Search Documents

By J. H. Hamilton, J. R. Lewis, J. C. Nixon, C. L. Graverson

Recently there has been much speculation concerning the advantages of using oxygen enriched air or pure oxygen in pyrometallurgical processes. The advantage of using oxygen in the iron blast furnace and elsewhere in ferrous production metallurgy has been given careful consideration and, as a result, several experiments have been tried and a number of papers have recently appeared on this subject.1,2 The use of oxygen in nonferrous smelting likewise poses interesting problems, therefore any experimental data obtained in this area should likewise be of general interest.3 Ashcroft4 in 1933 claimed to have obtained improved results when copper concentrates were roasted in pure oxygen. However, his paper gives neither data nor experimental details. A few years ago a research program was started in this laboratory which had for its objective the determination of the mechanism of oxidation of metallic sulphides under varying conditions. To date we have studied the oxidation of galena,5 sphalerite, and chalcocite. It is a well known fact that copper sul-phde minerals are oxidized slowly by weathering agents, so that the sulphides of copper which find their way into a tailing pond are gradually changed into water-soluble and acid-soluble compounds. Commercially, the oxidation of copper sulphide minerals is accomplished by roasting them at elevated temperatures in air using a suitable (usually multiple hearth) roaster. Most copper smelters are equipped with such roasters. In this phase of the study we were especially interested in determining the effect of temperature on: (I) the air oxidation of chalcocite and (2) the oxidation of chalcocite using commercial oxygen. The amount of sulphur removed as sulphur dioxide, the percentages of water-soluble copper, and of acid-soluble copper were determined for the air oxidation tests. In the tests using commercial oxygen, the percentages of sulphur dioxide, water-soluble copper, acid-soluble copper, water-soluble sulphur and acid-soluble sulphur were determined. For these experiments the temperature was varied from 250 to 700°C. Experimental Preparalion of Chalcocite (Cu2S) Natural chalcocite is not pure, Minerals such as bornite, covellite, and chalcopy-rite may be present. It was decided, therefore, to prepare some chalcocite in our own laboratory. An intimate mixture of sulphur and hool divided metallic copper in the ratio of 4 g of copper to I g of sulphur was prepared. TO this was added a slight excess of

Jan 1, 1949

By Lawrence W. Teufel

Knowledge of in situ stress and natural fracture distribution at depth improves our ability to stimulate and produce low permeability reservoirs. The focus of this study is three closely spaced, 2.5 km deep vertical wells in the Piceance Basin of Colorado. The wells were completed through the tight lenticular and blanket gas sands of the Mesaverde Group. In situ stress directions and magnitudes were determined from hydraulic fracture tests and anelastic strain recovery measurements of oriented core. The distribution, orientation, and characteristics of natural fractures in the subsurface were determined from detailed observations of over 1300 m of core, of which 400 m was oriented. Stress measurements clearly show that horizontal stresses are strongly influenced by lithology. In a sandstone/shale sequence at a depth of about 2.0 km in situ stresses in sandstone formations are anisotropic, with the average ratios of the minimum and maximum horizontal stresses to the overburden stress being 0.82 and 0.96, respectively. In sharp contrast bounding shale formations are lithostatic. This stress contrast between sandstones and bounding shale formations could act as a barrier to hydraulic fracture propagation during stimulation and impede vertical fracture growth. Natural calcite-filled fractures are present in over 7 percent of the core, with several horizons having a much higher frequency of fractures. Fractures are found primarily in sandstone. The fractures have a strong preferred orientation of N 1060E[+]110, which is aligned with the maximum horizontal stress and direction of hydraulic fracture propagation. The interaction between a well developed fracture fabric and anisotropic stresses in sandstone formations produces a permeability anisotropy, with the maximum permeability aligned with the fracture fabric and maximum horizontal stress.

Jan 1, 1986

By G. A. Doyle

The White Pine Mine is the second-largest active underground copper mine in the United States, covering an area of approximately 13 square miles in the Upper Peninsula of Michigan. The mine operator intends to initiate in-stope solution mining by circulating a solution of mine water, sulfuric acid, and ferric iron through rubblized ore and recovering copper from solution. As planned, the solution would be retired in the mined-out stopes following completion of solution mining activities. Investigations into the fate of the retired solution mining fluid indicate that the solution, through time, will change from an acidic, metal-rich solution to a near-neutral, reducing solution containing much lower concentrations of metals. Investigations include reaction path modeling (EQ3/6) and laboratory and in-mine experiments. The combination of neutralization and reduction will result in precipitation of most metals, primarily as metallic sulfates, chlorides, and sulfides.

