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By Fabiana Fonseca de Morais

A sinterização é um dos mais importantes e mais antigos processos de aglomeração da indústria metalúrgica. Entender a realidade atual do processo de sinterização e as qualidades requeridas para o sínter é primeiro passo para o desenvolvimento de equipamentos ou processo. Este trabalho visa entender o impacto das diferentes características de minério e resíduos empregados em uma sinterização, seu comportamento na qualidade do sínter e a sugestão de equipamentos para amenizar problemas encontrados. Parâmetros como CaO/SiO2, SiO2, Al2O3 e MgO são avaliados para entender a tendência do mercado e o efeito na qualidade final do sínter. A correta avaliação das necessidades da planta para otimização dos equipamentos a matéria-prima disponível se faz necessário para o melhor resultado no alto-forno. A granulometria da matéria-prima também é um ponto importante a ser analisado. O sinter feed tradicionalmente possui uma maior fração entre 0,7 e 6 mm, uma fração menor entre 0,2 e 0,7 mm e um conteúdo de ultrafino (<0,150 mm) limitado a 15%. Estudos identificam uma tendência do sinter feed com maior conteúdo de sílica e o consequente aumento da utilização de ultrafinos. Como resposta ao incremento de ultrafinos na sinterização as grandes siderúrgicas já estão investindo em equipamentos que minimizem grandes perdas de produtividade, como a instalação do misturador intensivo, utilizado em projetos da Pau Wurth. Outra solução inclui a instalação de uma mini-sinterização dedicada para receber este material mais fino e resíduos. O sínter produzido poderá ser adicionado diretamente no forno e/ou ser utilizado como nuclueante na sinterização grande para aumento de sua produtividade.

Aug 16, 2017

By Leandro de Almeida

As curvas limite de conformação (CLC) são utilizadas há mais de 50 anos. Propostas inicialmente para o desenvolvimento de produtos provenientes da indústria automobilística, em função das necessidades apresentadas pela indústria de estampagem elas são aplicadas atualmente de maneira geral na produção de inúmeros tipos de peças, oferecendo previsões de possíveis falhas e/ou defeitos durante as etapas do processo de estampagem. As CLC´s permitem prever o afinamento excessivo, enrugamento, estiramento e é claro, a fratura da peça. A raiz da curva limite de conformação (CLC0) é considerada como a mínima deformação obtida pela curva, ou seja, a obtenção de deformações superiores pode levar a peça a falha. As ligas de latão compostas por cobre e zinco, são utilizadas em inúmeras aplicações que necessitam de excelente estampabilidade, como o repuxo profundo, objetivado na fabricação de projéteis. Desta forma, torna-se interessante o entendimento da CLC ou CLC0 para liga de latão em estudo. A obtenção da CLC0 através de ensaios de tração uniaxial no plano da chapa pode ser realizada de acordo com corpos de prova de formatos específicos, como os propostos por Björklund e Nilsson (2014), IRSID (1975) e Wagoner (1980 e 1981). Concluiu-se que o corpo de prova proposto pelo IRSID (1975) é o que melhor se apresentou na determinação das deformações e1 x e2 e com rompimentos dos corpos de prova na região central.

Oct 30, 2017

By Shengli Wu, Laixin Wang, Minyin Kou, Xinliang Liu, Weidong Zhuang, Yujue Wang

COREX process has obvious advantages in environment protection but still has some disadvantages, for example, it has a higher sulfur content of hot metal than blast furnace. In this paper, the thermodynamics and dynamics of desulfurization have been investigated to obtain the main operation parameters related to the mass fraction of sulfur in the hot metal. In addition, statistical analyses have been carried out to study the relationship between operating parameters and sulfur content of COREX hot metal based on actual plant data. It has been found that the mass fraction of sulfur in hot metal is significantly influenced by the C content in hot metal, MgO/Al2O3 in slag, the concentration of MgO in slag, the temperature of hot metal and binary basicity (R2).A linear model has been developed and subsequently used for reducing the mass fraction of sulfur in hot metal, improve the quality of hot metal and contribute to low carbon ironmaking.

