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By H. P. Leighly, F. C. Perkins

THERE have been several statements in the literature about the difficulty of producing single crystals of high-purity (99.99pct) by the strain-anneal method. Consequently, investigators tend to employ low-purity aluminum for their single-crystal experiments, or else resort to the Bridgman or other techniques which depend on solidification for the production of single crystals. The following paragraphs describe a solid-state method for the manufacture of single crystals of high-purity aluminum which should provide crystals with greater perfection than those formed by solidification. The starting material for this method of producing single crystals was secured from the Aluminum Corp. of America and has a purity of 99.99 pct, the balance being trace amounts of impurities. Specimens approximately 1 by 4 in. are sheared from sheet having a nominal 0.050 in. thickness. The specimens are given a preliminary anneal at 640°C for approximately 3 hr in order to remove fabrication strains and to produce an average grain size of about 1/4-in. diam. The specimens are then etched in Tucker's etchant (45 pct HC1, 15 pct HNO3, 15 pct HF and 25 pct H2O) to remove the oxide film. Critical strain is applied by wrapping each specimen about a 1 3/4 in. round and subsequently straightening it against a flat surface. The high-purity aluminum sheet is sufficiently soft that this operation can be accomplished by ordinary finger pressure. The specimens are immediately annealed again at 640°C for 3 hr and reetched for examination. Ordinarily, considerable growth of certain of the grains will have occurred, and occasionally a single crystal will be produced on the first attempt. The procedure of alternately straining, annealing and etching is repeated until the majority of a batch of specimens contains usable crystal sizes. Typical examples are illustrated in Fig. 1. The greatest changes in crystal sizes are produced in the initial treatments. As the average crystal sizes get coarser in the later treatments, the sever- ity of the strain must be increased in order to produce grain boundary- migration. This increase in severity is effected by decreasing the diameter of the round used for straining (to 1 1/2 in., for example) and/or wrapping the specimens about the round twice, with opposite faces in contact with the round, before flattening. Usually the strain treatments described are not severe enough to produce nucleation in coarse grain high-purity aluminum. The growth of grains occurs by strain-induced grain-boundary migration. It has been observed that the grain boundaries move most readily during the first hour or so of each annealing treatment and that the rate of movement decreases with extended holding times at temperature. Prolonged annealing treatments are therefore not usually beneficial. Similarly, the rate of growth of each crystal appears to depend upon the orientation of the crystal with relation to those of its neighbors. Frequently island grains are formed after the initial heat treatment as the result of slow grain-boundary migration. These sometime become stationary during later heat treatments. Twin orientation interfaces are frequently developed during annealing. These imperfections can usually be removed by increasing the severity of strain to produce actual nucleation of new grains of more favorable orientation at the imperfection interfaces. The largest single crystals produced in our laboratory by the above method measured 4 by 1 by 0.050 in. Examination of Laue back-reflection patterns from a limited area of the specimens, gave no evidence of polygonization. Probably there is some indication of polygonization in the original grain area provided a more sensitive technique is used for detection. Experiments to produce wider specimens were less successful, possibly because wider sheets increase the complexity of the strains induced by deformation and promote widespread nucleation. Grain boundary migration occurs preferentially in a direction parallel to the longitudinal axis of the specimen. The choice of specimen geometry with respect to the rolling direction of the sheet appears to be immaterial in regard to the production of single crystals.

Jan 1, 1961

By J. A. Wates

Stope backfilling in South African gold mines uses the coarser cyclone fraction of the gold tailings. The disposal of the overflow from the cyclones, which is finer and of higher moisture content than normal gold tailings, presents some problems. This paper describes an investigation undertaken to define the parameters that are required for a quantitative and qualitative assessment of the operation and stability of slimes dams built of such material. However, seeing the investigation was conducted on the slimes from only one mine, it is recommended that, until a wider range of data becomes available, tests should be conducted for each individual mine.

Jan 1, 1988

By T. M. Morris

THE following data have been compiled from in- formation submitted by 24 plants in answer to a questionnaire sent to cyclone manufacturers and to companies using cyclones for wet classification, either for closed circuit grinding or for desliming.