Jan 1, 1996

By John M. Devine

The oxygen bomb-is used extensively for determining sulphur in petroleum, although it has been suspected that the results obtained with this method are somewhat lower than the true varies. In this paper are compared the results given by the oxygen-bomb and Carius methods, the latter being generally accepted as the standard procedure for the determination of sulphur in organic compounds. The Carius determinations given hero were made in connection with a special study of this method.4 Only petroleum oils of the less-volatile type are covered in the present work. Summary and Conclusions. When used with oils containing 2.3 to 0.15 per cent of sulphur the oxygen-bomb method gives results that are consistenly if slightly lower than those obtained with the Carius method. This variation, for the oils used, amounts to 3.1 per cent (on tae basis of sulphur present) for the sample containing 2.47 per cent of sulphur, and gradually increases (as the percentage of sulphur in the oils decreases) to 7.3 per cent for the oil containing 0.15 per cent of sulphur. With the oils studied the presence of ammonium nitrate in the bomb does not influence the results materially.

Jan 1, 1928

By S. D. Brady

In Monongalia County, West Virginia, the Pittsburgh and Sewickley beds lie west of the Monongahela River and underlie practically all the western end of the county. The average thickness of the Pittsburgh bed is 8 ft., where it is being mined at present, sometimes running up to 9 ft. The Sewickley bed is 4½ to 6 ft. thick and lies 90 to 100 ft. above the Pittsburgh bed. As the Pittsburgh bed had a known value, a large part of it was bought up without consideration of the Sewickley bed. When the Monongahela Railway was built up the west side of the Monongahela River, other interests bought up the Sewickley bed, as it was found to be equal in quality to the Pittsburgh, with slight local exceptions. The two beds, therefore, were owned by different people, and naturally each owner opened his mine and ran it without regard to the working of the other bed. Consequently, considerable portions of the upper bed were seriously affected for economical mining, especially on Scotts Run. In recent years there has been a tendency, influenced by the decision of the West Virginia Supreme Court, on the part of the operators in Monongalia County to try to coordinate their projections in the layout of their mines. A typical geologic section, according to the report of the West Virginia State Geological Survey on Monongalia County, agrees with Fig. 1. It is apparent that the rock above the Sewickley bed and between the Sewickley and Pittsburgh beds is of a rather friable ~lature, therefore it is easily broken in pillaring. About the only difference between this section and the geologic section in the Lowsville district is that in the latter district the rock between the coals is a denser sandstone and contains little shale and limestone and no evidence of Redstone coal. It is a laminated sandstone, and although it makes a harder mass, it is easily broken. While working in the Lowsville district, the author had an opportunity to examine a neighboring mine in the Sewickley bed, which was over a section being pillared in the Pittsburgh bed. The two mines belong to dif-

Jan 1, 1931

By Eduardo Pimenta de Melo, Rambabu Pothina, Rajive Ganguli

Sensors are everywhere in the mining industry, with sensor information being used to monitor and operate processes. Therefore, when sensor information is wrong, economic losses can occur. Unfortunately, sensor errors are usually not detected till they become large. This is problematic as most calibrate their sensors no more than once a year (Beamex, n.d.). Using principles of data mining, where all relevant information is tapped to glean hidden information, Pothina [8] designed an algorithm to detect errors in temperature sensors in gold stripping circuit in Pogo mine, Alaska. This paper continued his work by analyzing the behavior of the algorithm on baseline data and testing the algorithm in new data and under more rigorous conditions. It also made a change to the algorithm. The modified algorithm performed very well in the new data. It also worked well under the new error conditions. Three types of errors were seeded, a fixed additive error (+ 2%), a fixed subtractive error (− 2%), and a noisy, normally distributed error, with a mean value of + 2%. Artificially seeded errors were detected within about 20 gold stripping cycles. Inherent bias in operation impacted algorithm performance by increasing the number of cycles needed to detect errors. This paper reinforced Pothina’s [8] conclusion that when data mining approach is used, sensor errors can be detected even when they are pretty low. Significant economic losses can thus be minimized.

