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By K Katov, S T. Ciutina, J D. Pyke

The development and optimisation of mill discharge trommels, and specifically their screen panels, can be a neglected area in the complex operation of a minerals processing plant. Trommels are often seen as a ‘set and forget’ component of the circuit, even when significant improvements in design are possible. A redesigned trommel and panel arrangement has simplified and added flexibility to the plant shutdown schedule at Kirkland Lake Gold’s Fosterville Gold Mine in Central Victoria.Prior to the trommel redesign, the shutdown frequency was determined by the expected life of trommel panels at 14 weeks. Planning downtime around this item led to higher maintenance costs and wastage in other areas of the plant. This was particularly disruptive with respect to mill lining change-outs, which were forced out of sequence and often changed prematurely. Fosterville Gold engaged Metso Australia Limited to propose a new trommel design that would better suit the site. The new trommel was engineered to balance simplicity with performance, and incorporated the latest in Modular trommel design, modelling and Finite Elemental Analysis (FEA). Modular Panels and Spiral Segments achieve significantly longer life, and allow in-situ panel change outs, flexibility in spiral and dam positioning and an improvement in classification performance. Trommel panel life has significantly increased from 14 to 71 weeks in the trommel’s highest wearing zone. The new design has eliminated some risks to safety by reducing manual labour and lifting requirements during shutdowns. There is greater flexibility with respect to shutdown requirements. The site is no longer at the mercy of trommel panel lifespan, which allows for better optimisation of wear components in the circuit. CITATION:Pyke, J D, Katov, K and Ciutina, S T, 2018. Modular SAG mill discharge trommel for maintenance flexibility and performance, in Proceedings 14th AusIMM Mill Operators' Conference 2018, pp 613–620 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 29, 2018

By M L. Muller, A R. O’Donnell

The Mount Isa Mines (MIM) Copper Concentrator has an extensive history of reagent trials, with different reagents coming in and out of favour over the years. The research and use of carbon depressants is particularly prevalent, as carbonaceous pyrite is a major source of concentrate dilution. Years of research led to the use of naphthalene sulphonate due to its excellent carbon depression properties. However, due to rising reagent costs carbon depression ceased in the late 1990s. This led to the loss of knowledge about the use and value of naphthalene sulphonate. Cyanide is used at the Copper Concentrator for the sole purpose of pyrite depression and over the years multiple projects have been devoted to finding alternatives to it. In 2012 the neighbouring MIM Lead-Zinc Concentrator replaced cyanide with naphthalene sulphonate which resulted in cost savings and the elimination of a hazardous reagent. In 2013, plant trials were conducted at the Copper Concentrator in hopes to replicate the outcomes obtained at the Lead-Zinc Concentrator. The results of the trials conducted at the Copper Concentrator showed that naphthalene sulphonate could not replace cyanide and this work was set aside to pursue more promising projects. Further research conducted in 2014 found that mineralogy and a better understanding of the depressing mechanism of naphthalene sulphonate held the key to improved pyrite depression at the Copper Concentrator. The findings showed that Mount Isa copper ore contains two forms of pyrite; euhedral pyrite (cubic pyrite) and framboidal pyrite (carbon rimmed spheres of pyrite), both of which require different reagents to sufficiently depress them. Naphthalene sulphonate was found to be an excellent carbon depressant, suitable for depressing graphite and framboidal pyrite, whilst cyanide specifically targets euhedral pyrite.In 2015 laboratory test work was conducted to examine the use of naphthalene sulphonate in conjunction with cyanide to selectively target both forms of pyrite. This work led to a full plant trial, the results of which showed a significant increase in plant performance, with higher copper concentrate grades and recoveries being achieved. This paper aims to focus on the benefits and importance of understanding past work and linking a detailed knowledge of feed mineralogy to reagent selection for improved plant outcomes.CITATION:O’Donnell, A R and Muller, M L, 2018. Selectively targeting hydrophobic gangue minerals at the Mount Isa Mines Copper Concentrator, in Proceedings 14th AusIMM Mill Operators' Conference 2018, pp 413–421 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 29, 2018