Jan 8, 1957

By B. S. Spottiswoode

Lack of visibility makes it difficult for continuous miner (CM) operators to judge the desired sump depth. The resulting inaccuracies have proven to lead to significant production losses. This problem of measuring the depth of sump has been addressed in the past and a few measurement techniques have evolved. Despite various attempts, a suitable commercial depth of sump sensor does not yet exist. A system using the Doppler effect has been patented, developed and successfully tested. The method is non-intrusive and involves a beam of microwaves being projected obliquely at the roof. The received signal is analysed with respect to the transmitted signal, yielding the desired measure of displacement. Surface tests have revealed an accuracy of a few centimetres. Underground simulation tests on a load haulage dump (LHD) machine have verified the repeatability under the harsh conditions of interest. The system is presently being installed on a CM where it is to undergo a long-term performance evaluation. This paper presents the theory behind such a system, the hardware developed, the signal processing requirements and an analysis of the test results.

Sep 1, 2001

By Roland Heersink, Charles H. Wells

This paper discusses how a mill uses off-site data hosting approach to effectively utilize an entire suite of advanced applications to optimize daily operations, without incurring the overhead of on-site systems, staff and support. Details of the solution are provided, together with a live view of actual plant operations. Security and authentication mechanisms are also outlined so that users may gain an appreciation of the actual security of the remotely hosted data. A number of Web-hosted software applications provide direct connectivity to the database offering rapid and deterministic response times to clients. A 24x7 help-desk is available to authorized users from any Internet connected device. The paper shows how mill management advantageously use wireless PDA's to view what is going on at anytime and from anywhere. It concludes with a summary of how the approach is being used to speed decision-making and capture spot market opportunities.

Jan 1, 2002

By George M. Fowler, J. P. LYDEN

T HE relationship of geological structure to orebodies and to the great masses of chert in the Tri-State mining district is of such significance that it prompts a brief recital of the existing information regarding the various periods of structural deformation. We began to note a relationship between structure and orebodies early in our studies of the field, and further work revealed a like relationship of structure to the great masses of chert so commonly associated with the ore-

Jan 1, 1934

By Alexandre Monteiro

Alumina precursor powders can be precipitated from aqueous solutions, using hydrothermal decomposition of urea to deliver base homogeneously to the system. Primary particles agglomerate early in the process, generating a wide size distribution. The presence of a polymeric surfactant such as polyacrylate can suppress or delay agglomeration, reducing particle size and narrowing the size distribution. The stabilization of commercially available a-Alp03 powder with polyacrylate was studied, investigating the effects of polyacrylate molecular weight, ionic strength and temperature. The effect of aluminum concentration, polyacrylate molecular weight and urea concentration on the precipitation of alumina precursors in a sulfate- urea system in the presence of polyacrylate/polyacrylic acid was then studied. The hydrolysis kinetics were followed, and particle sizes were determined. Precipitates were further characterized using energy dispersive spectroscopy. The particle characteristics are discussed in terms of the process conditions.

Jan 1, 1994

The purpose of this study was to investigate the immobilization as a host for metallic pollutants (Cr, Cu, Pb, and Zn) by ettringite phase. Ettringite phase is produced through hydration reaction of calcium aluminate with gypsum. From the XRD patterns, it is known that the distance between spaces in 010 planes in ettringite crystal increase with an increase of ionic radius of heavy metal except Pb; no big difference is shown. For this reason, the d-value of 010 planes in ettringite crystal increased with the substitution of Cr, Cu and Zn having a big Al ironic radius. But in case of Pb, because the substitution occurred at calcium site, it does not influence to increase d-value of 010 planes.

Jan 1, 2006

By M. Wallin

Millions of tons of sludge from different metallurgical processes are produced worldwide annually, and the environmental impact of landfilling these often hazardous sludges stresses the need to understand their role as valuable resources. The current work explores the potential of producing a saleable low-phosphorous ferromanganese alloy by utilizing sludge from the silicomanganese industry together with an iron source. The aim of the project is to explore the feasibility and practical challenges related to reduction and dissolution of manganese and silicon from the sludge to liquid metal and slag. Parameters such as ratio of input material as well as the effect of adding limestone and coke to the mixture were explored by thermodynamic calculations and adapted experimentally. Results show that a ferromanganese alloy, in fact, can be formed, while silicon and calcium forms a complex slag that captures a significant amount of impurities.

By B. I. Hop

The f10wfield set up by the standard Hydro gas purging unit has been predicted by a numerical model. In addition turbulent trajectories of gas bubbles released from the rotor are predicted. Here the deposition rate of inclusions on the bubble surface is allowed to depend on local conditions. Bubbles passing regions with strong pressure gradients, such as close to the rotor, will experience large slip velocities and large deposition rates. This model can deal with any distribution of bubble sizes and inclusions. The results found from the multidimensional flow predictions are discussed in relation to what can be obtained from a much simpler metallurgical engineering approach. The differences between these two approaches to predict the same process will be discussed. The model predictions are compared to experimental results for removal of SiC-particles from aluminium.