Jan 1, 2016

By Dan Wang, Qian Xu, Guangshi Li, Xionggang Lu, Xingli Zou, Zhongfu Zhou, Hongwei Cheng, Changyuan Lu

The preoxidation of the ore has a profound significance to the concentration, separation and purification of nickel and copper from the lean complex ore. In this paper, the natural Ni-Cu sulfide mineral samples under the elevated temperature condition in air were investigated, as well as under isothermal condition at 600 oC in air. The mineralogical characterization was studied using XRF, ICP and the Rietveld method. The oxidation behavior and the element migration of the Ni-Cu sulfide ore were studied by XRD, SEM-EDS and TG. The XRD Rietveld method was successfully developed in the phase identification and quantification of this complex ore powder sample. The oxidative intermediates (Cu/Ni-ferrite) were detected by XRD, and the process of the element migration was obviously revealed by the line scans using SEM-EDS. It is the preoxidation of this mineral that provides guidance for the extraction of valuable metals from low-grade Ni-Cu sulfide ores in the future.

Jan 1, 2015

By Steve Lloyd, Ryan J. Foy, Brandon Steinborn, Jerome P. Downey

Research was performed to evaluate copper and silver extraction from samples of bornite flotation concentrate. Sulfation roasting experiments were performed in a rotary tube furnace, a fluidized bed reactor, and a static bed muffle furnace. Roasting was plagued with rapid, lowtemperature calcine sintering, apparently related to the presence of organic matter in the concentrate. Calcine entered a weak acid leaching process to remove copper, and silver was extracted from the weak acid leach residue in a ferric chloride and hydrochloric acid solution. Copper extraction efficiencies in excess of 90% were attained in the weak acid leach while 90% silver extraction was achieved in the ferric chloride leach, along with copper and lead extractions as high as 93% and 99% respectively. The two-stage leaching process resulted in overall extraction efficiencies of 99% copper and 90% silver.

Jan 1, 2015

By Carla Lupi, Alessandro Pescetelli

"Spent lead battery recycling still shows few weak points in the achievement of a 100% recycling of different waste matters and by- products arising from the recycling process. Some of said problems are dealing with aqueous streams outgoing the recycling plant, and more particularly, a) the waste waters discarded from the breaking and separation unit, b) purification of the spent electrolyte drained from waste batteries and upgrade to a quality compatible with full re-use by the batteries’ manufacturers, c) purification of the mother liquors discarded in the sodium sulfate crystallization process so to produce a salt of commercial grade. All of the above listed problems have been satisfactorily overcome applying an electrochemical process that, through different process conditions and parameters, is able to remove the harmful impurities that hinder the successful commercialization of such by products, or, at least, that can avoid heavy and expensive treatment plant and operation.IntroductionAlmost 100% of commercial lead and lead alloys produced by secondary lead plants is recycled to the new lead accumulators manufacture. The other by-products and residues produced through the lead recycling process may be classified into two groups:a) matters reusable in the new accumulators production processb) matters produced as a result of various reagents and additives used in the recycling process, to be sold to different market sectorsQuality and saleability of by-products are significant points for the economics of the secondary lead plant operation, because, if said by-products are not saleable, they are just wastes, so offsetting potential revenues, and, at the same time, adding a heavy burden to operating cost, like disposal cost [1]. When looking at a typical, modern lead scrap batteries recovery cycle, it is quite evident that we are still rather far from dealing with a waste-less technology (fig.1).The group a) includes 3 by-products produced through the breaking process: among those matters the polypropylene only usually reaches a standard quality suitable for sale to lead manufacturing sector or to other sectors as well. The other two by-products, electrolyte and separators, do not still reach, through a viable and effective regeneration process, a quality standard sufficient for their re-use in the lead batteries sector ."