By A Price, D Okle, K Brooks

The operation of flotation plants has been improved over the years by use of fundamentally based design techniques, a better understanding of reagent chemistry, online metal analysis and the use of digital control systems. However, optimal operation of flotation banks is not consistently achieved using manual operation. The reason for this is that the system is a highly interacting one, with changes in air addition, cell interface level and reagent dosages all being available, without it necessarily being clear as to which change should be made for a particular situation.This situation is made more complex by the fact that the feed to a flotation bank can vary in flowrate, composition and density over a fairly short period of time. It is not possible for a human operator to reject these disturbances, given the extent of the operation that is typically being monitored.Model predictive control (MPC) is a control and optimisation technique, developed in the oil refining industry, that aims to manage just such interacting multiple input multiple output (MIMO) systems. This technology makes use of linear dynamic models of the plant, that are experimentally derived. These models are then used in a receding horizon strategy to determine an optimal trajectory of the inputs to the system.MPC has been applied to four areas of the lead zinc flotation unit at Mount Isa mines. A total of 31 cells are being controlled by the system, which varies air to the cells, levels and reagent addition on a minute-by minute basis. The MPC controls concentrate and tail grades, reagent dosages, as well as recoveries to ranges set by the plant metallurgists.The development of the MPCs is discussed, together with the benefits realised. The key factors in insuring an ongoing return on investment are described.CITATION:Price, A, Okle, D and Brooks, K, 2018. Glencore Mount Isa lead zinc flotation circuit – experiences from the implementation of model predictive control, in Proceedings 14th AusIMM Mill Operators' Conference 2018, pp 101–110 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 29, 2018

By T D. H McGrath, W P. Staunton

Benchmarking, comparing an operation or process with the industry standard, is known to be a useful method for identifying plant optimisation opportunities, and in many cases providing the pathway to realise the benefits. The difficulty is generating the database of plant data necessary for a benchmarking exercise. Larger companies can benchmark internally; this option is not available to smaller companies, and the full value can only be realised with a comprehensive “industry wide” approach.The Gold Technology Group at Curtin University through the AMIRA P420 series of projects has undertaken several comprehensive metallurgical industry surveys in the gold industry over the last two decades. Analysis of these surveys has demonstrated areas where many operations can benefit from re-assessment of their operating practices.This paper will review the work undertaken by the Group in this area, in particular the 1999 surveys of gold companies in the Australasian region, and the 2012 international survey of the industry. The challenges of, and opportunities arising from these surveys will be discussed. Some of the highlights from analysis of these databases will be presented as well as noting changes in processing practices observed by the Group over the last 20 years.CITATION:McGrath, T D H and Staunton, W P, 2018. Keeping up with the Joneses – the value of industry surveys and benchmarking, in Proceedings 14th AusIMM Mill Operators' Conference 2018, pp 509–516 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 29, 2018

By E Ruhanen, S Kauvosaari, M Kosonen, C Meintjes

The Yara Siilinjärvi plant is located in the central part of Finland. Siilinjärvi is Western Europe's only apatite mine and annually it produces 1 Mt of apatite concentrate, which creates approximately 10 Mt of tailings.At the beginning of 2017, tailings handling in Yara Siilinjärvi was brought to a new era, by replacing the conventional tailings storage facility with a new tailings treatment plant. The new high-density tailings disposal system with two paste thickeners increased the percentage of solids in the slurry from 45–48 per cent to 66-68 per cent, making it possible to deposit as a paste. This extended the life-span of the current tailings storage facility by 15 years; from 2020 to 2035.This paper presents the storyline of the Yara Paste Plant Project. The project began with laboratory testing and then progressed to pilot-scale thickening and beaching trials. After some successful pilot trials, the final process design was implemented. Process instrumentation and automation played a key role in the project, as the aim of the Yara Project was to make the plant operable remotely from the main plant. An advanced control system is needed to maintain process stability and the desired operation point in various operational circumstances.This paper discusses the results from the Yara site since the new tailings treatment plant commenced. Some of the main points are that the operation has been running consistently with an underflow solids content of 66-68 per cent, with average beach slope angles of 3.5 degrees in the tailings disposal area. This control system additionally facilitates minimum use of flocculant, which delivers significant savings to operating costs. Robust thickener operation also leads to the trouble-free high-density pumping and high availability of the Paste Plant. During the first year of operation, the plant’s availability has been very good, over 97 per cent.Currently, the plant still has its own staff working there during the daytime, but the Paste Plant is now already operated remotely during the night shifts. The long-term goal is to gradually transition into operating the plant completely remotely.CITATION:Ruhanen, E, Kosonen, M, Kauvosaari, S and Meintjes, C, 2018. Optimising the operation of paste thickening at the Yara Siilinjärvi Plant, in Proceedings 14th AusIMM Mill Operators' Conference 2018, pp 297–310 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 29, 2018