Jan 1, 1996

By Ruth A. Maurer, Steven L. Capt. Van Drew

Coal preparation for a company having several sources of coal and several contracts for sale of coal was modeled. The objective was to minimize wash loss by selecting the quantity of coal to be supplied from each source and the appropriate washbox specific gravity setting to yield contract quality for a given shipment. constraints inposed by silo and stockpile sizes, plant and rehandling capacities, and varying coal quality specifications were included in the model. Solution is by iterative linear programming on an Apple II.

Jan 1, 1987

By D Suppel, Y Miezitis, S Jaireth

The competition between various options for the use of land is ever increasing. Commonly in Australia large tracts of land were un-encumbered by sweeping land use option limitations, but this situation has been rapidly altering in recent decades as governments are obliged to maximise the utility of the land for a broad range of competing interests. While the interests of miners have always been considered, the effects on limiting access to land for exploration and possible mining have not always been effectively incorporated into decision-making processes. As a result the challenge for national and state organisations representing these interests has been to develop a transparent process to allow for the mineral potential of an area to be systematically assessed and for information to be presented for use by specialists and non-specialists. Government agencies are called upon to implement government policy but also to provide accurate and meaningful advice which can assist in policy and land use decisions. Commonly timeframes are short and information can be less than complete. Nevertheless on-going decisions are made based upon the best available understanding. It is in this operational framework that the methods described in this paper are set. The paper describes a process for quickly and systematically providing advice on mineral potential for use by government agencies and ultimately the community within tight time and resource constraints. It is a method of combining the accumulated knowledge about mineral resources and their potential and presenting this information in an easily accessible form which can be used in a negotiation and policy development environment. Development of the method was undertaken to meet the needs of the Regional Forestry Agreement process in Australia. The method has been applied to study areas in New South Wales, Tasmania, Western Australia and elsewhere. Examples in this paper are taken from north eastern New South Wales.

Jan 1, 1999

By Neal Schwartz, Robert De Saro, Richard Rosenthal, Ed Kear

"A Stack Melter has been installed and is currently operating at Lexington Die Casting. The Stack Melter consists of a 1 meter (3 foot) diameter refractory tube, 2 meters (7 feet) high. Specification ingots are continuously fed to the top of the melter and piled to nearly the top. A burner fires through the scrap which melts the lower portion and preheats the upper portion. As the lower portion is melted, it is drawn out and the upper preheated scrap falls to a lower level where it in tum melts. The molten metal is fed to one of two holding furnaces for eventual delivery to a casting machine.The Stack Melter's energy use is approximately 2900 joules/g (1,250 Btu/lbm), resulting in an overall energy savings of about 58%. This energy savings is brought about primarily because the flue gases preheat the scrap and the flue gas temperature is dropped to well under 528°C (1000°F)."

Jan 1, 2000

GWILLIAM H. CLAMER* (Philadelphia, Pa.).-Sulphur is not so detrimental in its effect if oxygen is also present, so that in sulphur-carrying bronzes and brasses, it is advantageous to maintain a certain percentage of oxygen. As a matter of fact, it would be possible sometimes to correct difficulties by actually adding oxygen. If the cathodes were charged directly into an electric furnace in a neutral or reducing atmosphere, a very high grade of copper would result by a simple melting operation. This would very largely eliminate the loss occasioned by melting in a reverberatory furnace. In such a furnace a large amount of slag is produced during the oxidizing stage of refining. Notwithstanding the fact that melting in an electric furnace might be somewhat more expensive than melting in a fuel furnace, the ultimate result would be a saving and the production of a very high grade of copper.

Jan 1, 1919

By Frank P. Frandina, Diane R. Hirsch, David P. Field, Colin R. Weeks

To accommodate growth in air service and to follow the Master Plan for long-term airport development, the Metropolitan Washington Airports Authority established thed2 Development Program at Washington Dulles International Airport. A sub-surface Automated People Mover (APM) System is under construction to replace the Mobile Lounges as the primary people mover system at Dulles. To minimize disruption to airport operations the majority of the APM System’s crossings of Taxi lanes will be undertaken using Tunnel Boring Machines (TBM) or the New Austrian Tunneling Method (NATM). This paper explores the planning and design of these shallow tunnel segments for future generation aircraft loads, within the constraints of minimal construction access under post 9/11 security requirements and the context of the overall airport expansion program.