By K Uchino, M Inoue

Self-potential anomalies are generated by fluid pressure gradient, by temperature gradient or by chemical gradient. On the basis of this principle, a new technique is proposed to locate the fire source of spontaneous combustion of coal by the self-potential method. In order to investigate whether this method can be applied to locate the spontaneous combustion of coal in practice, surveys of self-potential distributions were undertaken in a coal waste pile undergoing spontaneous combustion. The results showed that there is a negative centre of the electrical potential distribution in the measurement area. The potential in this centre is about 140 mV lower than that in the surrounding area. Moreover, the negative centre of electrical potential distribution almost overlaps with the high temperature zone. Therefore, it is concluded that it is possible to locate the heat source by the measurement of self-potential distribution.

Jan 1, 2005

By K. J. Anusavice, R. T. DeHoff, A. G. Guy, T. B. Lindemer

As one oi the approacizes to understanding multicorn-ponent dimsion, an expevinzental sturly is being jnade of tracer diffusion in the copper corner of the CLI-Ni-Zn syste?n, out to 30 at. pct each of nickel and zinc, and in the 150°C range oJ temperature just below tlze solidts te?rlperature. The reslts obtained using the Znm isotope are reported heve, while studies with nickel and copper isotopes are planned for a future paper. The fifteen alloys investigated were melted in sealed wear lubes, sroaged, homogenized, and then analyzed, using the conventional isotope-plating plus lathe- sectiorzing teclzniqlte. The data obtaiued show that the difJusion coeflcient of the zinc isotope increases titlz increase in zinc content, and decreases t'itlz incease in nickel content. The correlation xith solidus temperature is particularly strong. Diffirsiui-ties ranged fro u sq cm per sec nt tlze Iiigh-zinc, low-nickel compositions. The activation energy /or tracer diffusion ravied j.or 31.000 to 54,000 calper mole. It is now generally recognized that diffusion data and theories are needed for multicomponent systems, where extensive practical developments and even some theoretical studies have already been made. For example, much recent work on precipitation from solid solution has been concerned with ternary solid solutions such as A-M-Z' while Zener relaxation has been studied on Au-Ag-Zn alloys,' although adequate diffusion data are available for neither of these systems. Actually, the only ternary systems for which systematic diffusion studies have been begun, in addi- tion to the one reported here, are CO-i-cr3 and Cu-A-Au. Since the theory of multicomponent diffusion is still in the stage of active development5 it is important to distinguish the various kinds of diffusion data that can be determined. An oversimplified approach, widely used prior to 1950, was to determine the influence of a third element, such as nickel, on the diffusion behavior of a binary alloy, such as CU-Z. Later it was recognized7 that four diffusion coefficients can be used to describe ordinary interdiffusion in a ternary system, while as many as six coefficients may be required to include the Kirkendall effect. It is likely that the number of independent coefficients will be shown to be less than four and six, respectively, through the application of the thermodynamics of irreversible processes.5 The simplest type of diffusion in a multicomponent system is tracer diffusion, since each component is characterized by its own tracer-diffusion coefficient in an alloy of a given composition. Thus, in a ternary alloy there are three tracer-diffusion coefficients, each a function of composition and temperature. The present research program is a study of tracer diffusion in the copper corner of the Cu-Ni-Zn system out to 30 at. pct each of Ni and Zn in a 150°C range of temperature just below the solidus temperature. The

Jan 1, 1967

By G. M. Thain

Ancient Mining - The following three contributions were received for publication in addition to the preceding papers. 1. Ancient gold-mining sites in the Transvaal G. M. THAIN* Pre-European gold mining and working in South Africa is a tantalizing field for conjecture. Well over thousand sites have been identified in Rhodesia, but here we have had to reach double figures, judging by published accounts. Geologically, the Transvaal is less amenable primitive exploitation, but it difficult to reject the idea that the knowledge gained to the north did not have its influence south of the Limpopo.