By L Mikhael Gurieff, D Baas

The Phu Kham Copper-Gold Operation (Phu Kham Operation) is located in the Lao People's Democratic Republic and is owned and operated by the Lao-registered company, Phu Bia Mining Limited (PBM). Australian-headquartered copper and gold producer, PanAust Limited holds a 90 per cent interest in PBM; the Government of Laos owns the remaining 10 per cent. The Phu Kham Operation was commissioned in 2008 with an initial concentrator nameplate throughput of 12 million tonnes per annum (Mt/a). Subsequent improvement projects, including the Phu Kham Upgrade Project (PKU), completed in 2012, and the Phu Kham Increased Recovery Project (IRP), completed in 2013, increased the design throughput to 18 Mt/yr. In 2016, the actual mill throughput exceeded 19 Mt/a, this throughput is budgeted to be maintained until the end of 2020.The concentrator flotation circuit upgrade, completed during the IRP, called for a non-selective bulk sulphide concentrate to be generated from the rougher circuit. This in turn caused the mechanical flotation cells in the cleaner circuit, particularly those in the second cleaner bank, to become volumetrically overload. The overload reduced the cleaner circuit performance to approximately 92 per cent copper recovery at a 23 per cent copper concentrate grade, below the expected 95 per cent recovery. This bottleneck restricted copper units entering the plant to approximately 14.5 tonnes per hour (t/h) due to uncontrolled recirculating load build-up in the mechanical cleaning circuit.Maintaining the operating methodologies would have led to a copper production shortfall beyond 2016, to address this shortfall the Phu Kham Operation looked to optimise the Jameson Cell and mechanical cleaner circuit performance. The work included fundamental application of flotation practice and modelling, mineralogical analysis, bubble size analysis, plant surveys and test work. The results were used to develop and implement an innovative automated control system strategy incorporating flotation theory and operating strategies. The automation has the ability to quickly adapt to disturbances in the circuit and maintain optimised performance with little or no intervention by flotation operators.Upon completion, cleaner recovery increased to 95 per cent at a final concentrate grade of 23 per cent copper, and copper units entering the plant increased to 17.5 t/h.CITATION:Baas, D and Mikhael Gurieff, L, 2018. Developing flotation circuit control and automation for the Phu Kham Copper-Gold Operation concentrator, in Proceedings 14th AusIMM Mill Operators' Conference 2018, pp 37–58 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 29, 2018

By B Wong, R G. Coleman

In flotation, the selection of the size, number and type of cell for a particular duty depends on two important factors. Firstly, the required flotation residence time and secondly, the physical constraints of how much concentrate can be recovered for a given froth surface area and concentrate lip length. The residence time is influenced by ore type and characteristics such as liberation, kinetics and reagent dosage. The amount of concentrate that can be recovered for a given froth surface area and lip length depends on ore type and other characteristics such as particle size, specific gravity and mineral grade. Residence time is determined through a combination of laboratory-scale test work and design scale-up factors. However the critical froth transport parameters such as froth carry rate and froth lip loading cannot be determined in a laboratory. This is because the froth is scraped during a laboratory flotation test and thus does not exhibit natural behaviour, and it is not possible to scale-up froth transport distance or air rate. These values are generally compared via calculation to rule-of-thumb maximum values to establish if these values will be exceeded by the flotation cell selection.This paper first reviews these critical froth transport parameters and then discusses actual parameter values across diverse operating sites, with varying cell duties, cell sizes and types, orebodies and particle sizes. These values are compared against the industry rule-of-thumb to test the applicability of the rule-of-thumb to actual performance. Options are also presented for adjusting these parameters in operating flotation cells.CITATION:Coleman, R G and Wong, B, 2018. Flotation launder design and the measurement of critical froth transport parameters, in Proceedings 14th AusIMM Mill Operators' Conference 2018, pp 353–362 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 29, 2018

