, strong (quartz-rich) and weak (relatively quartz-poor) greisens, dikes, faults, and pervasively argillized rocks.This method should be useful in the valuation of other shallow mineral prospects in similar settings in other parts of the world, especially deposits for which the location of vertical contrasts is important, such as veins or mineralized zones associated with the apexes of small igneous cupolas."

Jan 1, 1993

By L. Blain

In practice, geochemical analyses can be grouped in two broad categories according to their aim. Those that seek to determine the exact chemical composition of geological materials fall under the heading of assays, whereas applied geochemistry concerns itself with the detection of anomaly contrasts. Recent trends have blurred the distinction between both approaches for many users, as methods that were traditionally used for assays are being adopted in applied geochemistry and assays make increasing use of instrumental techniques. Nevertheless. it is important to keep a clear distinction between the two types of analyses because it has immediate practical consequences, cost is the most obvious, as well as fundamental implications. In the broadest terms, the goal of geochemistry is to strike an optimal balance between throughput and accuracy, at the lowest reasonable cost, while assays strive for accuracy. Traditionally, complete silicate analysis has been the concern of assayers whereas exploration geochemists have been more interested in base metal analyses where acid extractions of the elements, without dissolution of the silicate matrix, has been the norm. This kind of distinction is less realistic now, especially with the growth in lithogeochemical studies, and some overlap in methodology is unavoidable. However, where such overlaps occur the distinction remains in the emphasis of the work. A commonly used example is that although HF acid preparations are used by both, the emphasis in applied geochemistry is on sample throughput and batch analysis, whereas assayers are more concerned with the range of elements to be determined (Thompson and Walsh, 1983).

Jan 1, 1993

By H. W. Renner

The paper industry is an $80 billion/year business that is the largest consumer of industrial minerals. Paper industry generally refers to paper and paperboard products, including pulp mills. Grades and uses of paper and paperboard are very diverse, including such things as napkins, paper plates, corrugated boxes, magazines, newsprint, currency, and copier paper. Only about 40% of paper utilizes industrial minerals as fillers or coating materials. Minerals are used for both functional and economic reasons. Most often, minerals such as kaolin clay and calcium carbonate are used to improve print quality, brightness and opacity of paper. The minerals can be added as fillers into the paper in the wet end of the papermaking system, or can be applied as part of a coating to the paper. Coated papers are the highest quality paper, being used for magazines, advertising brochures and annual reports. Common uses for filled uncoated paper are books, copier paper, envelopes and many of the Sunday newspaper advertising inserts.

Jan 1, 1993