Jan 1, 1974

By G. W. Grove, H. R. Burdelsky, F. E. Griffith

"INTRODUCTION The work of using a system of air locks in unsealing a mine in Ohio following a fire probably was one of the outstanding jobs of its kind in a medium-thick coal bed.The fire in this mine, thought to have been of electrical origin, was discovered at about 1:30 a.m. on December 11, 1941. Forty-four men were working in the affected section at the time; 5 escaped unassisted, and 37, who had barricaded themselves, were rescued. The bodies of two men, who had succumbed after breathing fumes given off by the fire, were brought part way out of the mine before it became necessary to seal the mine.Direct attempts to extinguish the fire with water were abandoned when hazardous amounts of 'carbon monoxide, methane, and other inflammable gases were detected in return air passing through the main haulageway and escape-way of the mine.The mine was completely sealed on the surface at about 8 p.m. on December 12, 1941, with the two bodies remaining in the mine. Sixteen days after the mine had been sealed, the two bodies were recovered. This was accomplished by air-locking through a partitioned-off stairs compartment of a ventilation shaft. This work was done under adverse barometric and atmospheric conditions.A method for collecting representative air samples from the immediate fire area was used successfully by utilizing a vacuum pump on about 10,000 feet of existing water line that had been broken near the fire area.The immediate fire region was sealed, and confined to a relatively small area; the remainder of the mine was recovered, and operations were resumed February 9, 1942, or 59, days from the time of sealing the mine on the surface. This recovery was made by air-locking the main entries inby from the shaft and No. 2 right-face entries.The distance between air locks averaged about 500 feet, and as each new set of seal stoppings and air locks was completed, the old or outby seals were taken out and the area between was ventilated. In ventilating this area, it was often necessary to use line curtains to direct the air into dead-end places."

Oct 1, 1947

By Johne Jesus Mol Peixoto, Ciro Azevedo Silva, Itavahn Alves da Silva, Weslei Viana Gabriel, Leticia Queiroz Ribeiro, Carlos Antonio da Silva, Varadarajan Seshadri

In this study,the influence of the immersion depth, casting speed on the flow characteristics in a beam blank mold with two tubular nozzles have been investigated using a physical model as well as CFD simulations.The results of CFD simulations were found to be consistent with the results of experiments in the physical model.The liquid jet spreads faster the flange region compared to the web region. This can lead to a non-uniform shell thickness along the cross section resulting in uneven solidification of the skin. The jet penetration depth ranged between 66 and 77 cm. The average intensity of meniscus fluctuation was 0.22 mm, and the maximum fluctuation was found to be 0.85 mm. Based on these results, the suggested optimum operating parameters for immersion depth and casting speed were 75 mm and maximum casting speed of 1 m/min.

Mar 1, 2017

By D. D. Pollock, D. I. Finch

PREVIOUS work' on a four-component system (Cu-Mn-Ni-Fe) resulted in the development of consistent relationships between the chemical composition and the electrical properties of these manganin-type alloys. The present study was undertaken to develop alloys with temperature coefficients of resistivity and thermoelectric properties more desirable than those of the manganin type, and to determine whether the relationships which had been found for the Cu-Mn-Ni-Fe alloys could be extended to five-and six-component alloy systems. PREPARATION OF ALLOYS The five- and six-component alloys were made from OFHC copper rod, ARMCO iron, electrolytic nickel, manganese cathode chip, and special high-purity aluminum and indium. A Cu-Mg master was used for deoxidation. The compositions of these materials are given in Table I. The alloys were melted and cast as indicated previously,' except that no cover was used and the melts were teemed. EXPERIMENTAL PROCEDURE The finished wire size of 0.0808 in. diam was again selected for the reason that the test specimens would be self-supporting, thus eliminating any extraneous effects which might have been introduced by winding smaller diameter wire on spools or forms. The following tests were performed on the finished wires: A) Chemical Analyses—All of the components of these alloys were determined by premium gravimetric methods. The principle residual impurity contained in these alloys is 0.008 pct Mg (by weight), maximum. Tables II and 111 present the mean analyses computed from at least four determinations of each constituent. B) Electrical Characteristics—The test procedures forthe determination of the thermal emf vs copper, resistivity, and the resistance-temperature relationship are given in detail in Ref. 1. It was also shown that the resistance-temperature relationship is of the form Pt = P,n + At -B/2, [1] where P, is the resistance at t C expressed in percent of a given standard resistance, P, is this per- 0 centage at 0°C, and A and B are constants for a given, properly treated, composition. The results of the electrical tests are also given in Tables II and 111. INTERPRETATION OF DATA The modified Linde2 formula, known to be valid for dilute binary solid solutions, was applied to the complex Cu-Mn-Ni-Fe type alloys. This relationship is of the form where Ap is the increase in resistivity. Zb the valence of the solute, Zn the valence of the solvent, and K and K are designations assigned by Robinson and Dorn3 to the constants for the periodic group to which solute element belongs. The units of K, are -cm per valence difference squared per at. pct; those of K2 are pa-cm per at. pct. For the sake of brevity, these units are not repeated in the following discussion. Calculations were made to determine if this formula was accurate for five-component systems. No experimental studies were made of the Cu-In and Cu-A1 binary systems. The effects of indium additions upon the resistivity of copper are given by Linde. These data, along with those of the effects of Mn and Fe, permitted the calculation of the effects of Al.