By J K. Claflin, S R. La Brooy, A M. Claflin

Rotary kilns have been in service in the gold industry to regenerate carbon for 65 years. At the time oxide ores with gold head grades of 8 to 10 g/t were being treated. Carbon could be regenerated adequately at 650°C and solution losses were less than 1%. Forty years ago, research indicated that heavily fouled carbon from flotation circuits had to be held at 750 to 850°C for ten to twenty minutes for full reactivation (Avraamides and La Brooy, 1987), gold head grades were typically 5 g/t and solution losses typically 0.02 ppm – still less than 1%. In 2017 it was determined (Claflin et al., 2017) that a residence time of less than 1 minute at 750°C can be adequate to reactivate carbon fouled with organics sufficiently to achieve 0.005 ppm solution losses in a flotation tailings leach plant.With the potential for discovery head grades to drop below 0.6 g/t, solution losses of 0.02 ppm represent over 3% loss. Tight operation of the whole carbon circuit is required to keep gold solution losses below 1% going forward.There are alternatives to a rotary carbon kiln, e.g. vertical kilns of which the Minfurn, Rintoul and Combustion Air kilns are examples. The alternative kilns can be heated using electrical heating elements, induction, and microwave. These kilns can operate successfully under the right conditions, however, they are almost exclusively for small carbon throughputs and are not suitable for the large carbon advance rates that are required to process low head grade ore deposits. Large throughput carbon kilns are are almost exclusively fossil fuel fired rotary kilns and the subject of this paper. In the view of the principal author, a fossil fuel fired vertical carbon kiln is preferred to a rotary kiln, however, it is not currently used in the industry.Thermal regeneration of activated carbon has a major impact on gold recovery in the carbon circuit. The carbon kiln and associated equipment constitute 3 to 5% of the capital cost for an oxide processing plant and up to 10% of the capital cost if flotation tails are leached. Despite the capital cost and impact on recovery, the carbon kiln is often poorly selected, operated and maintained.Six years ago Ausenco embarked on the Carbon Kiln Initiative to reduce solution gold losses. This body of knowledge has been published in a series of papers culminating in this paper on how to:1. Select a kiln appropriate for the flowsheet;2. Maintain the kiln to achieve design operation; and3. Operate the kiln to minimise costs and maximise reactivation.CITATION:Claflin, J K, La Brooy, S R and Claflin, A M, 2018. Carbon kiln selection, operation and maintenance, in Proceedings 14th AusIMM Mill Operators' Conference 2018, pp 251–274 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Aug 29, 2018

By Osmar de Sousa Santos

NiTi shape memory alloys (SMA) have been widely used as construction materials due to their shape memory and superelastic properties. Usually the application of the NiTi alloy is in the wire form, which is ideal shape to make springs, orthodontic arc-wire and endodontic files. Since our research group (ITASMART) started producing NiTi wires, it was noticed that NiTi SMA produced by Vacuum Induction Melting (VIM) presents carbon contamination, which is due to the melting process. Therefore, alloys rich in carbon remove titanium from matrix, forming precipitates of TiC (titanium carbide). Also, Ti2Ni precipitation removes titanium from the matrix and these two precipitates TiC and Ti2Ni can produce internal volumetric defect in the wire drawing process. Seeing the importance of NiTi wires as base of many applications, this work studies the formation of volumetric defects caused by precipitates in the wire drawing process of a NiTi wire drawn down to 0,39 mm in diameter.