Jan 1, 2008

By and M. V Roper, H. N. Engelbrecht

Quality control interventions emanate from process upsets and trends that move product quality beyond the natural variation expected in a stable process. The ability to detect upset conditions and react in an effective manner protects both resource utilisation and compliance to specifications. Product quality control on coal processing plants traditionally relies on the reference (combined sampler and laboratory) system to measure product qualities. The introduction of online analyser (OA) technology, applied in different configurations, creates a second source of measurement information for control decision making. The case study was done on the primary sample stream of the final product stream at Exxaro’s GG7 and 8 plants, part of the Grootegeluk complex. It explores the OLA system’s ability to meet the OEM performance guarantee, perform equally to the reference system without analytical delay time, and assesses the effort to achieve this performance in a by-line analyser (BLA) configuration. In the paper, a conceptual comparison of the two measurement systems is done and the theoretical and practical comparison of measurement performance is discussed. Results demonstrate that the OA outperformed the OEM’s performance guarantee and achieved similar levels of performance to the reference system without the response delay. Keywords: Online analyser (OLA), by-line analyser (BLA), coal quality measurement, measurement performance

Jan 1, 2020

By Rafael Duclou Rito

Com temperaturas altíssimas atingidas, os fornos são equipamentos responsáveis pelo aquecimento de materiais na produção de tubos sem costura. Assim, o investimento requerido de um forno em bom funcionamento é quase todo em combustível. Este trabalho foi desenvolvido objetivando a qualidade dos produtos e a otimização dos períodos em que o forno não produz. Durante os períodos citados, o forno é desligado ou mantido a uma temperatura menor que a de operação. Estudando a transferência de calor, principalmente no refratário, é possível analisar a melhor prática em situações improdutivas. Portanto, foi desenvolvido um simulador da temperatura dos refratários ao longo do tempo do forno em questão, sendo possível espelhar parâmetros reais para encontrar o controle de temperatura ótimo do forno, em que a temperatura da atmosfera interna é a principal entrada no programa. Termopares foram instalados ao longo das paredes refratárias para que o modelo fosse validado e aprimorado. Paralelamente, pontuou-se a relação dos materiais enfornados com as medições dos termopares, a fim de encontrar uma temperatura ideal de enfornamento. Os resultados foram positivos e permitem o uso de artifícios de refinamento dos resultados.

Oct 30, 2017

By Carolina Passanante

Aços Inoxidáveis Supermartensíticos surgiram na indústria petroquímica como um material alternativo para confecção de dutos, devido principalmente ao sinergismo de suas propriedades mecânicas e de corrosão. Com esta nova demanda, tornou-se necessária a caracterização deste material em suas diversas propriedades, destacando-se neste trabalho o efeito da microestrutura na resistência à corrosão. Objetivou-se, portanto, o estudo da resistência à corrosão por pite de um aço inoxidável supermartensítico 13Cr-5Ni-2Mo-Nb em função da fração volumétrica de ferrita-delta (d) presente na microestrutura. A variação da ferrita-delta foi alcançada através de tratamentos de recozimento, a 1.050°C, durante diferentes tempos (de 0,5h a 48h). As amostras foram submetidas a ensaios de polarização potenciodinâmica em eletrólito contendo 3,5% NaCl, naturalmente aerado. Quantificou-se, ainda, a porcentagem de ferrita em cada uma das condições através de ataque eletrolítico com solução 20% NaOH. Os resultados obtidos evidenciaram a diminuição desta fase com o aumento do tempo de recozimento, chegando praticamente à sua eliminação com tratamento de 48h. Paralelamente, a resistência à corrosão por pite deste aço foi melhorada de modo proporcional à diminuição da fase ferrita, resultando em um aumento de aproximadamente 115 mV da pior para a melhor condição, comprovando que, de fato, a presença de ferrita-delta prejudica as propriedades de resistência à corrosão localizada.