Jan 1, 1959

By F Butler, G E. Batley, A C. Hogan, A R. Butler

The ANZECC/ARMCANZ (2000) Water Quality Guidelines (the Guidelines) are the primary reference used in Australia and New Zealand for managing and regulating water quality. For most mining operations in Queensland, the environmental authority (EA – licence) incorporates the national default guideline values (GVs) for ecosystem protection as trigger levels (TLs). Exceedances of TLs ‘trigger’ further investigation and reporting. A review of the surface water compliance history at a metalliferous mine in North West Queensland identified minor exceedances of the cobalt GV as a common trigger for investigation and compliance reporting.The reliability of GVs is dependent on the availability and quality of ecotoxicology data for the relevant contaminant. The current national default GV for cobalt of 1.4 µg/L is classified as a low reliability GV due to the lack of available data at the time it was derived (ANZECC/ARMCANZ, 2000).The Guidelines are presently being revised and the toxicant GVs will be available as a set of web-based values and associated technical briefs. The new platform will enable the timely revision of existing GVs and inclusion of GVs for additional toxicants. Cobalt was considered a priority toxicant for the Guidelines’ revision, but was not included in the revision process.A preliminary review of the international literature indicated that at least 15 additional chronic cobalt toxicity studies had been published since 2000, sufficient to derive a high reliability cobalt GV using the protocols developed for the revision of the Guidelines (Batley et al, 2014; Warne et al, 2015). This presented an opportunity to improve environmental management by increasing the reliability of the performance measure.CITATION:Hogan, A C, Butler, A R, Butler, F and Batley, G E, 2016. Derivation of high reliability water quality guideline values for cobalt in freshwaters – improving water quality guidelines for better water quality compliance management in mining, in Proceedings Life-of-Mine 2016 Conference , pp 205–208 (The Australasian Institute of Mining and Metallurgy: Melbourne).

Jun 28, 2016

By Qidong Xu

Abstract - The metavolcanic rocks of the Dahongshan area have been subjected to both widespread hydrothermal alteration from circulating seawater and to regional metamorphism, such that their mineralogic and chemical compositions have been changed significantly. Studies of immobile elements show that these rocks were originally tholeiitic basalts with geochemical characteristics of T-type MORB formed in a mid-ocean ridge environment. The accompanying Cu-Fe-rich VMS mineralization is in keeping with the original petrology and tectonic setting of these metavolcanic rocks. Regional alteration evident in K-Mg enrichment is related to sericitization and chloritization. Local alteration associated with Cu-Fe mineralization appears to have been accompanied by Si enrichment and Na depletion. P enrichment identifies metasomatism related to Cu-Fe reconcentration in the mineralized zone.

Jan 1, 1999

By Jacques B. Wertz

It is well known that the major fractures and lineaments presently recorded in Western North America are preferentially oriented along a general northwest direction (Figure 1). There are other features, however, more subtle, more elusive as a rule and which can only be inferred, occurring at right angle to this broad NW direction. It is intended a) to examine some of these NE or transverse trends, b) to compare these regional NE breaks to similar ones that transversally cut through the eastern part of the European Tethys, more specifically in Iran and Turkey, and c) to study their potential relationship to mineralization in both areas.

Jan 1, 1973

By Jr. Kirschner

An abandoned waste impoundment located within a portion of the Kellogg, Idaho Superfund site constitutes a field research area for studying the feasibility of recovering heavy metals in-situ from unsaturated mine and mill wastes. A prototype in-situ leaching cell has been evaluated using liquid-phase tracer tests and other hydro-geologic tests prior to introducing a lixiviant. The results of the tests suggest that: (1) the cell can be operated excursion-free with a low-density lixiviant at an injection/withdrawal rate of approximately 0.32 l/s; and (2) each hydro-geologic unit is highly heterogeneous at the different scales studied.