Aug 8, 2018

By Tadeu Castro da Silva

As ligas Ni-Ti com composição em torno de 55% de Ni em peso sofrem influência nas temperaturas de transformação de fase quando submetidos a tratamentos térmicos de recozimento na faixa de temperatura de 300ºC a 500ºC. O objetivo do presente trabalho é avaliar a influência do tratamento térmico de recozimento a 350°C onde os CP´s de uma liga NiTi mantidos por tempos de 10 minutos, 1 hora e 24 horas. Os efeitos do tratamento são avaliados com base nas temperaturas de transformação de fase, medida por meio de Calorimetria Diferencial de Varredura (DSC). Os resultados revelaram o maior aumento das temperaturas de transformação de fase para amostra com menor tempo de resfriamento em relação a amostra sem tratamento térmico.

Aug 8, 2018

By Gilberto Álvares da Silva

New elements have been inserted in NiTi lately, resulting in ternary alloys with specific characteristics beyond Shape Memory Effect and Superelasticity. Among all others alloying elements, the Ag additions itself gives potential antibacterial activity to that smart material. So on, the elaboration procedures of ternary NiTiAg alloys was studied in order to obtain a melting procedure to ensure further studies on this alloy. Microstructural and thermal analyses were used to evaluate the VAR-remelting production of NiTiAg with 4.0% wt silver content. The microstructure is composed by a NiTi matrix, pure Ag precipitates, and, scarcely, TiC inclusions. Heat treatments at high temperature could not dilute those Ag particles, but could lead to the precipitation of new ones. The silver element reduces the temperature of the martensitic transformation, yielding a material with superelastic behavior, beyond induces the R-phase on cooling stage of this alloy.

Aug 8, 2018

By Niédson José da Silva

Ligas com memória de forma (LMF) são materiais ativos que apresentam como característica a resposta a impulsos externos, recuperando deformações aparentemente plásticas. Esses materiais têm forte potencial aplicativo como atuadores termomecânicos em diversos setores industriais, sendo de interesse o aperfeiçoamento de suas propriedades termomecânicas. A conformação mecânica do ECAE (Equal Channel Angular Extrusion) resulta em melhorias quanto às propriedades mecânicas destas ligas. Esta melhoria está relacionada à redução de tamanho de grãos devido ao cisalhamento interno que estes sofrem ao passar pelos canais interceptantes, apesar de não ocorrer nenhuma alteração na área da seção transversal do corpo de prova. Neste trabalho, realizou-se a fabricação de ligas com memória de forma da família NiTi e da matriz para a extrusão em canal angular. A conformação mecânica foi realizada numa máquina de ensaios universal. O resultado desse estudo foi a observação da melhoria das propriedades mecânicas e alteração das temperaturas de transformação, as quais são essenciais para a utilização do efeito de memória de forma. Essa análise se torna relevante quando da aplicação desse tipo de material em situações em que se requer elevada resistência mecânica aliada a eficácia dos fenômenos de memória de forma.

Aug 8, 2018

By Tatiane Potiguara Oliveira

O compósito metal-cerâmico Al2O3 – Cu alia as propriedades de baixa densidade, alta resistência ao desgaste, dureza e biocompatibilidade da fase cerâmica alumina a excelente condutividade elétrica, e alta tenacidade do cobre metálico. Tal compósito pode ser aplicado como ferramenta de corte, entre outras. Este trabalho discute a influência da moagem de alta energia na microestrutura e densificação do compósito Al2O3–Cu. Pós de Al2O3 e Cu na razão de 5% em massa de Cu foram moídos por até 100 horas em moinho planetário de alta energia. A razão em massa de pó para bola usada foi de 1:5. O álcool etílico foi usado como solvente. Na moagem, amostras de pós foram colhidas após 2, 10, e 50 horas. Pós moídos foram prensados uniaxialmente em matriz cilíndrica a 100 MPa e sinterizados a 1.300°C por 1 hora sob atmosfera de Ar e H2. A taxa de aquecimento foi de 10°C/min. Análises de DRX, AG caracterizaram os pós moídos. O MEV e o EDS foi empregado para observar a microestrutura das partículas dos pós moídos e dos corpos sinterizados. Um pequeno tamanho de partícula da fase cerâmica e uma estrutura mais homogênea são produzidos quando os pós foram moídos até 100 horas.