Aug 7, 2018

By Karl Berger

Today we are talking about Industry 4.0, as the latest revolution of industrial processes and progress, considering that the steam engine (Industry 1.0), railways and cars, mass production in the 1920th (2.0), Industrial Automation (3.0), and finally integrated manufacturing, integrated communication, and internet (4.0) can be seen as the state-of-the-art situation in industry, nowadays. Similar to the Industry progress, we can approach the rolling process of material, which started about 150 years ago in a very basic way. Steam engine- and belt driven-mills were very operators’ intensive, brutal and risky to operate. Mechanical improvements brought throughput, safety and quantity, as also quality of the products. The rolling of steel, in particular of rails, beams, rebar, strip (focus in this paper) and plate has enabled the large scale transport and travel, the building of bridges and buildings, the manufacturing of ships and cars. From single stands to continuous rolling trains the production and quality of mills increased significantly. From ingots and blooms to slabs, we have to admit a big jump in which has changed the face of the world significantly. Thin Slab Rolling has revolutionized the output and the throughput of rolling mills (Generation 3.0 to 5.0). Finally, Endless Rolling, has boosted the quality and quantity of rolling mill processes and permitted nowadays to enter in market niches which were not thinkable a decade ago. Mastering the automation and applying reliable systems (mechanical and electronically) of drives, actuators and sensors, as also communication and information interchange to all levels of automation are the success factors of such complex mills, we call herein after “Rolling Mills of Generation 6.0”.

Aug 16, 2017

By Luis Armando Espitia

AISI 410 martensitic stainless steel specimens were low temperature plasma nitrided at 400°C in a mixture of 75%N2:25%H2, during 20 h. Active screen technic was used to avoid any edge effect The nitrided case is composed of expanded martensite (a’N) and e-Fe3N iron nitride, whilst chromium nitride precipitation was avoided. Surface hardness reached 1275 HV0.01. The transverse microhardness profile shows a gentle hardness gradient with a NHT nitrided case depth of 28 µm. Nanoindentation tests were carried out in order to assess the hardness (H), the Young modulus (E), the H/E and H3/E2 ratios and the elastic recovery (We) of both nitrided and non-nitrided specimens. The cavitation erosion mass losses were measured as a function of exposure time. The results showed a decrease of 27 times of the mass loss compared to the non-nitride specimens. Wear rate decreased from 2.56 mg/h for the non-nitrided condition to 0.085 mg/h after nitriding. The increment in the elastic recovery and the higher hardness values are responsible for the greater cavitation erosion resistance exhibited by the expanded martensite. Such results showed that low temperature plasma nitriding and the formation of expanded martensite are effective to increase cavitation erosion resistance of AISI 410 stainless steel.

Jul 31, 2018

By Arnaud-Guilhem de Loze

Este artigo apresenta uma ferramenta de simulação computacional desenvolvida com o objetivo de auxiliar a adoção de melhores práticas de controle do forno durante períodos sem produção. O sistema desenvolvido permite simular as temperaturas do revestimento refratário de um forno de tratamento térmico de tubos em função da evolução da temperatura da atmosfera interna em diferentes cenários. O simulador foi desenvolvido baseado em um modelo matemático dinâmico validado, que utiliza um sistema de equações de transferência de calor discretizadas. Realizou-se a validação desta ferramenta computacional com a utilização de dados reais de uma campanha de medição de temperaturas. A comparação dos resultados apresentou pequeno erro entre simulação e valores reais coletados. A utilização desta ferramenta auxiliou a definição de estratégias de controle do forno durante períodos improdutivos, possibilitando redução do consumo de energia e retomada da produção com garantia da qualidade do produto.

Aug 17, 2017

By Fabiano Soares

Strand guide rolls in continuous casters are crucial components for guaranteeing an optimum process for the production of high-quality steel grades. The properties of these rolls greatly influence the quality of the slab produced. The most commonly used designs so far have been the axle roll and the solid roll. A quite new roll concept is the STEC-Roll®. It combines the advantages of the axle roll with those of the solid roll. This paper explains the development of this roll type and shows the current design. The characteristics of the STEC-Roll® are presented in greater detail and are underlined by a number of simulation results. Beside the design itself, the benefits for casting and maintenance are explained, including for example the easy assembly and dismantling or the use of the roll for dry casting. A brief examination is made of the TCO for the STEC-Roll® and an estimation is provided of the exchangeability of this roll. To conclude, an overview on the current applications is presented.