Jan 1, 2005

Faced with low prices and weak demand in an oversupplied market, the Australian coal industry must seek to further reduce its costs. The paper examines minesite competitiveness of the open cut coal industry in Australia with some references to the coal operations of M.I.M. Holdings Limited. The make-up of F.O.R. mine costs is analysed in order to identify where efforts should be directed to maintain competitiveness. The scope for mine site improvements through changes to working practices, the application of new technology and cost management is examined.

Jan 1, 1987

By Maria Thornhill, Rolf Arne Kleiv

INTRODUCTION The last decade has given rise to an increasing number of deep-sea mining concepts (DSMCs) outlining technical solutions for the production chain from seafloor mining to mineral or metal extraction. The vast technological and logistical challenges coupled with immature but rapidly evolving technology has spawned a great variety in proposed concepts, and the exact implications of the phrase ‘best available technology’ is very much an open question. DSMCs differ significantly with respect to choice of technology, technological readiness level, degree of resource utilization, logistics, OPEX and CAPEX requirements, overall profitability, legal and political implications, not to mention environmental impact. Hence, a system for classifying concepts could provide a useful identification and structuring tool when performing economic, judicial or environmental assessments of DSMCs, as well as offering a general terminology to describe concepts sharing fundamental traits. This abstract proposes a DSMC classification system based on how a concept makes use of mineral separation at the different stages in the ore’s journey from the deposit to the ocean surface and ultimately to onshore facilities. Mineral separation, as a process step, is the key factor in determining both the state and mass flow of materials along the production chain and has, as such, a decisive effect on economy and environmental impact of any deep-sea mining project. A DSMC that is based on bringing the entire volume of broken ore to onshore facilities for processing will look very different from a concept based on pre-concentration (i.e. mineral separation) at the seafloor. Whereas the latter offers savings in the form of reduced energy cost for vertical transport, it also represents a substantial additional technological challenge. Furthermore, whether or not a concept relies on mineral processing at the seafloor or on a floating facility at the ocean surface above the deposit also determines the point at which mineral separation waste (i.e. tailings) must be managed. Different concepts offer different opportunities for tailings deposition, and are at the same time bound by different requirements.

Jan 1, 2018

By S. Kelebek, E. Yalcin

"Diethylenetriamine (DETA) and/or triethylenetetramine (TETA) are reagents that can generally be categorized under ""flotation modifiers"". These polyamines are known to be effective for the deactivation/depression of pyrrhotite that is present in Canadian nickel-copper sulphide ores in large quantities. Recent bench scale testing on some of these complex ores indicated that chalcopyrite flotation can also be adversely affected under certain conditions involving polyamines, which may be taken to be an evidence of their specific affinity towards chalcopyrite. In general, DETA shows no significant depressant action on chalcopyrite while TETA's promotion of hydrophilicity for this mineral has been observed even in the presence of xanthate. This prompted an investigation on thermodynamic equilibria involving these polyamines and copper ions. Results serve a useful purpose to identify conditions for deactivation phenomena. CuDETA2+ and CuTETA2+ chelates as products of sequestration have large predominance areas covering a wide range of redox and pH conditions, where copper xanthate species are not stable, especially in the presence of TETA."

Jan 1, 2009

By Gordon DM

Tyres account for 25-30 per cent of the operating costs of large capacity haul units as used in open-cut mines.Tyre operating costs can be substantially reduced and often contained in real terms by applying knowledge that is now available.This paper describes certain specific advances in tyre management, namely batching, bias adjustment, cumulative plotting and the so-called "pressure-temperature" system of tyre pressure control, originated on the Mt Newman Mining Company's Newman minesite, and discusses the contribution that each has made to improving tyre management and reducing costs.

Jan 1, 1983

Seven legendary figures of American mining will be enshrined in the National Mining Hall of Fame in ceremonies on Saturday, Sept. 7 at the Little America Hotel in Salt Lake City, UT. The 15th annual induction banquet will begin with a reception at 6 pm, followed at 7 pm by the dinner and the program. Of the seven inductees, one is living. He is Alexander Murray (Bud) Wilson, 80, of Los Altos, CA. Wilson led Utah Construction (later Utah International) to become one of the world’s most diversified and successful mining companies in the 1960s and 1970s. It was acquired by General Electric in 1976.

Jan 1, 2002