Jan 1, 1993

By Kenneth H. Johnston

This report describes an in situ combustion project and three waterflood projects in Allen, Anderson, and Wilson Counties, Kansas, that will be visited during the 1964 annual tour of the Kansas-Oklahoma Waterflood Association. Among the unique features of the projects are the movement of heavy crude oil through the reservoir and into the wellbore with energy furnished by burning a portion of the crude oil therein. Another feature is the simultaneous injection of C02 and water, through separate tubing into input wells during early development, to increase injectivity at moderate pressures, Discussion of individual projects includes information on their early history, source and treatment of injection fluids, oil production-decline curves, and the results of water injection on oil production.

Jan 1, 1964

By Heimo Thalhammer

During the refining of lead, copper or other metals the furnaces used in the process · often produce waste gases. This paper illustrates how these waste gases can be successfully treated and destroyed by CTP 2-bed or multi-bed compact systems, modified for the additional reduction of dioxins and furans. The CTP regenerative thermal oxidizer also destroys voes (organic compounds and odours) using ceramic blocks as a heat exchanging media. The raw gas is forced through the ceramic beds where it is heated up to the oxidation temperature level. The voes, dioxins and furans are destroyed in the combustion chamber, subsequently generating water, eo2 and heat. The hot purified gas heats up a second ceramic bed, which is used to preheat the raw gas after the valves have been switched. This process does not produce any secondary waste such as contaminated water, polluted air or any other products that have to be disposed of.

Jan 1, 2000

By Franklin P. Hall

U.S. supply and demand data for utility electricity by States and regions were tabulated for the years 1960 and 1965. Estimates are provided of State-by-State quantitative data for the utility electricity industry that can be integrated into State and regional energy balances by source, form, and major consuming sectors, and used to determine basic flow-patterns. The difficult problem of compiling interstate and interregional shipments of electricity was resolved by (a) assuming the negligibility of interregional shipments and (b) deriving a theoretical line loss percentage used for determining interstate shipments. The data developed were able to show an estimated total supply of utility electricity available for consumption. The tables also report the distribution of the supply among the major consuming sectors (household and commercial, industrial, and transportation). To compare the various energy sources of utility electricity, quantities were converted to their British thermal unit (Btu) equivalents. The Federal Power Commission, Edison Electric Institute, and Bureau of Mines are the sources of the data used in this study.

Jan 1, 1969

By Emad Farouz, Roger Failmezger

"The proposed reconstruction of I-75 downtown consists of widening an approximately 2.46 Km section of IR-75 through the northern section of downtown Dayton, OH, USA. Bridge B-13 is a 9-span continuos prestressed concrete I-beam, 319.0-meter (1,048-foot) long bridge with a stub abutment on MSE walls for the rear abutment, and a stub abutment with spill-through slopes for the forward abutment. The piers in the river were located parallel to the Great Miami River, and are full-height reinforced concrete walls. PRESSUREMETER TEST PROCEDUREThe driller advanced either casing or augers approximately 1 meter above the pressuremeter test. Steel casing was used to advance borings performed in the river, and augers were used for borings on land. Mud rotary drilling with a large diameter roller bit was used to remove all of the gravel and cobble fragments inside the casing or augers.At the pressuremeter test elevation the driller used a 63.5-mm (2.5-inch) carbide button bi-cone bit, using a rotation rate of about 60 rpm, a mud fl ow rate of about 10 gallons per minute (40 liters per minute), and an advance rate of 6 to 10 minutes per meter (2 to 3 minutes per foot). To minimize vibrations, advance rates were slower where excessive cobbles were encountered. The 63.5-mm (2.5-inch) O.D. slotted casing pressuremeter was lowered to the test elevation, often requiring either pushing or hammering into the test zone. We believe that the test zone was not perfectly straight, or that gravel or cobble fragments jutted into the test zone and had to be displaced to advance the pressuremeter into the test zone. The slotted casing prevented membrane damage during insertion. A photograph of the slotted casing being lowered into the borehole is shown below.The pressuremeter was calibrated for system compressibility and membrane resistance. At full expansion of 800 cm3, the membrane resistance of the slotted casing was about 2.5 bars.Strain-controlled tests were performed using a Texam control unit with a monocell probe. Volume increments of 20 cm3 were injected into the probe and corresponding pressures were measured. Near the end of the elastic portion of the test, an unload-reload cycle was done. A creep test was performed for 10 minutes at the next volume increment. The test continued until either 800 cm3 were injected or the membrane burst."

Jan 1, 2007