Aug 17, 2017

By Nestor Ferreira Carvalho

Com o intuito de garantir a segurança das pessoas, meio ambiente e o patrimônio das empresas, os vasos de pressão e caldeiras instalados no Brasil devem ser protegidos por válvulas de segurança, cuja função é evitar que o equipamento seja pressurizado acima da pressão de projeto. A escolha do melhor local para instalação dessas válvulas deve levar em consideração, além dos itens usuais de projeto, os esforços gerados quando da abertura dessas válvulas. Esse artigo, faz uma análise da fratura, com o propósito de determinar as causas básicas da falha e evitar sua repetição. A análise foi realizada com o apoio de literaturas sobre fractografia e fadiga.

Aug 16, 2017

By Moisés Paulo Teixeira

The use of tailings for the synthesis of new materials is a worldwide concern today. This paper approaches the utilization of tailings of soapstone (steatite) in order to produce ceramics. The results show that the addition of soapstone in a ratio over 20% in the ceramic mass has enhanced the bending resistance of the ceramic samples when they were fired at temperatures of 900°C or 1000°C.

Oct 30, 2017

By Peter Fajfa, Heinz Palkowski, Jakob Kraner, Matjaž Godec

The study of asymmetric rolling on the AA 5454 aluminium alloy plates was carried out. The plates were taken directly from the industrial hot rolled sheet. They were cold rolled on the laboratory mill with different rotation speed of the upper and the lower work roller with the strains around 33 % and 44 %. To get closer to the industrial conditions the maximal dimensions of the rolled plates for laboratory rolling mill and the special industrial lubricant were used. After deformation the plates were annealed to the soft condition. This research was focused on all possible effects of asymmetric rolling: The reduction of rolling force, the increase of strain at same set roll gap, bending of workpiece, finer microstructure, more heterogeneous textures and as a consequence of that better mechanical properties. The asymmetric rolling with favourable mechanisms in the deformation zone has created the material with the homogeneous hardness in the cross section and with lower anisotropy, which is crucial for improvement of formability properties of aluminium work hardened alloys and to get closer to properties of steels. In the presented paper the general impact and different effects of speed difference of rollers was investigated on cold rolled aluminium alloy. Obtained and analysed results explain the function of asymmetry in rolling process and the options to implement the asymmetric rolling in industrial plant.

Oct 1, 2019

By Pierre Montmitonnet, Yukio Shigaki, Jonatas Mezêncio Silva

A precise roll stack deformation model of a flat rolling mill is crucial for strip profile assessment as it depends strongly on the roll’s deformation. The need for more and more advanced products with stringent both geometrical and mechanical tolerances (e.g., Advanced High Strength Steels – AHSS), with thinner and harder steel strips, demands more advanced simulation models. The present paper addresses assumptions made in Finite Element Method (FEM)-based roll stack models on some important, yet barely discussed features: What is the impact on precision of the simplifications such as symmetry and anti-symmetry? Should roll neck boundary conditions in bearings be considered as fixed or simply supported? In this paper a hybrid model developed by the authors for a general flat rolling mill is used to assess those questions. This model runs much faster (100x in some cases) than a whole-FEM-modeled 6-high rolling mill with the elastoplastic strip deformation, thanks to its simplifications adopted. This model assumes a steady state rolling condition, and the roll stack is modeled with tridimensional finite elements, and the loads are calculated via a slab method adopting a plane strain state for the strip deformation (especially true for thin strips). An industrial 6-high cold rolling mill is modeled and results on the application of symmetries and different boundary conditions on the roll’s necks are presented. It is concluded that the application of symmetries and anti-symmetries for the 6-high rolling mill is possible for thin strips. And the way the necks are modeled does not impact on the final strip shape, though it influences the magnitude of the roll’s displacement. The coupling of the strip with the work roll applied assuming a symmetry plane of the arc of contact has little influence on the strip shape.