Aug 8, 2018

By Vera Lúcia Othéro de Brito

Literature has shown that spinel Co-Mn ferrite have potential application in magneto-mechanical sensors, due to its relatively high magnetoelastic sensitivity. In this work, Co-Mn ferrite was processed by means of the ceramic method, using Fe2O3, MnO and Co3O4 as raw materials. Samples were liquid-phase sintered, using Bi2O3 additive as liquid-phase former. X-ray fluorescence analysis was carried out in the raw materials in order to evaluate their impurity content. Atomic absorption spectrometry analysis was used for quantifying the Co/Mn/Fe proportion in the ferrite. The microstructure of the sintered sample was analyzed by means of Scanning Electron Microscopy. The magnetization and magnetostrictive behavior of the ferrite were evaluated, obtaining curves for magnetic hysteresis, magnetostriction and magnetoelastic sensitivity. The impurity inclusions and the Bi-rich particles formed from the liquid phase were characterized. The sintered ferrite had a total magnetostriction of -126ppm, which is lower than the values reported in literature for a Co-Mn ferrite of similar composition. It was verified that sintering was carried out within a critical temperature range, in which the decomposition of Mn ferrites may occur when sintering in air. This decomposition affects the magnetic properties of the material, and it may be avoided by using controlled sintering atmospheres.

Aug 8, 2018

By Sara Silva Ferreira de Dafé

Os aços com um alto teor de Mn (15-30%) e os elementos de liga, Si e Al, apresentam plasticidade excepcional devido à geração de maclas de deformação (efeito TWIP) ou múltiplas transformações martensíticas (efeito TRIP). Este trabalho avaliou a evolução microestrutural, a formação da textura e sua influência sobre o comportamento mecânico de um aço contendo 17%Mn-0,06%C laminado a frio com reduções de 45% e 90%, e recozimentos a 700°C durante tempos diferentes. A microestrutura foi analisada por microscopia óptica e eletrônica de varredura, EBSD e difração de raios X. A redução um frio favorece a formação da martensita a'. No aço recozido estão presentes as fases martensita a? e e e austenita. O limite de escoamento e de resistência à tração alcançaram 750 e 950 MPa, respectivamente, com o alongamento total de 45%, confirmando sua alta capacidade de encruamento. A reversão da martensita para austenita ocorre simultaneamente com a recristalização desta.

Aug 8, 2018

By Ana Maria Gontijo Figueiredo

Muitos dispositivos biomecânicos têm sido produzidos com ligas superelásticas (SE) de NiTi. Na maioria das aplicações, o material é submetido a solicitações mecânicas cíclicas, tornando seu comportamento sob fadiga um parâmetro importante. Neste trabalho são apresentados resultados de ensaios de fadiga por flexão rotativa de um fio SE, ensaiado a seis temperaturas diferentes, sob amplitudes de deformação (?a) variando de 1% a 12%. As curvas mostram que a vida em fadiga do material na fase martensítica estável (ME) é cerca de 100x maior do que na fase austenítica estável (AE). A curva do fio SE se aproxima da curva do fio AE para pequenas ?a e, com o seu aumento, se aproxima da curva do fio ME quando ?a aumenta. As superfícies de fratura obtidas foram observadas ao microscópio eletrônico de varredura e foram calculadas as áreas correspondentes à fratura por fadiga (af). Os resultados mostram que, para o fio nas fases AE e ME, af decresce continuamente com o aumento da ?a. Para o caso do fio SE, af permanece relativamente constante para valores intermediários de amplitude de deformação (2% a 8%). Para uma mesma deformação, af cresce com a redução da temperatura, com o consequente aumento do número de ciclos para falha.

Aug 8, 2018

By Leandro de Arruda Santos

O objetivo deste trabalho foi avaliar o comportamento mecânico sob flexão de um instrumento endodôntico constituído de Ni-Ti M-Wire e comparar suas respostas com aquelas obtidas de um instrumento de Ni-Ti superelástico convencional com a mesma geometria, utilizando-se simulação por elementos finitos. Um instrumento ProTaper Universal F1 foi selecionado para este estudo. O modelo geométrico para a simulação numérica foi gerado através de micro-tomografia computadorizada e os dados para os modelos constitutivos foram obtidos por meio de ensaios de tração realizados em laboratório. A simulação numérica foi realizada em ABAQUS, com condições de contorno baseadas na especificação ISO 3630-1. Os resultados mostram que instrumentos de Ni-Ti M-Wire apresentam maior flexibilidade e menores valores de tensão quando submetidos à flexão, o que indica que estes instrumentos são mais resistentes à fadiga por flexão.