Oct 1, 2019

By C. Sunderman, R. Jacksha

"Mine monitoring through various sensors is a vital component of successful miner safety and health programs. Data from environmental, geotechnical, infrastructure and other types of sensors are increasingly used to discover and mitigate health and safety concerns in underground mines. In many smaller underground mines, as well as in the new development headings of larger underground mines, leaky feeder communication systems may be the only available means to transport crucial monitoring data. In addition, data transport is increasingly being delivered using Internet Protocol (IP), while older forms of serial communication are being retired. This paper presents the selection, configuration and testing methodologies employed by researchers from the U.S. National Institute for Occupational Safety and Health (NIOSH) to integrate commercially available land mobile data radios into an existing leaky feeder communication system to provide IP data transport.IntroductionTo enhance the health and safety of their mining workforce, mine owners and operators are increasingly installing environmental monitoring and control systems in underground mines. Real-time, mine-wide monitoring is becoming a reality with the implementation of the Industrial Internet of Things (IIoT) into the underground mining industry (Zhou et al., 2017). However, not all underground mines, especially smaller mines and new development headings in larger mines, have the information technology infrastructure in place to handle the data transport requirements for the newer Internet Protocol (IP)-based technologies that are part of IIoT.This was the case with a mine in the Western United States. It lacked the infrastructure to perform critical monitoring in remote headings. Therefore, the mine partnered with the U.S. National Institute for Occupational Safety and Health’s (NIOSH) Spokane Mining Research Division (SMRD) to develop and evaluate a cost-effective solution for the real-time monitoring of geotechnical conditions in relatively remote sections of the mine. This paper describes SMRD’s solution to leverage the mine’s existing leaky feeder communications system to achieve IP data transport using commercially available land mobile data radios (NIOSH, 2013; Forooshani et al., 2013; Novak, Snyder and Kohler, 2010; Yarkan et al., 2009). The solution, fully evaluated in laboratory and mine environments, requires no modifications to the existing system, is economical, simple to implement, and reliable. It also allows for transition to higher-bandwidth IT networks, such as fiber optic or WiFi, should they become available."

Dec 1, 2018

By Jiang Wenli, Zhang Yimin

In order to enhance the quality of iron concentrate from magnetic separation, reverse-flotation technology is often applied in an iron ore dressing plant.However, this technology has disadvantages in terms of operating cost,energy consumptionand environmental protection(Zhao, Wu& Wang,2005).Developing innovative equipment to process magnetite ore more-effectively is a way to get rid of these disadvantages of reverse flotation and improve the quality of iron concentrate.This paper describes the development of Complex Flashing-Field Magnetic Cleaner,a new kind of equipment based on the principle of combination of separation in magnetic field and separation in gravity field(Hao & Jiang, 2002).This innovative equipment possesses a tailor-made magnetic system and has the characteristics of a magneticfieldwhich can strengthen the formation of magnetic agglomerations and the dispersion of gangue mineralsto improvethe quality of separation.The automatic control system developed specifically for this equipment can further increase the accuracy of separation and stabilize the process.

Jan 1, 2014

By V. B. Achanti

This paper deals with the effect of various bit geometric parameters on failure characteristics of rock material. Improvement of rock cutting efficiency of continuous mining machines has been an interesting research topic for the last few decades. In the current study, an automated rotary rock cutting simulator, duplicating a continuous miner, was utilized to study these parameters in the laboratory. Improvement of bit performance in terms of its life, cutting efficiency, dust production and energy consumption has drawn wide spread attention over the years. Research shows that optimizing bit parameters can result in efficient fragmentation of rock. Indiana limestone rock material was utilized in this study while bit tip angle, bit tip size, bit spacing, depth of cut and cutting velocity of rotary drum were varied to investigate the failure characteristics. The cutting pressure, penetrating pressure and the depth of cut were monitored on the simulator during the cutting process. Air borne dust and settled dust were measured for each experiment. Then, the specific airborne dust and specific energy were determined for the each type of bit. Triaxial tests were carried out to correlate the failure angle of the rock in static case to dynamic cutting process failure. The physical and mechanical properties of the rock were also determined in order to assess their influence on the wear characteristics of each bit.

Jan 1, 1998