Aug 8, 2018

By Daniel Luiz Rodrigues Júnior

O presente trabalho avalia o efeito da indução máxima sobre a energia dissipada por histerese magnética em amostras de aços elétricos de grão não orientado. Tal relação foi descrita por Steinmetz como uma lei de potência cujo expoente tem valor 1,6. No entanto, esta lei falha quando aplicada a uma ampla faixa de induções magnéticas. Com o objetivo de se avaliar a aplicabilidade dessa equação chapas de aço elétrico foram caracterizadas. Ciclos de histerese foram extraídos com indução máxima variando entre 0,4 e 2,2 T com frequência 5 mHz. A área no interior dos ciclos corresponde à energia dissipada. Estes resultados mostraram uma diminuição do valor do expoente para induções entre 1,2 e 1,6 T. Este fato pode ser explicado pela estagnação do valor do campo coercivo nessa faixa de dados.

Aug 8, 2018

By Paulo Sergio Olivio Filho

A aspersão térmica é utilizada para produzir revestimento quando há necessidade de aumentar a vida útil de sistemas e peças, podendo ser também utilizada na recuperação delas, em alguns casos. Com o intuito de compreender melhor o processo de aspersão térmica por chama a pó, o objetivo deste trabalho é analisar os fatores influentes no aumento de espessura depositada pelo processo, utilizando o delineamento de experimento de Taguchi para avaliar os fatores e níveis dos fatores que geram as melhores condições de aplicação para o revestimento. Para isto, foram escolhidos três fatores de controle com três níveis cada um, dos quais foi possível seu controle em laboratório. A deposição foi realizada em chapas de aço SAE1020, e revestida com pó de alumínio não atomizado. A seção transversal dos revestimentos foi analisada por microscópio ótico. Os resultados dos experimentos foram analisados através de estatística descritiva, gráfica e análise pelo delineamento de Taguchi, baseada na análise de Sinal/Ruído. Sendo evidente que os fatores do processo são estatisticamente significativos: número de passes, fluxo de nitrogênio e a taxa de alimentação de pó. Esta análise se mostrou eficaz, gerando os resultados esperados para otimização dos parâmetros do processo.

Aug 8, 2018

By Rodrigo Perito Cardoso

Low-temperature nitriding of stainless steels is applied to obtain wear resistant surfaces without losing its corrosion resistance. The treatment consists in introducing nitrogen into the steel surface avoiding chromium nitride precipitation. The corrosion resistance of martensitic stainless steels is expected to be improved if the treatment parameters are correctly selected. It can be related to ?Fe2-3N and a'N phase formation on the treated surface. In the present work the influence of the pretreatment and treatment temperature on corrosion resistance of plasma nitrided AISI 420 steel samples is studied. Annealed, as-quenched and 400ºC-tempered samples were nitrided at 300, 350, 400, 450 and 500°C, for 6 h at 600 V. The pressure was 3 Torr and the gas mixture was composed of 70%N2, 20%H2 and 10%Ar, at a gas flow rate of 3.34×106 Nm3s-1. Plasma was generated using a square-wave pulsed DC power supply and the sample temperature was controlled by the duty cycle. The modified layers were characterized by optical microscopy, X-ray diffraction and microhardness measurement. The corrosion resistance was studied by electrochemical characterization, by means of Open circuit potential and Anodic polarization curves. The maximum surface hardness was achieved at 400°C. This temperature seems to be near the limit temperature for low-temperature treatment aiming to improve or at least to keep unaltered the corrosion resistance in relation to that verified for non-treated steel samples. Results confirm that the pretreatment and treatment temperature significantly affects the corrosion resistance of the treated surface.

Aug 8, 2018